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    • 1. 发明授权
    • Method of curing a fuser member overcoat at low temperatures
    • 在低温下固化定影构件外涂层的方法
    • US07048970B1
    • 2006-05-23
    • US09608818
    • 2000-06-30
    • Jiann H. ChenJoseph A. PavliskoCharles C. AndersonRobert A. Lancaster
    • Jiann H. ChenJoseph A. PavliskoCharles C. AndersonRobert A. Lancaster
    • B05D3/02
    • G03G15/2057C08L83/08C09D127/12C08L2666/14
    • A method of making a fuser member having a support comprising the steps of: A) providing a support; B) coating from an organic solvent onto the support a coating composition comprising a fluorocarbon thermoplastic random copolymer, a curing agent having a bisphenol residue, a particulate filler containing zinc oxide, an aminosiloxane, and antimony-doped tin oxide particles, the fluorocarbon thermoplastic random copolymer having subunits of: —(CH2CF2)x—, —(CF2CF(CF3)y—, and —(CF2CF2)z—, wherein x is from 1 to 50 or 60 to 80 mole percent, y is from 10 to 90 mole percent, z is from 10 to 90 mole percent, x+y+z equals 100 mole percent; and C) curing the coating composition for 5 to 10 hours at a temperature in the range of 25° C. to 275° C.
    • 一种制造具有支撑件的定影器构件的方法,包括以下步骤:A)提供支撑件; B)从有机溶剂涂布到载体上,涂料组合物包含氟碳热塑性无规共聚物,具有双酚残基的固化剂,含氧化锌的颗粒填料,氨基硅氧烷和锑掺杂的氧化锡颗粒,碳氟化合物热塑性随机 具有亚基的共聚物:<?in-line-formula description =“In-line Formulas”end =“lead”? - (CH 2 2 CF 2)x- , - (CF 2 CF 3(CF 3)y - )和 - (CF 2 CF 2)z - ,<?in-line-formula description =“In-line Formulas”end =“tail”?>其中x为1至50或60至80摩尔%,y为10至90摩尔%,z为 10至90摩尔%,x + y + z等于100摩尔%;和C)在25℃至275℃的温度下将涂料组合物固化5至10小时。
    • 8. 发明授权
    • Method of preparing thermoplastic random copolymer composition containing zinc oxide and aminosiloxane
    • 制备含有氧化锌和氨基硅氧烷的热塑性无规共聚物组合物的方法
    • US06444741B1
    • 2002-09-03
    • US09607731
    • 2000-06-30
    • Jiann H. ChenJoseph A. PavliskoCharles C. AndersonMuhammed Aslam
    • Jiann H. ChenJoseph A. PavliskoCharles C. AndersonMuhammed Aslam
    • C08J328
    • C08L27/12C08L83/08C08L2666/14
    • A method of preparing a composition containing a fluorocarbon thermoplastic random copolymer comprising the steps of: (a) providing a mixture having: (i) a fluorocarbon thermoplastic random copolymer having subunits of: —(CH2CF2)x—, —(CF2CF(CF3)y—, and —(CF2CF2)z—,  wherein x is from 1 to 50 or 60 to 80 mole percent, y is from 10 to 90 mole percent. z is from 10 to 90 mole percent. x+y+z equals 100 mole percent; (ii) a filler comprising zinc oxide; (iii) a curable amino functional polydimethyl siloxaie copolymer comprising aminofunctional units selected from tile group consisting of (aminoethylaminopropyl) methyl, ( aminopropyl) methyl and (aminopropyl) dimethyl; and (iv) a bisphenol residue curing agent; and (b) curing the mixture for 3 to 10 hours at a temperature in the range of 220° C. to 280° C. and for an additional 2 to 10 hours at a temperature in the range of 250° C. to 270° C.
    • 一种制备含有氟碳热塑性无规共聚物的组合物的方法,包括以下步骤:(a)提供具有以下物质的混合物:(i)具有亚基的氟碳热塑性无规共聚物,其中x为1至50或60至80摩尔% y为10至90摩尔%,z为10至90摩尔%,x + y + z为100摩尔%;(ii)包含氧化锌的填料;(iii)可固化的氨基官能的聚二甲基硅氧烷共聚物,其包含氨基官能单元 选自由(氨基乙基氨基丙基)甲基,(氨基丙基)甲基和(氨基丙基)二甲基组成的瓦片组; 和(iv)双酚残基固化剂; 和(b)在220℃至280℃的温度下将混合物固化3至10小时,并在250℃至270℃的温度下再固化2至10小时 C。