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1. 发明授权

US07273899B2 Materials and method for making splayed layered materials 失效
标题翻译：制作展开层状材料的材料和方法
公开(公告)号：US07273899B2
公开(公告)日：2007-09-25
申请号：US10254352
申请日：2002-09-25
申请人： Jin-Shan Wang , Xiaoru Wang , Samuel Chen , Thomas N. Blanton
发明人： Jin-Shan Wang , Xiaoru Wang , Samuel Chen , Thomas N. Blanton
IPC分类号： C08J3/12 , C08K9/04 , C08K3/34 , C04B33/04
CPC分类号： C08J3/205 , C08K3/01 , C08K7/00
摘要： The present invention relates to a splayed material comprising a layered material splayed with a particle having a diameter equal to or less than 3 micrometers. Another embodiment of the invention includes an article comprising a matrix and a layered material splayed with a polymeric particles dispersed in a medium. The invention also relates to methods for preparing these materials via mixing, milling and emulsifying a solvent borne polymer with a surfactant. A further method describes a method for preparing a nanocomposite from a splayant particle prepared by combining an emulsion polymerization monomer and a surfactant dispersible in a medium wherein the monomer is not dispersible in the medium.
摘要翻译：本发明涉及一种展开材料，其包括用直径等于或小于3微米的颗粒展开的层状材料。本发明的另一个实施方案包括包含基质和分散在介质中的聚合物颗粒展开的层状材料的制品。本发明还涉及通过混合，研磨和乳化溶剂型聚合物与表面活性剂制备这些材料的方法。另外的方法描述了一种通过将乳液聚合单体和可分散在其中单体不能分散在介质中的介质中分散的表面活性剂组合而制备的帆布颗粒制备纳米复合材料的方法。

2. 发明授权

US07166657B2 Article utilizing highly branched polymers to splay layered materials 失效
标题翻译：使用高支化聚合物喷涂层状材料的文章
公开(公告)号：US07166657B2
公开(公告)日：2007-01-23
申请号：US10099092
申请日：2002-03-15
申请人： Yuan Q. Rao , Jin-Shan Wang , Thomas N. Blanton , Samuel Chen , Robert J. Kress , Debasis Majumdar
发明人： Yuan Q. Rao , Jin-Shan Wang , Thomas N. Blanton , Samuel Chen , Robert J. Kress , Debasis Majumdar
IPC分类号： C08K9/04 , C08K3/34 , C08L67/00
CPC分类号： C01B33/44
摘要： The present invention relates to a splayed layered material comprising a layered material splayed with a highly branched polymer. Additional embodiments include a splayed layered material comprising a matrix polymer and layered material wherein said layered material is splayed with a highly branched polymer, an article comprising the splayed layered material in a matrix, and an exfoliated material.
摘要翻译：本发明涉及一种展开的层状材料，其包括用高支化聚合物展开的层状材料。另外的实施方案包括显示的层状材料，其包含基质聚合物和层状材料，其中所述层状材料用高度支化的聚合物显影，包含基质中的被张开的层状材料的制品和剥离材料。

3. 发明授权

US07655212B2 Production of silver sulfate grains using a fluorinated additive 有权
标题翻译：使用氟化添加剂生产硫酸银颗粒
公开(公告)号：US07655212B2
公开(公告)日：2010-02-02
申请号：US12101237
申请日：2008-04-11
申请人： David W. Sandford , Thomas N. Blanton
发明人： David W. Sandford , Thomas N. Blanton
IPC分类号： C01G5/00 , C08K3/00
CPC分类号： C01G5/00 , A61K8/23 , A61Q11/00 , A61Q17/005 , C01P2004/61 , C08K3/30 , C08K5/41 , C09C1/00
摘要： An aqueous precipitation process for the preparation of particles comprising primarily silver sulfate, comprising reacting an aqueous soluble silver salt and an aqueous soluble source of inorganic sulfate ion in an agitated precipitation reactor vessel and precipitating particles comprising primarily silver sulfate, wherein the reaction and precipitation are performed in the presence of an aqueous soluble fluorinated additive, the amount of additive being a minor molar percentage, relative to the molar amount of silver sulfate precipitated, and effective to result in precipitation of particles comprising primarily silver sulfate having a mean grain-size of less than 50 micrometers.
摘要翻译：一种用于制备主要包含硫酸银的颗粒的水性沉淀方法，包括将水溶性银盐和无机硫酸根离子的水溶性来源在搅拌的沉淀反应器容器中反应并沉淀出主要包含硫酸银的颗粒，其中反应和沉淀是在水溶性氟化添加剂的存在下进行，相对于沉淀的硫酸银的摩尔量，添加剂的量为次摩尔百分数，并且有效地导致主要包含平均粒径为小于50微米。

4. 发明授权

US07321036B2 Process for preparing aluminum trisquinoline complex 有权
标题翻译：制备三羟基喹啉络合物的方法
公开(公告)号：US07321036B2
公开(公告)日：2008-01-22
申请号：US10834827
申请日：2004-04-29
申请人： Thomas N. Blanton , Manju Rajeswaran
发明人： Thomas N. Blanton , Manju Rajeswaran
IPC分类号： C07D401/14 , C07D215/30
CPC分类号： C07F5/069
摘要： A process for forming the facial isomer of an aluminum trisquinoline complex comprises heating the solid aluminum trisquinoline complex material at a temperature at least 50° C. below the melting point temperature of the solid for a time sufficient to convert the aluminum trisquinoline complex to at least 99 mol % of one polymorph of the facial-isomer that fluoresces with a maximum intensity below 510 nm.
摘要翻译：形成三羟基喹啉铝复合物的面部异构体的方法包括在固体的熔点温度以下至少50℃的温度下加热固体三羟基喹啉络合物材料足够的时间以将铝三羟基喹啉复合物转化为至少 99mol％的面部异构体的一个多晶型物以最大强度在510nm以下发荧光。

5. 发明授权

US07169484B2 Process for forming a composite including an aluminum trisquinoline complex 有权
标题翻译：用于形成包含三羟基喹啉铝复合物的复合物的方法
公开(公告)号：US07169484B2
公开(公告)日：2007-01-30
申请号：US10834621
申请日：2004-04-29
申请人： Manju Rajeswaran , Thomas N. Blanton , Ching W. Tang
发明人： Manju Rajeswaran , Thomas N. Blanton , Ching W. Tang
IPC分类号： H01L51/50 , H05B33/14
CPC分类号： C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , C09K2211/1029 , C09K2211/107 , C09K2211/186 , H01L51/0026 , H01L51/0081 , H01L51/5012 , Y10S428/917
摘要： A process for forming a film of the facial-isomer of an aluminum trisquinoline complex comprises depositing a film of an aluminum trisquinoline complex on a support, depositing an inert barrier layer over the layer of aluminum trisquinoline complex that encapsulates aluminum trisquinoline complex to form a multilayer composite, and then heating the composite at a temperature below the melting point temperature of the complex for a time sufficient to convert the aluminum trisquinoline complex to at least 99 mol % of the facial-isomer that fluoresces with a maximum emission intensity below 510 nm. The product has a blue hue.
摘要翻译：形成铝三喹啉复合物的面体异构体的膜的方法包括在载体上沉积三羟基喹啉铝复合物的膜，在包封铝三羟基喹啉复合物的铝层上沉积惰性阻挡层，形成多层复合物，然后在低于复合物熔点温度的温度下将复合物加热足够的时间，足以将铝三喹啉复合物转化为具有低于510nm的最大发射强度发荧光的至少99mol％的面状异构体。该产品具有蓝色色调。

6. 发明授权

US06686407B2 Exfoliated polystyrene-clay nanocomposite comprising star-shaped polymer 失效
公开(公告)号：US06686407B2
公开(公告)日：2004-02-03
申请号：US10155256
申请日：2002-05-24
申请人： Douglas R. Robello , Nori Yamaguchi , Thomas N. Blanton , Craig L. Barnes
发明人： Douglas R. Robello , Nori Yamaguchi , Thomas N. Blanton , Craig L. Barnes
IPC分类号： C08L334
CPC分类号： B82Y30/00 , C08K9/04 , C08L25/06 , C08L2205/02 , Y10S977/712 , Y10S977/778 , Y10S977/788 , Y10S977/844 , Y10S977/847 , C08L2666/04
摘要： A nanocomposite made with an inorganic layered material and a star-shaped polystyrene that can be blended with normal linear polystyrene is disclosed. The inorganic layered material can have an exfoliated structure, substantially exfoliated, or intercalated structure. The exfoliated structure can result in significantly improved physical properties, even with only a very low content of clay. The invention is also directed to a process that can be used to make the compositions of the present invention. In one embodiment, a physical mixture of clay and star polymer is prepared and then the mixture is heated for several hours, preferably under high-shear mixing, to increase the rate of exfoliation, after which mostly inexpensive commodity linear polystyrene polymer completes the composition.

7. 发明授权

US06475696B2 Imaging elements with nanocomposite containing supports 有权
标题翻译：具有纳米复合材料的成像元件
公开(公告)号：US06475696B2
公开(公告)日：2002-11-05
申请号：US09751192
申请日：2000-12-28
申请人： Debasis Majumdar , Narasimharao Dontula , Dennis J. Massa , Thomas N. Blanton , Jose L. Garcia , Eric E. Arrington , Thaddeus S. Gula
发明人： Debasis Majumdar , Narasimharao Dontula , Dennis J. Massa , Thomas N. Blanton , Jose L. Garcia , Eric E. Arrington , Thaddeus S. Gula
IPC分类号： G03C1765
CPC分类号： G03C1/795 , G03C1/79
摘要： The invention relates to an imaging member comprising an image layer and a support comprising at least one layer comprising an inorganic particle having an aspect ratio of at least 10 to 1, a lateral dimension of between 0.01 &mgr;m and 5 &mgr;m, and a vertical dimension between 0. 5 nm and 10 nm, and polymeric resin.
摘要翻译：本发明涉及一种成像构件，其包括图像层和支撑体，该支撑体包括至少一层，该层包含长宽比为至少10:1，横向尺寸为0.01μm和5μm之间的无机颗粒，以及垂直尺寸为 0.5nm和10nm，以及聚合树脂。

8. 发明授权

US6120984A Solid electrolyte particles comprising MAg.sub.4 I.sub.5 失效
公开(公告)号：US6120984A
公开(公告)日：2000-09-19
申请号：US98968
申请日：1998-06-17
申请人： Thomas N. Blanton , Seshadri Jagannathan , Mark E. Irving
发明人： Thomas N. Blanton , Seshadri Jagannathan , Mark E. Irving
IPC分类号： G03C1/498
CPC分类号： G03C1/49818
摘要： This invention comprises a process for generating particles of MAg.sub.4 I.sub.5, wherein M is a monovalent cation, which comprises dissolving AgI and MI in a polar solvent followed by precipitating particles of MAg.sub.4 I.sub.5 by adding the solution to a nonpolar solvent. The resulting MAg.sub.4 I.sub.5 is in the form of anisotropic crystalline particles. The MAg.sub.4 I.sub.5 particles can be used in the preparation of a photothermographic element. The invention also comprises method of preparing a stable aqueous emulsion of MAg.sub.4 I.sub.5 particles.

9. 发明授权

US5891611A Clay containing antistatic layer for photographic paper 失效
标题翻译：粘土含有相纸的抗静电层
公开(公告)号：US5891611A
公开(公告)日：1999-04-06
申请号：US937685
申请日：1997-09-29
申请人： Debasis Majumdar , Sharon M. Melpolder , Charles C. Anderson , Paul A. Christian , Thomas N. Blanton
发明人： Debasis Majumdar , Sharon M. Melpolder , Charles C. Anderson , Paul A. Christian , Thomas N. Blanton
IPC分类号： G03C1/79 , D21H19/22 , D21H19/40 , D21H19/58 , D21H19/62 , D21H19/82 , D21H19/84 , G03C1/85 , G03C1/95 , G03C1/89
CPC分类号： G03C1/853 , D21H19/84 , D21H19/22 , D21H19/40 , D21H19/58 , D21H19/62 , D21H19/828 , Y10T428/31667
摘要： The present invention is a photographic paper which includes a paper sheet with a polyolefin resin layer on each surface of the paper sheet. The photographic paper includes a print retaining antistatic layer having a dry coverage of from 80 mg/m.sup.2 to 1000 mg/m.sup.2 on one of the free surfaces of the polyolefin layers. The print retaining antistatic layer includes a smectite clay, and a polymeric binder wherein the polymeric binder can sufficiently intercalate inside or exfoliate the smectite clay. The photographic paper can include a silver halide light sensitive emulsion layer on the other free surface.
摘要翻译：本发明是一种在纸张的每个表面上具有聚烯烃树脂层的纸张的相纸。照相纸包括在聚烯烃层的一个自由表面上具有80mg / m 2至1000mg / m 2的干覆盖率的印刷保留抗静电层。印刷保持抗静电层包括蒙脱石粘土和聚合物粘合剂，其中聚合物粘合剂可以充分地嵌入或剥落蒙脱石粘土。照相纸可以在另一自由表面上包括卤化银感光乳剂层。

10. 发明授权

US07931880B2 Production of silver sulfate grains using inorganic additives 有权
标题翻译：使用无机添加剂生产硫酸银颗粒
公开(公告)号：US07931880B2
公开(公告)日：2011-04-26
申请号：US11694582
申请日：2007-03-30
申请人： David W. Sandford , Thomas N. Blanton
发明人： David W. Sandford , Thomas N. Blanton
IPC分类号： C01G5/00
CPC分类号： C01G5/00 , A61K8/19 , A61K2800/412 , A61Q11/00 , A61Q17/005 , C01P2004/61 , Y10T428/256
摘要： An aqueous precipitation process for the preparation of particles comprising primarily silver sulfate, comprising reacting an aqueous soluble silver salt and an aqueous soluble source of inorganic sulfate ion in an agitated precipitation reactor vessel and precipitating particles comprising primarily silver sulfate, wherein the reaction and precipitation are performed in the presence of an aqueous soluble inorganic additive compound containing a cation capable of forming a sulfate salt that is less soluble than silver sulfate or a halide anion or an oxyanion capable of forming a silver salt that is less soluble than silver sulfate, the amount of additive being a minor molar percentage, relative to the molar amount of silver sulfate precipitated, and effective to result in precipitation of particles comprising primarily silver sulfate having a mean grain-size of less than 70 micrometers.
摘要翻译：一种用于制备主要包含硫酸银的颗粒的水性沉淀方法，包括将水溶性银盐和无机硫酸根离子的水溶性来源在搅拌的沉淀反应器容器中反应并沉淀出主要包含硫酸银的颗粒，其中反应和沉淀是在含有能够形成硫酸盐的阳离子的水溶性无机添加剂化合物的存在下进行，所述阳离子能够形成比硫酸银更易溶解的硫酸盐，或能够形成比硫酸银溶解度低的银盐的卤化物阴离子或氧阴离子，的添加剂相对于沉淀的硫酸银的摩尔量是次摩尔百分比，并且有效地导致主要包含平均粒度小于70微米的硫酸银的颗粒的沉淀。

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