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1. 发明授权

US5910593A Highly selective process for the preparation of enantiomerically pure phenylsubstituted 1,4-dihydropyridine-3,5-dicarboxylic acid derivatives 有权
标题翻译：用于制备对映体纯的苯基取代的1,4-二氢吡啶-3,5-二羧酸衍生物的高选择性方法
公开(公告)号：US5910593A
公开(公告)日：1999-06-08
申请号：US158428
申请日：1998-09-21
申请人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
发明人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
IPC分类号： A61K31/4412 , A61P25/28 , C07D207/40 , C07D207/416 , C07D211/80 , C07D211/90 , C07D401/02 , C07D401/06 , C07D401/12 , C07D521/00
CPC分类号： C07D207/416 , C07D211/90 , C07D231/12 , C07D233/56 , C07D249/08 , C07D401/06 , C07D401/12
摘要： The present invention relates to a new highly selective process for the preparation of enantiomerically pure halogeno-phenyl-substituted 1,4-dihydropyridine-3,5-dicarboxylic esters of the general formula (I) ##STR1## in which R.sup.1 to R.sup.3 have the meanings given in the description.
摘要翻译：本发明涉及用于制备通式（I）的对映体纯的卤代苯基取代的1,4-二氢吡啶-3,5-二羧酸酯的新的高选择性方法，其中R 1至R 3具有如说明。

2. 再颁专利

USRE36607E Pyrrolidine compounds and process of preparing 有权
标题翻译：吡咯烷化合物及其制备方法
公开(公告)号：USRE36607E
公开(公告)日：2000-03-07
申请号：US276220
申请日：1999-03-25
申请人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
发明人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
IPC分类号： A61K31/4412 , A61P25/28 , C07D207/40 , C07D207/416 , C07D211/80 , C07D211/90 , C07D401/02 , C07D401/06 , C07D401/12 , C07D521/00
CPC分类号： C07D207/416 , C07D211/90 , C07D231/12 , C07D233/56 , C07D249/08 , C07D401/06 , C07D401/12
摘要： This invention relates to benzolididene compounds of the formula ##STR1## in which R.sup.2 represents the radical ##STR2## in which R.sup.4 and R.sup.5 are identical or different and denote halogen, cyano, ethinyl, trifluoromethoxy, methylthio, nitro, trifluoromethyl or straight-chain or branched alkyl, alkenyl, alkinyl or alkoxy having up to 4 carbon atoms, and one of the substituents optionally represents hydrogen,or a salt thereof.[...]..Iadd., andA represents hydrogen or straight-chain or branched alkyl having up to 8 carbon atoms, or represents phenyl or benzyl which are optionally substituted one to three times by identical or different substituents from the series consisting of hydroxyl, nitro, halogen, cyano, carboxyl, trifluoromethyl, trifluoromethoxy, straight-chain or branched alkoxy having up to 6 carbon atoms or by a group of the formula --NR.sup.6 R.sup.7 or --SO.sub.2 R.sup.8, in whichR.sup.6 and R.sup.7 are identical or different and denote hydrogen, phenyl or straight-chain or branched alkyl having up to 5 carbon atomsandR.sup.8 denotes straight-chain or branched alkyl having up to 4 carbon atoms or phenyl. .Iaddend.
摘要翻译：本发明涉及下式的苯偶姻化合物，其中R 2表示其中R 4和R 5相同或不同并且表示卤素，氰基，乙炔基，三氟甲氧基，甲硫基，硝基，三氟甲基或直链或支链烷基，烯基，炔基或具有至多4个碳原子的烷氧基，其中一个取代基任选代表氢或其盐[和]，A表示氢或具有至多8个碳原子的直链或支链烷基，或表示苯基或苄基，任选地被羟基，硝基，卤素，氰基，羧基，三氟甲基，三氟甲氧基，具有至多6个碳原子的直链或支链烷氧基或通过下式的基团取代的相同或不同的取代基取代一至三次： -NR6R7或-SO2R8，其中R6和R7相同或不同，表示氢，苯基或具有至多5个碳原子的直链或支链烷基，R8表示直链具有至多4个碳原子的直链或支链烷基或苯基。

3. 发明授权

US5700948A Pyrrolidine compounds and process of preparing 失效
标题翻译：吡咯烷化合物及其制备方法
公开(公告)号：US5700948A
公开(公告)日：1997-12-23
申请号：US563725
申请日：1995-11-28
申请人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
发明人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
IPC分类号： A61K31/4412 , A61P25/28 , C07D207/40 , C07D207/416 , C07D211/80 , C07D211/90 , C07D401/02 , C07D401/06 , C07D401/12 , C07D521/00
CPC分类号： C07D207/416 , C07D211/90 , C07D231/12 , C07D233/56 , C07D249/08 , C07D401/06 , C07D401/12
摘要： This invention relates to benzolididene compounds of the formula ##STR1## in which R.sup.2 represents the radical ##STR2## in which R.sup.4 and R.sup.5 are identical or different and denote halogen, cyano, ethinyl, trifluoromethoxy, methylthio, nitro, trifluoromethyl or straight-chain or branched alkyl, alkenyl, alkinyl or alkoxy having up to 4 carbon atoms, and one of the substituents optionally represents hydrogen, or a salt thereof.
摘要翻译：本发明涉及式（II）的苯偶姻化合物，其中R 2表示其中R 4和R 5相同或不同并表示卤素，氰基，乙炔基，三氟甲氧基，甲硫基，硝基，三氟甲基或直链的基团具有至多4个碳原子的链或支链烷基，烯基，炔基或烷氧基，其中一个取代基任选代表氢或其盐。

4. 发明授权

US5849924A Highly selective process for the preparation of enantiomerically pure phenyl-substituted 1,4-dihydropyridine-3,5-dicarboxylic acid derivatives 失效
标题翻译：用于制备对映体纯的苯基取代的1,4-二氢吡啶-3,5-二羧酸衍生物的高选择性方法
公开(公告)号：US5849924A
公开(公告)日：1998-12-15
申请号：US896275
申请日：1997-07-16
申请人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
发明人： Joachim Mittendorf , Peter Fey , Bodo Junge , Johannes Kaulen , Kai van Laak , Heinrich Meier , Rudolf Schohe-Loop
IPC分类号： A61K31/4412 , A61P25/28 , C07D207/40 , C07D207/416 , C07D211/80 , C07D211/90 , C07D401/02 , C07D401/06 , C07D401/12 , C07D521/00
CPC分类号： C07D207/416 , C07D211/90 , C07D231/12 , C07D233/56 , C07D249/08 , C07D401/06 , C07D401/12
摘要： The present invention relates to a new highly selective process for the preparation of enantiomerically pure halogeno-phenyl-substituted 1,4-dihydropyridine-3,5-dicarboxylic esters of the general formula (I) ##STR1## in which R.sup.1 to R.sup.3 have the meanings given in the description.
摘要翻译：本发明涉及用于制备通式（I）的对映体纯的卤代苯基取代的1,4-二氢吡啶-3,5-二羧酸酯的新的高选择性方法，其中R1至 R3具有说明书中给出的含义。

5. 发明授权

US07943644B2 Stabilization of iodine-containing biocides by means of special azole compounds 失效
标题翻译：通过特殊的唑化合物稳定含碘杀生物剂
公开(公告)号：US07943644B2
公开(公告)日：2011-05-17
申请号：US12281163
申请日：2007-02-21
申请人： Hermann Uhr , Johannes Kaulen , Thomas Jaetsch , Peter Spetmann
发明人： Hermann Uhr , Johannes Kaulen , Thomas Jaetsch , Peter Spetmann
IPC分类号： A61K31/41 , A61K47/00
CPC分类号： A01N47/12 , C09D5/14 , C09D167/08 , A01N2300/00 , C08L2666/28
摘要： Specific azole compounds are outstandingly suitable for stabilizing iodine-containing biocides in industrial materials, more particularly in paints based on alkyd resin.
摘要翻译：特定的唑类化合物特别适用于稳定工业材料中含碘杀生物剂，尤其适用于基于醇酸树脂的油漆。

6. 发明授权

US06673955B2 Preparation of triethyl phosphate 失效
标题翻译：磷酸三乙酯的制备
公开(公告)号：US06673955B2
公开(公告)日：2004-01-06
申请号：US10302543
申请日：2002-11-22
申请人： Karl-Heinz Mitschke , Kaspar Hallenberger , Ottfried Schlak , Johannes Kaulen
发明人： Karl-Heinz Mitschke , Kaspar Hallenberger , Ottfried Schlak , Johannes Kaulen
IPC分类号： C07F902
CPC分类号： C07F9/11
摘要： The invention relates to a process for preparing triethyl phosphate by reacting phosphorus oxychloride with a greater than stoichiometric quantity of ethanol under reduced pressure at temperatures of from 0 to 50° C. in a reaction vessel, wherein a) the volatile components resulting from the reaction are predominantly condensed by means of a reflux condenser and the remaining volatile components are passed into a scrubber filled with water, b) after the end of the reaction, the reaction mixture is separated distillatively in an outgassing column into a top product and a bottom product which predominantly comprises triethyl phosphate, c) the top product of the outgassing column is combined with the contents of the scrubber and d) the contents of the scrubber are separated distillatively in an azeotropic distillation to obtain water and ethanol as top product and the ethanol, preferably after dewatering, is preferably returned to the reaction.
摘要翻译：本发明涉及通过在反应容器中在0至50℃的温度下在减压下使磷酰氯与大于化学计量的乙醇反应来制备磷酸三乙酯的方法，其中a）由反应产生的挥发性组分为主要通过回流冷凝器冷凝，剩余的挥发性成分进入填充有水的洗涤器，b）在反应结束后，将反应混合物在脱气塔中蒸馏分离成顶部产物和底部产物，主要包括磷酸三乙酯，c）除气塔的顶部产物与洗涤器的内容物组合，d）洗涤器的内容物在共沸蒸馏中蒸馏分离，得到水和乙醇作为顶级产物和乙醇，优选在脱水，优选返回到反应中。

7. 发明授权

US4988823A Optically active oxiranes 失效
标题翻译：光学活性环氧乙烷
公开(公告)号：US4988823A
公开(公告)日：1991-01-29
申请号：US372062
申请日：1989-06-27
申请人： Johannes Kaulen
发明人： Johannes Kaulen
IPC分类号： A01N43/24 , C07B53/00 , C07C45/00 , C07C47/273 , C07C67/00 , C07C309/65 , C07D249/08 , C07D411/04 , C07D521/00
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08 , C07D411/04
摘要： Optically active oxiranes of the formula ##STR1## in which R represents substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl or represents substituted or unsubstituted phenyl, andR.sup.1, R.sup.2, R.sup.3, R.sup.4, R.sup.5 and R.sup.6 represent hydrogen or alkyl, at least one of the radicals representing alkyl, orR.sup.4 and R.sup.5 together represent alkanediyl, which is unsubstituted or substituted by alkyl, or R.sup.4 and R.sup.5 together with the adjacent carbon atoms represent a fused bicyclic hydrocarbon radical, which is unsubstituted or substituted by alkylare produced by reacting an enantiomerically pure oxathiane ketone of the formula ##STR2## with a sulphonium or sulphoxonium salt. The product can be converted to optically active 2-hydroxyethylazole derivatives of the formula ##STR3##
摘要翻译：式（I）的光学活性环氧乙烷，其中R表示取代或未取代的烷基，取代或未取代的环烷基或表示取代或未取代的苯基，且R 1，R 2，R 3，R 4，R 5和R 6表示氢或烷基，代表烷基的至少一个基团，或者R 4和R 5一起表示未被取代或被烷基取代的烷二基，或者R4和R5与相邻的碳原子一起表示稠合的双环烃基，其未被取代或被烷基取代通过将式（IMA）（II）的对映异构体纯的氧硫杂环己酮与锍盐或磺基锍盐反应。该产物可以转化成式（VI）的光学活性2-羟基乙唑衍生物，

8. 发明授权

US08002883B2 Amidoalkylamine-comprising azole compositions for protecting industrial materials 失效
标题翻译：酰氨基烷基胺的唑类组合物，用于保护工业材料
公开(公告)号：US08002883B2
公开(公告)日：2011-08-23
申请号：US12792907
申请日：2010-06-03
申请人： Bernd Koop , Martin Kugler , Andreas Böttcher , Johannes Kaulen
发明人： Bernd Koop , Martin Kugler , Andreas Böttcher , Johannes Kaulen
IPC分类号： A01N33/00 , A01N33/02 , A01N25/00 , A01N25/30 , A01N43/653 , A01P3/00 , B27K3/50 , C09D5/16
CPC分类号： A01N43/653 , B27K3/34 , B27K3/343 , B27K3/52 , A01N37/20 , A01N37/26 , A01N2300/00
摘要： Use of compositions comprising a) at least one azole and b) at least one amidoalkylamine of the formula (I), a salt and/or acid addition compound thereof, in which R1 represents optionally substituted C1-C40-alkyl or C2-C40-alkenyl, R2, R3 and R4 independently of one another represent hydrogen or C1-C8-alkyl and n represents an integer from 1 to 6 for protecting industrial materials against attack and/or destruction by microorganisms.
摘要翻译：使用包含a）至少一种唑和b）至少一种式（I）的酰氨基烷基胺，其盐和/或酸加成化合物，其中R 1表示任选取代的C 1 -C 40 - 烷基或C 2 -C 40 - 烯基，R 2，R 3和R 4彼此独立地表示氢或C 1 -C 8 - 烷基，n表示1至6的整数，用于保护工业材料免受微生物的攻击和/或破坏。

9. 发明申请

US20090140208A1 AQUEOUS CARBON BLACK FORMULATIONS FOR INK JET 审中-公开
标题翻译：用于墨水喷射的水性炭黑配方
公开(公告)号：US20090140208A1
公开(公告)日：2009-06-04
申请号：US12299800
申请日：2007-05-07
申请人： Johannes Kaulen , Erasmus Vogl
发明人： Johannes Kaulen , Erasmus Vogl
IPC分类号： C09K15/06 , C07C69/96
CPC分类号： C09K15/06 , A23L2/44 , A23L3/3463 , A23L3/3499 , A23L3/358 , C07C68/08 , C07C69/96
摘要： Finely divided solids are highly suitable for use as stabilizers for pyrocarbonic acid diesters, it being possible to use the mixtures obtained in this manner for preserving industrial materials and foodstuff.
摘要翻译：精细分散的固体非常适合用作热解碳酸二酯的稳定剂，可以使用以这种方式获得的混合物来保存工业材料和食品。

10. 发明申请

US20090104322A1 STABILIZATION OF DICARBONATE DIESTERS WITH PROTONIC ACIDS 有权
标题翻译：二氧化碳柴油与原子酸稳定
公开(公告)号：US20090104322A1
公开(公告)日：2009-04-23
申请号：US12297493
申请日：2007-04-11
申请人： Steffen Kahlert , Johannes Kaulen , Erasmus Vogl
发明人： Steffen Kahlert , Johannes Kaulen , Erasmus Vogl
IPC分类号： A23L3/34 , C07H3/02 , C07C59/265 , C07C59/245 , C07C59/255 , C07C53/08 , C07C309/29 , C07C309/04 , C07C69/96
CPC分类号： C07C68/08 , A23L2/44 , A23L3/3463 , A23L3/3517 , A23L3/358 , C12H1/14 , C07C69/96
摘要： By using protonic acids, diesters of dicarbonic acid may be stabilized against thermal and chemical decomposition over a relatively long period. Mixtures of diesters of dicarbonic acid and protonic acids are outstandingly suitable for preserving foods.
摘要翻译：通过使用质子酸，可以在相对长的时间内稳定二碳酸二酯以防止热和化学分解。二碳酸和质子酸二酯的混合物非常适合保存食物。

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