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1. 发明授权

US07018757B2 Photoconductor materials based on complex of charge generating material 失效
标题翻译：基于电荷产生材料复合材料的感光体材料
公开(公告)号：US07018757B2
公开(公告)日：2006-03-28
申请号：US10356683
申请日：2003-01-31
申请人： Jiayi Zhu , Zbigniew Tokarski , James A. Baker , Ronald J. Moudry , David T. Ask , Nusrallah Jubran , Kam W. Law
发明人： Jiayi Zhu , Zbigniew Tokarski , James A. Baker , Ronald J. Moudry , David T. Ask , Nusrallah Jubran , Kam W. Law
IPC分类号： G03G5/047
CPC分类号： G03G5/047 , G03G5/06 , G03G5/0696 , G03G7/0033
摘要： An electrophotographic article having a complex of charge generating material and at least one transfer material selected from the group consisting of electron transfer material and hole transfer material is formed by admixing the charge generating material, at least one transfer material, and an organic binder in a solvent to form a coatable dispersion comprising a complex of charge generating material and said at least one transfer material; and coating said coatable dispersion onto a conductive substrate to form a charge transfer layer on the electrophotoconductive article. A novel S-form titanyl oxyphthalocyanine is also preferred, the novel form displaying major peaks of Bragg's 2theta angle to the CuK-alpha characteristic X-ray (wavelength 1.541 Angstrom) at least at 9.5±0.2 degrees, 9.7±0.2 degrees, 11.7±0.2 degrees, 13.5±0.2 degrees, (optionally at 21±0.2 degrees and/or 23.5±0.2 degrees,) 24.1±0.2 degrees, 26.4±0.2 degrees, and 27.3±0.2 degrees group. Additional peaks, approaching or equivalent to major peaks, may also be present as 15.0, 15.3 and 16.0±0.2 degrees.
摘要翻译：通过将电荷产生材料，至少一种转印材料和有机粘合剂混合在一起形成具有电荷产生材料和选自电子转移材料和空穴转移材料的至少一种转移材料的复合物的电子照相制品，溶剂以形成包含电荷产生材料和所述至少一种转移材料的复合物的可涂覆分散体; 并将所述可涂覆分散体涂覆到导电基材上以在电子导电制品上形成电荷转移层。一种新型的S型氧基氧代酞菁也是优选的，这种形式显示了布拉格2θ角与CuKα特征X射线（波长1.541埃）至少9.5±0.2度，9.7±0.2度，11.7± 24度±0.2度，26.4±0.2度和27.3±0.2度组（可选地为21±0.2度和/或23.5±0.2度）。接近或等同于主峰的附加峰也可以以15.0,15.3和16.0±0.2度的形式存在。

2. 发明授权

US06815132B2 Photoconductor materials based on new phase of titanyl phthalocyanine 失效
标题翻译：基于氧化钛酞菁新相的感光体材料
公开(公告)号：US06815132B2
公开(公告)日：2004-11-09
申请号：US10328697
申请日：2002-12-24
申请人： Jiayi Zhu , Zbigniew Tokarski , James A. Baker , Ronald J. Moudry , David T. Ask , Nusrallah Jubran , Kam W. Law
发明人： Jiayi Zhu , Zbigniew Tokarski , James A. Baker , Ronald J. Moudry , David T. Ask , Nusrallah Jubran , Kam W. Law
IPC分类号： G03G506
CPC分类号： C09B67/0026 , G03G5/047 , G03G5/0696 , G03G7/0033
摘要： A crystalline phase of titanyl oxyphthalocyanine, referred to herein as the S-phase, has an internal blend of lattice arrangements is provided by treatment of the gamma-form of titanyl oxyphthalocyanine. The S-phase is a truly new phase, and not a mixture of particles of various phases (e.g., combinations of the beta-phase and the gamma-phase), with internal lattice distributions of atoms and molecules forming a new, non-continuous, non-uniform lattice structure. The x-ray spectrum shows a blend of diffraction peaks, having peaks that have previously been distinctly present only collectively among various crystalline forms of titanyl oxyphthalocyanine, but can now be provided in a single crystalline form. The visible spectra show significant absorption differences. The novel S-form titanyl oxyphthalocyanine is also used in a photoconductor displaying major peaks of Bragg's 2 theta angle to the CuK-alpha characteristic X-ray (wavelength 1.541 Angstrom) at least at 9.5±0.2 degrees, 9.7±0.2 degrees, 11.7±0.2 degrees, 13.5±0.2 degrees, (optionally at 21±0.2 degrees and/or 23.5±0.2 degrees,) 24.1±0.2 degrees, 26.4±0.2 degrees, and 27.3±0.2 degrees group. Additional peaks, approaching or equivalent to major peaks, may also be present as 15.0, 15.3 and 16.0±0.2 degrees.
摘要翻译：钛氧基氧酞菁的结晶相，本文称为S相，具有格子排列的内部共混物，通过处理γ型氧钛氧基酞菁得到。 S相是一个真正的新阶段，而不是各种相的粒子的混合物（例如，β相和γ相的组合），原子和分子的内部晶格分布形成新的非连续的，不均匀的晶格结构。 X射线光谱显示了衍射峰的混合物，其具有先前已经明确存在于各种结晶形式的氧钛氧酞菁中的峰，但现在可以单晶形式提供。可见光谱显示出显着的吸收差异。新型的S型氧基氧代酞菁也用于显示布拉格2θ角与CuK-α特征X射线（波长1.541埃）的主峰至少9.5±0.2度，9.7±0.2度，11.7± 24度±0.2度，26.4±0.2度和27.3±0.2度组（可选地为21±0.2度和/或23.5±0.2度）。接近或等同于主峰的附加峰也可以以15.0,15.3和16.0±0.2度的形式存在。

3. 发明授权

US06869741B2 Electrophotographic photoreceptors with novel overcoats 有权
标题翻译：具有新颖大衣的电子照相感光体
公开(公告)号：US06869741B2
公开(公告)日：2005-03-22
申请号：US10167932
申请日：2002-06-10
申请人： Jiayi Zhu , Zbigniew Tokarski , Ronald J. Moudry , Kristine A. Fordahl , David T. Ask , Jonas Sidaravicius , Edmundas Montrimas , Kam W. Law , Valentas Gaidelis
发明人： Jiayi Zhu , Zbigniew Tokarski , Ronald J. Moudry , Kristine A. Fordahl , David T. Ask , Jonas Sidaravicius , Edmundas Montrimas , Kam W. Law , Valentas Gaidelis
IPC分类号： G03G5/07 , G03G5/05 , G03G5/06 , G03G5/147
CPC分类号： G03G5/0661 , G03G5/0532 , G03G5/0542 , G03G5/0546 , G03G5/0616 , G03G5/0648 , G03G5/1473 , G03G5/14734 , G03G5/14791 , G03G5/14795
摘要： A photoreceptor with good mechanical and physical properties is provided with an overcoat layer comprising a copolymer of an α,β-ethylenically unsaturated carboxylic acid and an α,β-ethylenically unsaturated monomer wherein the weight percent of the α,β-ethylenically unsaturated carboxylic-acid is at least 25% up to 99% of the copolymer. The copolymer may comprise an α,β-ethylenically unsaturated carboxylic acid and an α,β-ethylenically unsaturated monomer wherein the copolymer has an acid value of at least 150 mg KOH/g the copolymer. The copolymer may be present in a blend with a second polymer or copolymer comprised of units derived from a second α,β-ethylenically unsaturated monomer that is different from the an α,β-ethylenically unsaturated carboxylic acid and/or the α,β-ethylenically unsaturated monomer. The copolymer or the copolymer blend may be present in a layer that is crosslinked or crosslinkable, the crosslinking being effected through a distinct crosslinking agent that reacts with group(s) on the an α,β-ethylenically unsaturated carboxylic acid or the α,β-ethylenically unsaturated monomer.
摘要翻译：提供具有良好机械和物理性质的感光体，其具有包含α，β-烯键式不饱和羧酸和α，β-烯属不饱和单体的共聚物的外涂层，其中α，β-烯键式不饱和羧酸 - 酸是至少25％至99％的共聚物。共聚物可以包含α，β-烯属不饱和羧酸和α，β-烯属不饱和单体，其中共聚物的酸值至少为150mg KOH / g。共聚物可以与第二聚合物或共聚物一起存在，所述第二聚合物或共聚物由衍生自不同于α，β-烯键式不饱和羧酸和/或α，β-烯属不饱和羧酸的第二α，β-烯属不饱和单体的单元组成，烯属不饱和单体。共聚物或共聚物共混物可以存在于交联或可交联的层中，交联通过与α，β-烯属不饱和羧酸或α，β上的基团反应的不同交联剂进行烯属不饱和单体。

4. 发明授权

US06890693B2 Organophotoreceptor with an electron transport layer 失效
标题翻译：具有电子传递层的有机光感受器
公开(公告)号：US06890693B2
公开(公告)日：2005-05-10
申请号：US10396536
申请日：2003-03-25
申请人： Jiayi Zhu , Nusrallah Jubran , Zbigniew Tokarski , James A. Baker , Ronald J. Moudry
发明人： Jiayi Zhu , Nusrallah Jubran , Zbigniew Tokarski , James A. Baker , Ronald J. Moudry
IPC分类号： G03G5/043 , G03G5/047 , G03G5/06 , G03G5/14 , G03G5/147
CPC分类号： G03G5/047 , G03G5/0696 , G03G5/142 , G03G5/14708
摘要： Improved organophotoreceptor have an electrically conductive substrate, a charge generation layer comprising a charge generation compound and optionally a charge transport compound, and an overcoat layer comprising an electron transport compound wherein the charge generation layer is between the overcoat layer and the electrically conductive substrate. The organophotoreceptor can optionally comprise a charge transport layer and/or other desired layers. The organophotoreceptors are useful in electrophotographic imaging apparatuses and corresponding processes.
摘要翻译：改进的有机光感受器具有导电基底，电荷产生层，其包含电荷产生化合物和任选的电荷输送化合物，以及包含电子传输化合物的外涂层，其中电荷产生层位于外涂层和导电基底之间。有机光感受器可任选地包含电荷传输层和/或其它所需的层。有机光感受器在电子照相成像设备和相应的工艺中是有用的。

5. 发明授权

US07183028B2 Organophotoreceptor with novel charge transport compounds having an epoxy group 失效
标题翻译：具有环氧基团的新型电荷传输化合物的有机光感受器
公开(公告)号：US07183028B2
公开(公告)日：2007-02-27
申请号：US10749164
申请日：2003-12-30
申请人： Zbigniew Tokarski , Nusrallah Jubran , Kam W. Law , Vytautas Getautis , Maryte Daskeviciene , Edmundas Montrimas , Janina Gavutiene
发明人： Zbigniew Tokarski , Nusrallah Jubran , Kam W. Law , Vytautas Getautis , Maryte Daskeviciene , Edmundas Montrimas , Janina Gavutiene
IPC分类号： G03G5/06 , C07D303/08
CPC分类号： C07D303/22 , C07D455/00 , G03G5/0616 , G03G5/0625 , G03G5/0638 , G03G5/0648 , G03G5/0661
摘要： Improved organophotoreceptor comprises an electrically conductive substrate and a photoconductive element on the electrically conductive substrate, the photoconductive element comprising: (a) a charge transport material having the formula where R1, R2, R3, and R4 are, independently, an alkyl group, an alkaryl group, an aryl group, or a part of a cyclic group; R5 is hydrogen, an alkyl group, an alkaryl group, an aryl group, or a heterocyclic group; X comprises an aromatic group, such as an aryl group or an aromatic heterocyclic group; Y is a linking group; and Z comprises an epoxy group; and (b) a charge generating compound. Corresponding electrophotographic apparatuses and imaging methods are described.
摘要翻译：改进的有机光感受器包括在导电衬底上的导电衬底和光电导元件，光电导元件包括：（a）具有下式的电荷传输材料：其中R 1，R 2， R 3，R 3和R 4分别独立地为烷基，烷芳基，芳基或环状基团的一部分; R 5是氢，烷基，烷芳基，芳基或杂环基; X包括芳基，例如芳基或芳族杂环基; Y是连接组; Z包含环氧基; 和（b）电荷产生化合物。描述相应的电子照相设备和成像方法。

6. 发明授权

US07090953B2 Organophotoreceptor with a charge transport compound having an epoxy group 有权
标题翻译：具有环氧基的电荷输送化合物的有机光感受器
公开(公告)号：US07090953B2
公开(公告)日：2006-08-15
申请号：US10772068
申请日：2004-02-04
申请人： Vytautas Getautis , Maryte Daskeviciene , Tadas Malinauskas , Edmundas Montrimas , Jonas Sidaravicius , Zbigniew Tokarski , Nusrallah Jubran , Kam W. Law
发明人： Vytautas Getautis , Maryte Daskeviciene , Tadas Malinauskas , Edmundas Montrimas , Jonas Sidaravicius , Zbigniew Tokarski , Nusrallah Jubran , Kam W. Law
IPC分类号： G03G15/06
CPC分类号： C07D405/14 , C07D303/36 , C07D407/12 , G03G5/06 , G03G5/0612 , G03G5/0618 , G03G5/0625 , G03G5/0696
摘要： This invention relates to a novel organophotoreceptor that comprises an electrically conductive substrate and photoconductive element on the electrically conductive substrate, the photoconductive element having a) a charge transport compound having the formula R1 is an aromatic group, an alkyl group, an alkenyl group, or a heterocyclic group; R2 comprises an (N,N-disubstituted)arylamine group; R3 comprises an epoxy group; R4 is H, an aromatic group, an alkyl group, an alkenyl group, or a heterocyclic group; and X is a first linking group; and (b) a charge generating compound. The epoxy group can be reacted with a functional group within the polymer to form a polymeric charge transport compound either directly or through a crosslinking agent. Corresponding electrophotographic apparatuses and imaging methods are also described.
摘要翻译：本发明涉及一种新型的有机光感受器，其包括在导电基底上的导电基底和光电导元件，所述光电导元件具有a）具有式R 1的电荷传输化合物是芳族基团，烷基，烯基或杂环基; R 2包含（N，N-二取代的）芳基胺基团; R 3包含环氧基; R 4是H，芳基，烷基，烯基或杂环基; X为第一连接基团; 和（b）电荷产生化合物。环氧基团可以与聚合物内的官能团反应，直接或通过交联剂形成聚合电荷输送化合物。还描述了相应的电子照相设备和成像方法。

7. 发明授权

US07037632B2 Organophotoreceptor with charge transport material with fluorenone azine groups 失效
标题翻译：具有芴酮吖嗪基团的电荷转运材料的有机光感受器
公开(公告)号：US07037632B2
公开(公告)日：2006-05-02
申请号：US10670483
申请日：2003-09-25
申请人： Nusrallah Jubran , Zbigniew Tokarski , Kam W. Law
发明人： Nusrallah Jubran , Zbigniew Tokarski , Kam W. Law
IPC分类号： G03G5/047
CPC分类号： G03G5/0633 , G03G5/0616 , G03G5/0618 , G03G5/062
摘要： Improved organophotoreceptor comprises an electrically conductive substrate and a photoconductive element on the electrically conductive substrate, the photoconductive element comprising: (a) a charge transport material having the formula where the formula is described in the especification; and (b) a charge generating compound.
摘要翻译：改进的有机光感受器包括在导电衬底上的导电衬底和光电导元件，光电导元件包括：（a）具有下式的电荷传输材料，其中在特定说明中描述了该公式; 和（b）电荷产生化合物。

8. 发明授权

US07348112B2 Polymeric charge transport materials having repeating units comprising an aromatic group and a —S— linkage 失效
标题翻译：具有包含芳基和-S-键的重复单元的聚合物电荷传输材料
公开(公告)号：US07348112B2
公开(公告)日：2008-03-25
申请号：US10883453
申请日：2004-07-01
申请人： Nusrallah Jubran , Zbigniew Tokarski , Valentas Gaidelis , Vytautas Getautis , Tadas Malinauskas , Edmundas Montrimas , Kam W. Law
发明人： Nusrallah Jubran , Zbigniew Tokarski , Valentas Gaidelis , Vytautas Getautis , Tadas Malinauskas , Edmundas Montrimas , Kam W. Law
IPC分类号： G03G5/047
CPC分类号： G03G5/076 , C08G61/124 , C08G73/00 , C08G73/02
摘要： Improved organophotoreceptor comprises an electrically conductive substrate and a photoconductive element on the electrically conductive substrate, the photoconductive element comprising: (a) a polymeric charge transport material having the formula where n is a distribution of integers between 1 and 100,000 with an average value of greater than one; Y comprises an aromatic group; X1 and X2, each independently, is a bond or a linking group; Q1 and Q2 are, each independently, O, S, or NR; and R, R1, and R2 comprise, each independently, H, an alkyl group, an alkenyl group, an alkynyl group, an acyl group, a heterocyclic group, or an aromatic group; and (b) a charge generating compound. Corresponding electrophotographic apparatuses, imaging methods, and methods of preparing the polymeric charge transport material are described.
摘要翻译：改进的有机光感受器包括在导电衬底上的导电衬底和光电导元件，光电导元件包括：（a）具有下式的聚合物电荷传输材料，其中n是1和100,000之间的整数分布，平均值较大比一个 Y包括芳族基团; X 1和X 2各自独立地是键或连接基团; Q 1和Q 2各自独立地为O，S或NR; 和R 1，R 1和R 2各自独立地包括H，烷基，烯基，炔基，酰基，杂环基，或芳族基团; 和（b）电荷产生化合物。描述了相应的电子照相设备，成像方法和制备聚合物电荷传输材料的方法。

9. 发明授权

US07094510B2 Organophotoreceptor with a charge transport material having two (9-fluorenylidene)malononitrile groups 有权
标题翻译：具有两个（9-亚芴基）丙二腈基团的电荷传输材料的有机光感受器
公开(公告)号：US07094510B2
公开(公告)日：2006-08-22
申请号：US10748424
申请日：2003-12-30
申请人： Nusrallah Jubran , Zbigniew Tokarski , Kam W. Law , Eric Morrison , Vytautas Getautis , Vygintas Jankauskas
发明人： Nusrallah Jubran , Zbigniew Tokarski , Kam W. Law , Eric Morrison , Vytautas Getautis , Vygintas Jankauskas
IPC分类号： G03G5/06 , C07C255/57
CPC分类号： C07D295/088 , C07C255/41 , C07C317/22 , C07C327/26 , C07C2603/18 , C07D285/125 , G03G5/0612 , G03G5/0618 , G03G5/062
摘要： Improved organophotoreceptor comprises an electrically conductive substrate and a photoconductive element on the electrically conductive substrate, the photoconductive element comprising: (a) a charge transport material having the formula X-Z-X′ where X and X′ are, each independently, a (9-fluorenylidene)malononitrile group, and Z is a linking group; and (b) a charge generating compound. Corresponding electrophotographic apparatuses and imaging methods are described.
摘要翻译：改进的有机光感受器包括在导电衬底上的导电衬底和光电导元件，光电导元件包括：（a）具有下式的电荷传输材料：“in-line-formula description =”In-line Formulas“end =” “XZ-X”<？in-line-formula description =“In-line Formulas”end =“tail”？>其中X和X'各自独立地为（9-亚芴基）丙二腈基，和 Z是连接基团; 和（b）电荷产生化合物。描述相应的电子照相设备和成像方法。

10. 发明授权

US07063928B2 Electrophotographic organophotoreceptors with novel charge transport materials 有权
标题翻译：具有新型电荷传输材料的电子照相有机光感受器
公开(公告)号：US07063928B2
公开(公告)日：2006-06-20
申请号：US10983020
申请日：2004-11-05
申请人： Kam W. Law , Nusrallah Jubran , Zbigniew Tokarski , Alan R. Katritzky , Ritu Jain , Rexiat Maimait
发明人： Kam W. Law , Nusrallah Jubran , Zbigniew Tokarski , Alan R. Katritzky , Ritu Jain , Rexiat Maimait
IPC分类号： G03G15/10 , C07D231/18
CPC分类号： C07D231/38 , C07C251/84 , C07C317/34 , C07C2603/18 , C07D207/34 , C07D249/18 , C07D257/06 , C07D333/48 , G03G5/0616 , G03G5/0618 , G03G5/062 , G03G5/0661
摘要： This invention relates to a novel organophotoreceptor that includes: (a) a charge transport material comprising a fluorenone hydrazone having a) least two fluorenone alkylsulfonylphenylhydrazone groups, b) at least two fluorenone pyrrolylhydrazone groups, c) at least two fluorenone benzotriazolylhydrazone groups, d) at least two fluorenone sulfolanylhydrazone groups, e) at least two fluorenone pyrazolylhydrazone groups, f) at least two fluorenone naphthylhydrazone groups, g) at least two fluorenone tetrazolylhydrazone groups, h) at least two fluorenone stilbenylhydrazone groups, or i) at least two fluorenone (9H-fluoren-9-ylidene)benzylhydrazone groups. Some of these fluoreneones may be represented by the formula where n is an integer between 2 and 6, inclusive; R1 is hydrogen, alkyl, or aryl; R2 is alkylsulfonylphenyl or one of its derivatives; X is a linking group having the formula —(CH2)m—, branched or linear. The compounds may form electrostatic imaging systems in combination with (b) a charge generating compound; and (c) an electrically conductive substrate.
摘要翻译：本发明涉及一种新型有机光感受器，其包括：（a）电荷传输材料，其包含芴酮腙，其具有a）至少两个芴酮烷基磺酰基苯基腙基团，b）至少两个芴酮吡咯基腙基团，c）至少两个芴酮苯并三唑基腙基团，d）至少两个芴酮砜基腙基团，e）至少两个芴酮吡唑基腙基团，f）至少两个芴酮萘基腙基团，g）至少两个芴酮四唑腙基团，h）至少两个芴酮茋基腙基团，或i）至少两个芴酮（9H-芴-9-亚基）苄腙基团。这些芴酮中的一些可以由下式表示：其中n是2和6之间的整数，包括端值在内; R 1是氢，烷基或芳基; R 2是烷基磺酰基苯基或其衍生物之一; X是具有下式的连接基团 - （CH 2 CH 2）m - 支链或直链。所述化合物可以与（b）产生电荷的化合物组合形成静电成像系统; 和（c）导电基板。

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