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1. 发明授权

US06187836B1 Compositions featuring cationically active and free radically active functional groups, and methods for polymerizing such compositions 失效
标题翻译：具有阳离子活性和自由基活性官能团的组合物，以及聚合这种组合物的方法
公开(公告)号：US06187836B1
公开(公告)日：2001-02-13
申请号：US09092550
申请日：1998-06-05
申请人： Joel D. Oxman , Matthew C. Trom , Dwight W. Jacobs
发明人： Joel D. Oxman , Matthew C. Trom , Dwight W. Jacobs
IPC分类号： C08F248
CPC分类号： A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/087 , C08G59/68 , C08G65/105 , Y10S522/908 , C08L63/00 , C08L33/00
摘要： Photopolymerizable compositions that include free radically active and cationically active functional groups, and methods for polymerizing such compositions, in which the onset of cationic polymerization is controllably delayed to extend the time between formation of a moldable gel and formation of a hardened solid.
摘要翻译：包括游离的自由基活性和阳离子活性官能团的光聚合组合物和聚合这种组合物的方法，其中阳离子聚合的开始被可控地延迟以延长形成可模制凝胶和形成硬化固体之间的时间。

2. 发明授权

US06306926B1 Radiopaque cationically polymerizable compositions comprising a radiopacifying filler, and method for polymerizing same 有权
标题翻译：包含放射性填料的不透射线的阳离子聚合性组合物及其聚合方法
公开(公告)号：US06306926B1
公开(公告)日：2001-10-23
申请号：US09168051
申请日：1998-10-07
申请人： Kathyrn R. Bretscher , Richard P. Rusin , Bradley D. Craig , Sumita B. Mitra , Joel D. Oxman , Janis R. Gust , Cheryl A. Hayne , James W. Westberg , Matthew C. Trom , Brant U. Kolb , Dwight W. Jacobs , David A. Kaisaki , James A. Baker
发明人： Kathyrn R. Bretscher , Richard P. Rusin , Bradley D. Craig , Sumita B. Mitra , Joel D. Oxman , Janis R. Gust , Cheryl A. Hayne , James W. Westberg , Matthew C. Trom , Brant U. Kolb , Dwight W. Jacobs , David A. Kaisaki , James A. Baker
IPC分类号： A61K6087
CPC分类号： A61K6/083 , A61K6/0073 , A61K6/087 , C01P2006/12 , C08K3/013 , C09C1/00 , C09C1/3045 , C09C1/40 , Y10S522/908 , Y10T428/2993 , C08L33/00 , C08L63/00
摘要： Polymerizable compositions that include: (a) a cationically active functional group; (b) an initiation system capable of initiating cationic polymerization of the cationically active functional group; and (c) a filler composition that includes various radiopacifying fillers in an amount sufficient to render the polymerizable composition radiopaque. Components (a), (b), and (c) are selected such that the polymerizable composition polymerizes to form a polymerized composition having a Barcol hardness, measured using a GYZJ-935 meter, of at least 10 within 30 minutes following initiation of the cationically active functional group at a reaction temperature of 25° C.
摘要翻译：可聚合组合物，其包括：（a）阳离子活性官能团; （b）能够引发阳离子活性官能团的阳离子聚合的引发体系; 和（c）包含足以使可聚合组合物不透射线的量的各种放射性填料的填料组合物。选择组分（a），（b）和（c），使得可聚合组合物聚合以形成具有Barcol硬度的聚合组合物，其在使用GYZJ-935米测量时在30分钟内至少10分钟阳离子活性官能团的反应温度为25℃

3. 发明授权

US6159012A Process for treating hard tissues 有权
标题翻译：硬组织治疗方法
公开(公告)号：US6159012A
公开(公告)日：2000-12-12
申请号：US387449
申请日：1999-09-01
申请人： Joel D. Oxman , Hoa T. Bui , Dwight W. Jacobs
发明人： Joel D. Oxman , Hoa T. Bui , Dwight W. Jacobs
IPC分类号： A61K6/00 , A61K6/083 , A61K6/087 , A61B17/06 , A61C5/00 , A61K6/08 , C08L63/00
CPC分类号： A61K6/0023 , Y10S522/908
摘要： In a first aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a composition that includes a cationically active functional group, a free radically active functional group, and a polymerization initiator capable of initiating free radical polymerization, where the number of moles of cationically active functional groups per gram of composition is no greater than about 0.0075; and (b) exposing the composition to polymerization conditions to form an adhesive bonded to the hard tissue.In a second aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a first polymerizable composition that includes a free radically active functional group and a polymerization initiator capable of initiating free radical polymerization, but is essentially free of polymerizable components having cationically active functional groups and is capable of forming an adhesive bonded to the hard tissue upon exposure to polymerization conditions; (b) applying a second polymerizable composition; and (c) exposing the second composition to polymerization conditions to form a hardened composition adhered to the hard tissue. The second composition includes (i) a cationically active functional group and (ii) an polymerization initiator capable of initiating cationic polymerization.
摘要翻译：第一方面，一种硬组织处理方法，包括：（a）向硬组织施加包含阳离子活性官能团，自由基活性官能团和能引发自由基聚合的聚合引发剂的组合物，其中每克组合物中阳离子活性官能团的摩尔数不大于约0.0075; 和（b）将组合物暴露于聚合条件以形成粘合到硬组织的粘合剂。在第二方面，一种硬组织处理方法，包括：（a）向硬组织施加包含自由基活性官能团的第一可聚合组合物和能引发自由基聚合的聚合引发剂，但基本上不含可聚合的具有阳离子活性官能团的组分并且能够在暴露于聚合条件时形成粘合到硬组织的粘合剂; （b）施加第二可聚合组合物; 和（c）将第二组合物暴露于聚合条件以形成粘附到硬组织的硬化组合物。第二组合物包括（i）阳离子活性官能团和（ii）能够引发阳离子聚合的聚合引发剂。

4. 发明授权

US6043295A Ternary photoinitiator system for curing of epoxy resins 有权
标题翻译：用于固化环氧树脂的三元光引发剂体系
公开(公告)号：US6043295A
公开(公告)日：2000-03-28
申请号：US362410
申请日：1999-07-28
申请人： Joel D. Oxman , Dwight W. Jacobs
发明人： Joel D. Oxman , Dwight W. Jacobs
IPC分类号： A61K6/00 , A61K6/087 , C08F2/50 , C08G59/40 , G03F7/004 , G03F7/029 , G03F7/038 , A61K6/08 , G03C1/73
CPC分类号： A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/087 , G03F7/029 , G03F7/038 , Y10S522/908
摘要： Photocurable, addition polymerizable compositions contain an epoxy resin and a photoinitiator system containing (a) an epoxy resin and (b) a photoinitiator system comprising: (i) an iodonium salt; (ii) a visible light sensitizer; and (iii) an electron donor compound, wherein the photoinitiator system has a photoinduced potential of at least about 0 mV relative to a standard solution of 2.9.times.10.sup.-5 moles/g diphenyl iodonium hexafluoroantimonate and 1.5.times.10.sup.-5 moles/g camphorquinone in 2-butanone. The compositions cure on exposure to light in the visible spectrum and are useful in a variety of applications, including dental adhesives and composites.
摘要翻译：可光固化的可加成聚合组合物含有环氧树脂和含有（a）环氧树脂的光引发剂体系和（b）光引发剂体系，其包含：（ⅰ）碘鎓盐; （ii）可见光敏化剂; 和（iii）电子给体化合物，其中光引发剂体系相对于2.9×10 -5摩尔/ g二苯基碘鎓六氟锑酸盐和1.5×10-5摩尔/ g樟脑醌的标准溶液，具有至少约0mV的光诱导电位丁酮。组合物在可见光谱下暴露于光下固化，并且可用于各种应用，包括牙科粘合剂和复合材料。

5. 发明授权

US5998495A Ternary photoinitiator system for curing of epoxy/polyol resin compositions 失效
标题翻译：用于固化环氧/多元醇树脂组合物的三元光引发剂体系
公开(公告)号：US5998495A
公开(公告)日：1999-12-07
申请号：US840093
申请日：1997-04-11
申请人： Joel D. Oxman , Dwight W. Jacobs
发明人： Joel D. Oxman , Dwight W. Jacobs
IPC分类号： A61K6/00 , A61K6/087 , C08F2/50 , C08G59/40 , C08G65/28 , G03F7/004 , G03F7/029 , G03F7/038 , C08L63/10
CPC分类号： A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/087 , G03F7/029 , G03F7/038 , Y10S522/908
摘要： Photocurable, addition polymerizable compositions contain an epoxy resin and a photoinitiator system containing (a) an epoxy resin, (b) a hydroxyl containing material and (c) a photoinitiator system comprising: (i) an iodonium salt; (ii) a visible light sensitizer; and (iii) an electron donor compound, wherein the photoinitiator system has a photoinduced potential of at least about 100 mV relative to a standard solution of 2.9.times.10.sup.-5 moles/g diphenyl iodonium hexafluoroantimonate and 1.5.times.10.sup.-5 moles/g camphorquinone in 2-butanone. The compositions cure on exposure to light in the visible spectrum and are useful in a variety of applications, including dental adhesives and composites.
摘要翻译：可光固化的可加成聚合组合物含有环氧树脂和含有（a）环氧树脂，（b）含羟基物质和（c）光引发剂体系的光引发剂体系，其包含：（ⅰ）碘鎓盐; （ii）可见光敏化剂; 和（iii）电子给体化合物，其中光引发剂体系相对于2.9×10-5摩尔/ g二苯基碘鎓六氟锑酸盐和1.5×10-5摩尔/ g樟脑醌的标准溶液，具有至少约100mV的光诱导电位丁酮。组合物在可见光谱下暴露于光下固化，并且可用于各种应用，包括牙科粘合剂和复合材料。

6. 发明授权

US5814682A Method of luting a provisional prosthetic device using a glass ionomer cement system and kit therefor 失效
标题翻译：使用玻璃离子交联聚合物水泥系统及其试剂盒来修补临时假体装置的方法
公开(公告)号：US5814682A
公开(公告)日：1998-09-29
申请号：US663727
申请日：1996-06-14
申请人： Richard P. Rusin , Paula D. Ario , Dwight W. Jacobs , Joel D. Oxman , Sumita B. Mitra , Ronald M. Randklev
发明人： Richard P. Rusin , Paula D. Ario , Dwight W. Jacobs , Joel D. Oxman , Sumita B. Mitra , Ronald M. Randklev
IPC分类号： A61K6/00 , A61K6/083 , C08K3/34
CPC分类号： A61K6/0091 , A61K6/0023
摘要： The present invention provides a method of luting a provisional prosthetic device to tooth structure using glass ionomer cement systems having reduced bulk shear adhesion. The invention also provides a kit for luting a prosthetic device to tooth structure. The kit contains at least three containers of glass ionomer luting cement compositions. The kit advantageously can be utilized for providing both a provisional and a permanent luting cement depending upon which components are admixed.
摘要翻译：本发明提供了一种使用具有减小的体积剪切粘合力的玻璃离聚物粘合剂体系将临时假体装置向牙齿结构提供的方法。本发明还提供了一种用于将假体装置向牙齿结构排出的套件。该试剂盒包含至少三个玻璃离子交换胶粘剂组合物的容器。该试剂盒有利地可以用于提供临时和永久性的水泥浆，取决于混合哪些组分。

7. 发明授权

US06187833B1 Ternary photoinitiator system for curing of epoxy/polyol resin composition 有权
标题翻译：用于固化环氧树脂/多元醇树脂组合物的三元光引发剂体系
公开(公告)号：US06187833B1
公开(公告)日：2001-02-13
申请号：US09362621
申请日：1999-07-28
申请人： Joel D. Oxman , Dwight W. Jacobs
发明人： Joel D. Oxman , Dwight W. Jacobs
IPC分类号： C08F250
CPC分类号： A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/087 , G03F7/029 , G03F7/038 , Y10S522/908 , C08L63/00 , C08L33/00
摘要： Photocurable, addition polymerizable compositions contain an epoxy resin and a photoinitiator system containing (a) an epoxy resin, (b) a hydroxyl containing material and (c) a photoinitiator system comprising: (i) an iodonium salt; (ii) a visible light sensitizer; and (iii) an electron donor compound, wherein the photoinitiator system has a photoinduced potential of at least about 100 mV relative to a standard solution of 2.9×10−5 moles/g diphenyl iodonium hexafluoroantimonate and 1.5×10−5 moles/g camphorquinone in 2-butanone. The compositions cure on exposure to light in the visible spectrum and are useful in a variety of applications, including dental adhesives and composites.
摘要翻译：可光固化的可加成聚合组合物含有环氧树脂和含有（a）环氧树脂，（b）含羟基物质和（c）光引发剂体系的光引发剂体系，其包含：（ⅰ）碘鎓盐; （ii）可见光敏化剂; 和（iii）电子给体化合物，其中光引发剂体系相对于2.9×10-5摩尔/ g二苯基碘鎓六氟锑酸盐和1.5×10-5摩尔/ g樟脑醌的标准溶液，具有至少约100mV的光诱导电位丁酮。组合物在可见光谱下暴露于光下固化，并且可用于各种应用，包括牙科粘合剂和复合材料。

8. 发明授权

US5980253A Process for treating hard tissues 失效
公开(公告)号：US5980253A
公开(公告)日：1999-11-09
申请号：US5885
申请日：1998-01-12
申请人： Joel D. Oxman , Hoa T. Bui , Dwight W. Jacobs
发明人： Joel D. Oxman , Hoa T. Bui , Dwight W. Jacobs
IPC分类号： A61K6/00 , A61K6/083 , A61K6/087 , A61B17/06 , A61C5/00 , A61K6/08 , C08L63/00
CPC分类号： A61K6/0023 , Y10S522/908
摘要： In a first aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a composition that includes a cationically active functional group, a free radically active functional group, and a polymerization initiator capable of initiating free radical polymerization, where the number of moles of cationically active functional groups per gram of composition is no greater than about 0.0075; and (b) exposing the composition to polymerization conditions to form an adhesive bonded to the hard tissue.In a second aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a first polymerizable composition that includes a free radically active functional group and a polymerization initiator capable of initiating free radical polymerization, but is essentially free of polymerizable components having cationically active functional groups and is capable of forming an adhesive bonded to the hard tissue upon exposure to polymerization conditions; (b) applying a second polymerizable composition; and (c) exposing the second composition to polymerization conditions to form a hardened composition adhered to the hard tissue. The second composition includes (i) a cationically active functional group and (ii) an polymerization initiator capable of initiating cationic polymerization.

9. 发明授权

US6025406A Ternary photoinitiator system for curing of epoxy resins 失效
公开(公告)号：US6025406A
公开(公告)日：2000-02-15
申请号：US838835
申请日：1997-04-11
申请人： Joel D. Oxman , Dwight W. Jacobs
发明人： Joel D. Oxman , Dwight W. Jacobs
IPC分类号： A61K6/00 , A61K6/087 , C08F2/50 , C08G59/40 , G03F7/004 , G03F7/029 , G03F7/038 , A61K6/08 , C08G65/04
CPC分类号： A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/087 , G03F7/029 , G03F7/038 , Y10S522/908
摘要： Photocurable, addition polymerizable compositions contain an epoxy resin and a photoinitiator system containing (a) an epoxy resin and (b) a photoinitiator system comprising: (i) an iodonium salt; (ii) a visible light sensitizer; and (iii) an electron donor compound, wherein the photoinitiator system has a photoinduced potential of at least about 0 mV relative to a standard solution of 2.9.times.10.sup.-5 moles/g diphenyl iodonium hexafluoroantimonate and 1.5.times.10.sup.-5 moles/g camphorquinone in 2-butanone. The compositions cure on exposure to light in the visible spectrum and are useful in a variety of applications, including dental adhesives and composites.

10. 发明授权

US08906981B2 Dental compositions comprising semi-crystalline resin and nanocluster filler 有权
标题翻译：包含半结晶树脂和纳米团簇填料的牙科组合物
公开(公告)号：US08906981B2
公开(公告)日：2014-12-09
申请号：US13814974
申请日：2011-08-31
申请人： Jie Yang , Naimul Karim , Todd D. Jones , Dwight W. Jacobs
发明人： Jie Yang , Naimul Karim , Todd D. Jones , Dwight W. Jacobs
IPC分类号： A61K6/083 , A61C13/00 , A61C5/08 , C08L33/10 , C08L67/07 , A61K6/087 , A61K6/00
CPC分类号： A61K6/087 , A61C5/70 , A61C13/00 , A61K6/0002 , A61K6/0073 , A61K6/083 , C08L67/07 , C08L33/10
摘要： Curable dental compositions, dental articles, and methods of making or using such compositions or articles are described. In one embodiment, the curable dental restoration composition comprises a resin system comprising a free-radically polymerizable semi-crystalline resin having a molecular weight no greater than 3000 g/mole and at least 50 wt-% of nanocluster filler.
摘要翻译：描述了可固化的牙科组合物，牙科用品以及制造或使用这些组合物或制品的方法。在一个实施方案中，可固化牙齿修复组合物包含树脂体系，其包含分子量不大于3000g / mol和至少50wt％的纳米团簇填料的可自由基聚合的半结晶树脂。

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