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1. 发明授权

US06221150B1 Perylene compounds and pigment preparations 失效
标题翻译：苝化合物和颜料制剂
公开(公告)号：US06221150B1
公开(公告)日：2001-04-24
申请号：US09255252
申请日：1999-02-22
申请人： Joachim Weber , Manfred Urban , Erwin Dietz
发明人： Joachim Weber , Manfred Urban , Erwin Dietz
IPC分类号： C07D47106
CPC分类号： C07D471/06 , C09B5/62 , C09B67/0033
摘要： The present invention relates to pigment dispersants of the formula (I) in which Z1 is a radical of the formula (Ia) —[X—Y]q—[X1—Y1]r—[X2—NH]sH (Ia) in which X, X1 and X2 are identical or different and are a branched or unbranched C2-C6-alkylene radical or a C5-C7-cycloalkylene radical which can be substituted by from 1 to 4 C1-C4-alkyl radicals, hydroxyl radicals, and/or by from 1 to 2 further C5-C7-cycloalkyl radicals; Y and Y1 are identical or different and are an NH—, —O— or N(C1-C6-alkyl) group, q is a number from 1 to 6, r and s independently of one another are a number from 0 to 6, but are not simultaneously zero; and Z is defined as Z1, Z2 or Z3, where Z2 is a radical of the formula (Ib) —[X—O]q1—[X1—O]qH (Ib) in which q1 is a number from 0 to 6, and Z3 is hydrogen, hydroxyl, amino or C1-C6-alkyl where the alkyl group can be substituted by from 1 to 4 substituents from the group consisting of Cl, Br, CN, OH, C6H5, carbamoyl, C1-C4-acyl, C1-C4-alkoxy and NR2R3, and to pigment preparations comprising organic base pigments and pigment dispersants, and to prepared pigment formulations prepared from the pigment preparations.
摘要翻译：本发明涉及式（I）的颜料分散剂，其中Z 1是式（Ia）的基团，其中X，X 1和X 2相同或不同，并且是支链或非支链的C 2 -C 6 - 亚烷基或C 5 - 可以被1至4个C 1 -C 4烷基，羟基自由基和/或1至2个其它C 5 -C 7环烷基取代的C 7 - 亚环烷基; Y和Y 1相同或不同，为NH - ，-O-或N（C 1 -C 6 - 烷基）基团，q为1至6的数，r和s彼此独立地为0至6的数，但不同时为零; Z定义为Z 1，Z 2或Z 3，其中Z 2是式（Ib）的基团，其中q 1为0至6的数，Z 3为氢，羟基，氨基或C 1 -C 6烷基，其中烷基可以由C1，Br，CN，OH，C6H5，氨基甲酰基，C1-C4-酰基，C1-C4-烷氧基和NR2R3组成的组中的1至4个取代基取代，以及包含有机基础颜料和颜料分散剂，并制备由颜料制剂制备的颜料制剂。

2. 发明授权

US06521756B2 Process for preparing perylene-3,4,9,10-tetracarboxylic diimide in transparent pigment form 有权
标题翻译：以透明颜料形式制备苝-3,4,9,10-四羧酸二酰亚胺的方法
公开(公告)号：US06521756B2
公开(公告)日：2003-02-18
申请号：US09777211
申请日：2001-02-05
申请人： Joachim Weber , Gerhard Wilker , Manfred Urban , Martin Böhmer , Erwin Dietz
发明人： Joachim Weber , Gerhard Wilker , Manfred Urban , Martin Böhmer , Erwin Dietz
IPC分类号： C07D47106
CPC分类号： C09B5/62 , C09B67/0022
摘要： The present invention provides a process for preparing transparent perylimide pigments of the formula (I) in which u is a number from 0 to 8 and, if u>0, E is a chlorine or bromine atom and, where u>1, may be a combination thereof, which comprises wet-grinding a crude perylimide pigment in a liquid medium in a stirred ballmill operated at a power density of from 1.0 kW per liter of milling space and at a stirrer tip speed of more than 12 m/s under the action of grinding media having a diameter of less than or equal to 0.9 mm, and isolating the resulting pigment.
摘要翻译：本发明提供制备式（I）的透明苝酰亚胺颜料的方法，其中0至8的数，如果u> 0，E是氯或溴原子，并且其中u> 1可以是其组合包括在搅拌球磨机中在液体介质中湿法研磨粗己二酰亚胺颜料，该搅拌球磨机以每升研磨空间的功率密度为1.0kW，搅拌器末端速度大于12m / s 的直径小于或等于0.9mm的研磨介质，并分离所得颜料。

3. 发明授权

US07056378B2 Method for producing vattable organic pigments 失效
标题翻译：生产有机颜料的方法
公开(公告)号：US07056378B2
公开(公告)日：2006-06-06
申请号：US10511857
申请日：2003-03-17
申请人： Joachim Weber , Manfred Urban , Erwin Dietz
发明人： Joachim Weber , Manfred Urban , Erwin Dietz
IPC分类号： C09B67/04 , C09B67/28 , C08K5/00
CPC分类号： C09B67/0096 , C09B67/0022 , C09B67/0077
摘要： The invention relates to a method for producing vattable organic pigments. The invention is characterized in that an agueous or an aqueous-organic suspension of a coarse crystalline raw mineral is vatted and re-oxidised, and the pigment suspension is ground to a diameter equal to or less than 0.9 mm during vatting and/or during oxidation by means of an agitator ball mill, which is operated at a power density of more than 1.0 KW per litre per grinding chamber and at an agitator peripheral speed of more than 12 m/s, using grinding bodies.
摘要翻译：本发明涉及一种生产有机颜料的方法。本发明的特征在于，将粗结晶原料矿物的水性有机悬浮液或水 - 有机悬浮液进行包覆并再次氧化，并且在蒸煮和/或氧化期间将颜料悬浮液研磨至等于或小于0.9mm的直径通过搅拌器球磨机，其使用研磨体在功率密度大于1.0KW / l每研磨室和搅拌器圆周速度大于12m / s的条件下操作。

4. 发明申请

US20050229817A1 Method for producing vattable organic pigments 失效
标题翻译：生产有机颜料的方法
公开(公告)号：US20050229817A1
公开(公告)日：2005-10-20
申请号：US10511857
申请日：2003-03-17
申请人： Joachim Weber , Manfred Urban , Erwin Dietz
发明人： Joachim Weber , Manfred Urban , Erwin Dietz
IPC分类号： C09B67/04 , C09B67/00 , C09B67/28 , C09B67/54 , C08K5/00
CPC分类号： C09B67/0096 , C09B67/0022 , C09B67/0077
摘要： The invention relates to a method for producing vattable organic pigments. The invention is characterised in that an aqueous or an aqueous-organic suspension of a coarse crystalline raw mineral is vatted and re-oxidised, and the pigment suspension is ground to a diameter equal to or less than 0.9 mm during vatting and/or during oxidation by means of an agitator ball mill, which is operated at a power density of more than 1.0 KW per litre per grinding chamber and at an agitator peripheral speed of more than 12 m/s, using grinding bodies.
摘要翻译：本发明涉及一种生产有机颜料的方法。本发明的特征在于，将粗结晶原料矿物的水性有机悬浮液或水 - 有机悬浮液进行水化和再次氧化，并且在蒸煮和/或氧化期间将颜料悬浮液研磨至等于或小于0.9mm的直径通过搅拌器球磨机，其使用研磨体在功率密度大于1.0KW / l每研磨室和搅拌器圆周速度大于12m / s的条件下操作。

5. 发明授权

US06646126B2 Process for preparing perylene-3,4,9,10-tetracarboxylic diimide in transparent pigment form 有权
标题翻译：以透明颜料形式制备苝-3,4,9,10-四羧酸二酰亚胺的方法
公开(公告)号：US06646126B2
公开(公告)日：2003-11-11
申请号：US10323070
申请日：2002-12-18
申请人： Joachim Weber , Gerhard Wilker , Manfred Urban , Martin Böhmer , Erwin Dietz
发明人： Joachim Weber , Gerhard Wilker , Manfred Urban , Martin Böhmer , Erwin Dietz
IPC分类号： C07D47106
CPC分类号： C09B5/62 , C09B67/0022
摘要： The present invention provides a process for preparing transparent perylimide pigments of the formula (I): in which u is a number from 0 to 8 and, if u>0, E is a chlorine or bromine atom and, where u>1, may be a combination thereof, which comprises wet-grinding a crude perylimide pigment in a liquid medium in a stirred ballmill operated at a power density of from 1.0 kW per liter of milling space and at a stirrer tip speed of more than 12 m/s under the action of grinding media having a diameter of less than or equal to 0.9 mm, and isolating the resulting pigment.
摘要翻译：本发明提供了制备式（I）的透明苝酰亚胺颜料的方法：其中0是0至8的数，如果u> 0，E是氯或溴原子，并且其中u> 1，可以是其组合包括在搅拌球磨机中在液体介质中湿法研磨粗己二酰亚胺颜料，该搅拌球磨机以每升研磨空间的功率密度为1.0kW，搅拌器末端速度大于12m / s，在具有直径小于或等于0.9mm的研磨介质的作用，并分离所得颜料。

6. 发明授权

US06413309B1 Pigment preparations comprising two or more perylene compounds 失效
标题翻译：包含两种或更多种苝化合物的颜料制剂
公开(公告)号：US06413309B1
公开(公告)日：2002-07-02
申请号：US09491318
申请日：2000-01-25
申请人： Joachim Weber , Manfred Urban , Manfred Opravil , Erwin Dietz
发明人： Joachim Weber , Manfred Urban , Manfred Opravil , Erwin Dietz
IPC分类号： C09B6720
CPC分类号： C09B67/0034 , C09B67/0033
摘要： Pigment preparations comprising a) at least one organic base pigment, b1) at least one perylene pigment dispersant of the formula (I) and b2) at least one acidic, carboxyl- or sulfo-containing perylene pigment dispersant have advantageous rheological and coloristic properties.
摘要翻译：包含a）至少一种有机基础颜料，b1）至少一种式（I）的苝颜料分散剂和b2）至少一种含酸性，含羧基或含磺基的苝颜料分散剂具有有利的流变学和着色性质。

7. 发明授权

US5264034A Pigment preparations based on perylene compounds 失效
标题翻译：基于苝化合物的颜料制剂
公开(公告)号：US5264034A
公开(公告)日：1993-11-23
申请号：US829046
申请日：1992-03-06
申请人： Erwin Dietz , Manfred Urban
发明人： Erwin Dietz , Manfred Urban
IPC分类号： C09B5/62 , C09B67/20 , C09B67/22 , C09D7/12 , C09D11/02 , C09D11/10 , C09D161/20 , C09D161/28 , C07D471/06 , C07D491/06 , C07D493/06
CPC分类号： C09B67/0033
摘要： Pigment preparations consisting essentially of (a) at least one pigment based on perylene-3,4,9,10-tetracarboxylic dianhydride or on corresponding monoimides or diimides of tetracarboxylic acid monoanhydride, or a halogenation product thereof, (b) at least one pigment dispergent based on perylene-3,4,9,10-monoimide substituted on one or both imide nitrogen atoms by alkylene or arylene sulphonic or carboxylic acid groups or on corresponding diimides of tetracarboxylic acid monoanhydride, or a halogenation product thereof. The dispergents used appreciably enhance the key properties of perylene pigments, such as dispersibility, coloring power, stability to flocculation, transparency, rheological behavior and surface properties of the application medium. These new preparations are suitable for the pigmentation of high-quality lacquers and synthetic resins.
摘要翻译： PCT No.PCT / EP90 / 01311 Sec。 371日期：1992年3月6日 102（e）1992年3月6日PCT PCT 1990年8月9日PCT公布。出版物WO91 / 02034 日本1991年2月21日。基本上由（a）至少一种基于苝-3,4,9,10-四羧酸二酐或相应的四羧酸单酐的一酰亚胺或二酰亚胺的颜料或其卤化产物，（b）至少一种基于通过亚烷基或亚芳基磺酸或羧酸基团在一个或两个酰亚胺氮原子上取代的二萘嵌苯-3,4,9,10-单酰亚胺或相应的四羧酸单酸二酰亚胺或卤化反应的颜料分散体其产品。所使用的残余物明显增强了苝颜料的关键性能，例如分散性，着色力，絮凝稳定性，透明度，流变行为和表面性质。这些新制剂适用于高品质漆和合成树脂的着色。

8. 发明授权

US5662739A Use of fatty acid taurides for the dispersion of polycyclic pigments 失效
标题翻译：脂肪酸牛磺酸用于多环颜料分散体的使用
公开(公告)号：US5662739A
公开(公告)日：1997-09-02
申请号：US368898
申请日：1995-01-05
申请人： Manfred Urban , Erwin Dietz
发明人： Manfred Urban , Erwin Dietz
IPC分类号： C09B67/08 , B01F17/22 , B01F17/32 , C09B19/02 , C09B48/00 , C09B67/10 , C09B67/20 , C09B67/22 , C09B67/46
CPC分类号： C09B67/0014 , C09B19/02 , C09B48/00 , C09B67/0034 , C09B67/006 , C09B67/0065 , C09B67/0086
摘要： Readily dispersible polycyclic pigments from the class of the quinacridones and dioxazines are prepared by using a fatty acid tauride of the formula (I)R.sup.1 --CO--NR.sup.2 --(CH.sub.2).sub.n --SO.sub.3.sup.- M.sup.+(I)in whichR.sup.1 is a straight-chain or branched alkyl group having from 10 to 24 carbon atoms andR.sup.2 is a hydrogen atom or a C.sub.1 -C.sub.6 -alkyl group,M.sup.+ is a hydrogen ion, ammonium ion, alkali metal ion or alkaline earth metal ion and n is 1 or 2, or a mixture of at least two fatty acid taurides of the formula (I).
摘要翻译：通过使用式（I）的R1-CO-NR2-（CH2）n-SO3-M +（Ⅰ）的脂肪酸牛磺酸制备喹吖啶酮类和二恶嗪类的易分散多环颜料，其中R1是直链 - 具有10至24个碳原子的直链或支链烷基，R 2是氢原子或C 1 -C 6烷基，M +是氢离子，铵离子，碱金属离子或碱土金属离子，n是1或2 ，或式（I）的至少两种脂肪酸牛磺酸盐的混合物。

9. 发明授权

US5248774A Inner salts based on ammonium and sulfonate groups of perylene-3,4,9,10-tetracarboxylic and derivatives thereof 失效
标题翻译：基于亚磺酸3,4,10,10-四羧酸及其衍生物的氨基磺酸盐组合的内盐
公开(公告)号：US5248774A
公开(公告)日：1993-09-28
申请号：US855608
申请日：1992-03-20
申请人： Erwin Dietz , Manfred Urban
发明人： Erwin Dietz , Manfred Urban
IPC分类号： C07D471/06 , C09B5/62 , C09B57/00 , C09B67/22
CPC分类号： C09B5/62 , C09B67/0034
摘要： Perylenetetracarboxylic diimides which contain a radical in the same molecule on one imide nitrogen which acts as an anion but contain a radical on the other imide nitrogen which acts as a cation, and on this basis form inner salts, are available by reaction of sulfo-containing alkylamines with perylenetetracarboxylic monoanhydride monoalkylaminoalkylimides or by reaction of alkylaminoalkylamines with perylenetetracarboxylic monoanhydride monosulfoalkylimides. As a result of their characteristic structural principle, these novel perylene compounds have excellent dispersing properties, in particular for pigments of the same chemical classes of compounds and can even be used themselves as pigments (colorants) depending on the substituent.
摘要翻译：在相同分子中含有一个酰亚胺氮上的基团的苝四羧酸二酰亚胺，其作为阴离子但在另一个酰亚胺氮上含有基团，其作为阳离子，并且在此基础上形成内盐，可通过含有烷基胺与苝四羧酸单酐单烷基氨基烷基酰亚胺或烷基氨基烷基胺与苝四羧酸单酐单磺酰亚胺的反应。由于它们的特征结构原理，这些新颖的苝化合物具有优异的分散性能，特别是对于化合物相同化学类别的颜料，甚至可以根据取代基自身用作颜料（着色剂）。

10. 发明授权

US5112404A Pigment formulations, processes for their preparation and their use 失效
公开(公告)号：US5112404A
公开(公告)日：1992-05-12
申请号：US506564
申请日：1990-04-04
申请人： Andreas Sommer , Erwin Dietz , Manfred Urban
发明人： Andreas Sommer , Erwin Dietz , Manfred Urban
IPC分类号： C09B67/08 , C09B67/20 , C09C3/08 , C09D17/00
CPC分类号： C09D17/003 , C09B67/006
摘要： The invention relates to readily dispersible pigment formulations which are stable to flocculation and are used for pigmenting naturally occurring and synthetic materials, preferably paints and printing inks, plastics and lacquers, in particular stoving lacquers. The pigment formulations contain compounds of the general formula (I) ##STR1## in which Q.sup.1, Q.sup.2 and Q.sup.3 each denote --X--A, --OR.sup.1, --SR.sup.1, halogen, --NR.sup.2 R.sup.3 or a radical Q which is built up from up to 15 trivalent groups (Ia) such that in each case one group (Ia) is bonded via W to a free valency of the next group (Ia) or to the triazine ring of (I) and the other free valencies are bonded to --X--A, --O--R.sup.1, halogen or --NR.sup.2 R.sup.3, at least one radical --X--A being present in (I), and A stands for an aromatic system with 2 to 6 rings and at least 9 ring atoms, or stands for a group of 2 to 3 aromatic ring systems, bonded via O, S, CO, SO, SO.sub.2 or C.sub.1 -C.sub.12 -alkylene, of in each case 1 to 4 rings, A optionally also being substituted by C.sub.1 -C.sub.24 -alkyl, OR', halogen, NR'R", COOR', CONR'R", NR'COR", CN, CF.sub.3 or NO.sub.2, and R' and R" denote H or C.sub.1 -C.sub.12 -alkyl or, with N, a heterocyclic radical with 5 or 6 ring atoms, X stands for NR*, O or S, in which R* denotes H, C.sub.1 -C.sub.6 -alkyl, -hydroxyalkyl or -alkoxyalkyl or C.sub.5 -C.sub.7 -cycloalkyl, R.sup.1, R.sup.2 and R.sup.3 each stand for H, alkyl, alkenyl, cycloalkyl, aralkyl, heteroalkyl, or phenyl, optionally substituted by C.sub.1 -C.sub.12 -alkyl, halogen, OR.sup.4, NR.sup.4 R.sup.5 COOR.sup.4, CONR.sup.4 R.sup.5, NR.sup.5 COR.sup.4, CN, CF.sub.3, NO.sub.2 or --T(CH.sub.2).sub.p NR.sup.o R.sup.t, in which R.sup.4 and R.sup.5 denote H or alkyl and R.sup.o and R.sup.t denote alkyl, p denotes 1-6 and T denotes a direct bond or O, S, CO, SO, SO.sub.2, NR.sup.a, NR.sup.a CO, NR.sup.a SO.sub.2, SO.sub.2 NR.sup.a or CONR.sup.a, and R.sup.a denotes H or C.sub.1 -C.sub.12 -alkyl, or stand for C.sub.1 -C.sub.12 -hydroxyalkyl or -polyhydroxylkyl or alkyl which is interrupted once or several times by O and/or NR.sup.v, in which R.sup.v denotes H or alkyl, and can be substituted by a 5- or 6-membered heterocyclic ring, or R.sup.1 has the above mentioned meaning and R.sup.2 and R.sup.3 together with N, stand for a 5- or 6-membered ring of a heterocyclic system with 1 or 2 rings, W is Y.sup.1 --Y--Y.sup.1, in which Y denotes alkylene, optionally interrupted by O, S, NH, N(alkyl), CO, SO, SO.sub.2, C.sub.5 -C.sub.7 -cycloalkylene, C.sub.5 -C.sub.10 -arylene or heteroarylene with 5-7 ring atoms or a 1-3-nuclear carbocyclic or heterocyclic ring system with 5 to 14 ring atoms or two of the ring systems, which are linked via a direct bond or O, S, CO, SO or SO.sub.2, and Y.sup.1 denotes O, S or NR.sup.5, in which R.sup.5 denotes alkyl, hydroxyalkyl, alkoxyalkyl or cycloalkyl or, together with N--Y--N, a heterocyclic ring.The dispersing agents used can be prepared by reaction of cyanuric halides with corresponding compounds H--X--A, HOR.sup.1, HSR.sup.1, HNR.sup.2 R.sup.3 and/or HWH.

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