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1. 发明授权

US07341980B2 Viscoelastic surfactant rheology modification 有权
标题翻译：粘弹性表面活性剂流变改性
公开(公告)号：US07341980B2
公开(公告)日：2008-03-11
申请号：US10994664
申请日：2004-11-22
申请人： Jesse Lee , Yiyan Chen , Timothy Pope , Eric Hanson , Samuel Cozzens , Taner Batmaz
发明人： Jesse Lee , Yiyan Chen , Timothy Pope , Eric Hanson , Samuel Cozzens , Taner Batmaz
IPC分类号： C09K8/584 , C09K8/588 , E21B21/00
CPC分类号： C09K8/68 , C09K8/602 , C09K2208/30
摘要： A method for shortening the shear recovery time of zwitterionic viscoelastic surfactant fluids by adding a rheology enhancer having the structure: R-(EO)x(PO)y—R′—OH in which R is an alkyl group that is straight chained or branched, saturated or unsaturated, and contains from 3 to about 18 carbon atoms, x is from 0 to about 14, y is from 0 to about 7, R′ is an alkyl group that contains from 0 to about 14 carbon atoms and is straight chained, branched if having more than 3 carbon atoms, saturated, unsaturated if having more than one carbon atom, the total number of carbon atoms in R plus R′ is from 3 to about 21, and the EO and PO groups, if present, may be in any order. The rheology enhancer also increases fluid viscosity and thermal stability. Preferred surfactants are betaines. The fluids are useful in oilfield treatments, for example fracturing and gravel packing.
摘要翻译：通过添加具有以下结构的流变增强剂来缩短两性离子粘弹性表面活性剂流体的剪切恢复时间的方法：<？in-line-formula description =“In-line Formulas”end =“lead”→> R-（EO）（PO）y-R'-OH <βin-line-formula description =“In-line Formulas”end =“tail”？>其中R是直链或支链，饱和或不饱和的烷基，含有3至约18个碳原子，x为0至约14，y为0至约7，R'为含0至约14个碳原子，如果具有多于3个碳原子，则是直链，支链的，如果具有多于一个碳原子是饱和的，不饱和的，R + R'中的总碳原子数为3至约21，EO 和PO组（如果存在）可以是任何顺序。流变增强剂还增加流体粘度和热稳定性。优选的表面活性剂是甜菜碱。这些流体可用于油田处理，例如压裂和砾石填充。

2. 发明申请

US20060111248A1 Viscoelastic surfactant rheology modification 有权
标题翻译：粘弹性表面活性剂流变改性
公开(公告)号：US20060111248A1
公开(公告)日：2006-05-25
申请号：US10994664
申请日：2004-11-22
申请人： Jesse Lee , Yiyan Chen , Timothy Pope , Eric Hanson , Samuel Cozzens , Taner Batmaz
发明人： Jesse Lee , Yiyan Chen , Timothy Pope , Eric Hanson , Samuel Cozzens , Taner Batmaz
IPC分类号： C09K8/584 , C09K3/00
CPC分类号： C09K8/68 , C09K8/602 , C09K2208/30
摘要： A method for shortening the shear recovery time of zwitterionic viscoelastic surfactant fluids by adding a rheology enhancer having the structure: R-(EO)x(PO)y—R′—OH in which R is an alkyl group that is straight chained or branched, saturated or unsaturated, and contains from 3 to about 18 carbon atoms, x is from 0 to about 14, y is from 0 to about 7, R′ is an alkyl group that contains from 0 to about 14 carbon atoms and is straight chained, branched if having more than 3 carbon atoms, saturated, unsaturated if having more than one carbon atom, the total number of carbon atoms in R plus R′ is from 3 to about 21, and the EO and PO groups, if present, may be in any order. The rheology enhancer also increases fluid viscosity and thermal stability. Preferred surfactants are betaines. The fluids are useful in oilfield treatments, for example fracturing and gravel packing.
摘要翻译：通过添加具有以下结构的流变增强剂来缩短两性离子粘弹性表面活性剂流体的剪切恢复时间的方法：<？in-line-formula description =“In-line Formulas”end =“lead”→> R-（EO）（PO）y-R'-OH <βin-line-formula description =“In-line Formulas”end =“tail”？>其中R是直链或支链，饱和或不饱和的烷基，含有3至约18个碳原子，x为0至约14，y为0至约7，R'为含0至约14个碳原子，如果具有多于3个碳原子，则是直链，支链的，如果具有多于一个碳原子是饱和的，不饱和的，R + R'中的总碳原子数为3至约21，EO 和PO组（如果存在）可以是任何顺序。流变增强剂还增加流体粘度和热稳定性。优选的表面活性剂是甜菜碱。这些流体可用于油田处理，例如压裂和砾石填充。

3. 发明申请

US20050124500A1 Carbon dioxide foamed fluids 有权
标题翻译：二氧化碳发泡流体
公开(公告)号：US20050124500A1
公开(公告)日：2005-06-09
申请号：US10860855
申请日：2004-06-04
申请人： Yiyan Chen , Jesse Lee , Timothy Pope
发明人： Yiyan Chen , Jesse Lee , Timothy Pope
IPC分类号： B01F17/00 , C09K8/38 , C09K8/516 , C09K8/70 , C09K8/74 , E21B43/00
CPC分类号： C09K8/706 , B01F17/0085 , C09K8/516 , C09K8/703 , C09K8/74 , C09K2208/30 , Y10S507/904
摘要： An aqueous viscoelastic surfactant (VES) fluid foamed or energized with carbon dioxide, in which the VES is more compatible with the carbon dioxide, is made by the addition of one or more than one synergistic co-surfactant. The synergist co-surfactant includes quaternary amines and ethoxylated carboxylates having a hydrophobic chain shorter than the hydrophobic chain of the VES. Improved compatibility is evidenced for a given surfactant concentration either by formation and maintenance of a foam under conditions at which the foam could not otherwise have been formed or maintained, or by either higher viscosity of the foamed fluid at a given temperature or longer foam life at a given temperature or a higher temperature at which useful fluid viscosity can be generated or maintained for a useful time. The aqueous carbon dioxide foamed fluids may be used in acidizing, acid fracturing, gravel packing, diversion, and well cleanout.
摘要翻译：通过添加一种或多种协同辅助表面活性剂，可以制备VES与二氧化碳更相容的二氧化碳发泡或赋能的含水粘弹性表面活性剂（VES）流体。增效剂助表面活性剂包括具有比VES的疏水链短的疏水链的季胺和乙氧基化羧酸盐。对于给定的表面活性剂浓度，通过在泡沫不能形成或保持的条件下形成和维持泡沫，或通过在给定温度下较高粘度的发泡流体或更长的泡沫寿命来证明给定的表面活性剂浓度的改进的相容性给定的温度或更高的温度，在该温度下可以产生或维持有用的时间。二氧化碳水溶液发泡流体可用于酸化，酸压裂，砾石填充，分流和清洁。

4. 发明申请

US20080070812A1 Carbon Dioxide Foamed Fluids 有权
标题翻译：二氧化碳发泡液
公开(公告)号：US20080070812A1
公开(公告)日：2008-03-20
申请号：US11858246
申请日：2007-09-20
申请人： Yiyan Chen , Jesse Lee , Timothy Pope
发明人： Yiyan Chen , Jesse Lee , Timothy Pope
IPC分类号： C09K8/68
CPC分类号： C09K8/706 , B01F17/0085 , C09K8/516 , C09K8/703 , C09K8/74 , C09K2208/30 , Y10S507/904
摘要： An aqueous viscoelastic surfactant (VES) fluid foamed or energized with carbon dioxide, in which the VES is more compatible with the carbon dioxide, is made by the addition of one or more than one synergistic co-surfactant. The synergist co-surfactant includes quaternary amines and ethoxylated carboxylates having a hydrophobic chain shorter than the hydrophobic chain of the VES. Improved compatibility is evidenced for a given surfactant concentration either by formation and maintenance of a foam under conditions at which the foam could not otherwise have been formed or maintained, or by either higher viscosity of the foamed fluid at a given temperature or longer foam life at a given temperature or a higher temperature at which useful fluid viscosity can be generated or maintained for a useful time. The aqueous carbon dioxide foamed fluids may be used in acidizing, acid fracturing, gravel packing, diversion, and well cleanout.
摘要翻译：通过添加一种或多种协同辅助表面活性剂，可以制备VES与二氧化碳更相容的二氧化碳发泡或赋能的含水粘弹性表面活性剂（VES）流体。增效剂助表面活性剂包括具有比VES的疏水链短的疏水链的季胺和乙氧基化羧酸盐。对于给定的表面活性剂浓度，通过在泡沫不能形成或保持的条件下形成和维持泡沫，或通过在给定温度下较高粘度的发泡流体或更长的泡沫寿命来证明给定表面活性剂浓度的改善的相容性给定的温度或更高的温度，在该温度下可以产生或维持有用的时间。二氧化碳水溶液发泡流体可用于酸化，酸压裂，砾石填充，分流和清洁。

5. 发明申请

US20060157248A1 Well treatment with dissolvable polymer 有权
标题翻译：用可溶性聚合物处理
公开(公告)号：US20060157248A1
公开(公告)日：2006-07-20
申请号：US11316021
申请日：2005-12-21
申请人： Ann Hoefer , Philip Sullivan , Golchehreh Salamat , Curtis Boney , Jesse Lee , Yiyan Chen , Dean Willberg , Marina Bulova , Christopher Fredd , Belgin Baser , Timothy Pope
发明人： Ann Hoefer , Philip Sullivan , Golchehreh Salamat , Curtis Boney , Jesse Lee , Yiyan Chen , Dean Willberg , Marina Bulova , Christopher Fredd , Belgin Baser , Timothy Pope
IPC分类号： E21B43/25 , C09K8/02
CPC分类号： C09K8/516 , C09K8/12 , C09K8/506 , C09K8/5083 , C09K8/512 , C09K8/52 , C09K8/68 , C09K8/70 , C09K8/80 , C09K2208/08 , C09K2208/26
摘要： Well treatment is disclosed that includes injecting a well treatment fluid with insoluble polyol polymer such as polyvinyl alcohol (PVOH) dispersed therein, depositing the insoluble polymer in the wellbore or an adjacent formation, and thereafter dissolving the polymer by reducing salinity and/or increasing temperature conditions in the environment of the polymer deposit. The method is disclosed for filter cake formation, fluid loss control, drilling, hydraulic fracturing and fiber assisted transport, where removal of the polyol at the end of treatment or after treatment is desired. The method is also disclosed for providing dissolved polyol as a delayed breaker in crosslinked polymer viscosified systems and viscoelastic surfactant systems. Also disclosed are well treatment fluids containing insoluble amorphous or at least partially crystalline polyol, and a PVOH fiber composition wherein the fibers are stabilized from dissolution by salinity.
摘要翻译：公开了一种井处理方法，包括用不溶性多元醇聚合物（如分散在其中的聚乙烯醇（PVOH））注入井处理流体，将不溶性聚合物沉积在井筒或邻近地层中，然后通过降低盐度和/或升高温度溶解聚合物聚合物沉积环境条件。公开了用于滤饼形成，流体损失控制，钻井，水力压裂和纤维辅助运输的方法，其中期望在处理结束或处理后去除多元醇。还公开了用于在交联聚合物增粘体系和粘弹性表面活性剂体系中提供溶解的多元醇作为延迟的破乳剂的方法。还公开了含有不溶性无定形或至少部分结晶多元醇的良好处理液，以及其中纤维通过盐度溶解而稳定的PVOH纤维组合物。

6. 发明申请

US20060128597A1 Viscoelastic surfactant rheology modification 有权
标题翻译：粘弹性表面活性剂流变改性
公开(公告)号：US20060128597A1
公开(公告)日：2006-06-15
申请号：US11012446
申请日：2004-12-15
申请人： Yiyan Chen , Jesse Lee , Philip Sullivan , Timothy Pope
发明人： Yiyan Chen , Jesse Lee , Philip Sullivan , Timothy Pope
IPC分类号： C11D1/10
CPC分类号： C09K8/68 , C09K8/602 , C09K2208/30
摘要： A method for shortening the shear recovery time of cationic, zwitterionic, and amphoteric viscoelastic surfactant fluid systems by adding an effective amount of a rheology enhancer selected from partially hydrolyzed polyvinyl ester and partially hydrolyzed polyacrylates. The rheology enhancer also increases fluid viscosity and very low rheology enhancer concentration is needed. Preferred surfactants are betaines and quaternary amines. The fluids are useful in oilfield treatments, for example fracturing and gravel packing.
摘要翻译：通过添加有效量的选自部分水解的聚乙烯酯和部分水解的聚丙烯酸酯的流变增强剂来缩短阳离子，两性离子和两性粘弹性表面活性剂流体体系的剪切恢复时间的方法。流变增强剂还增加了流体粘度，并且需要非常低的流变学增强剂浓度。优选的表面活性剂是甜菜碱和季胺。这些流体可用于油田处理，例如压裂和砾石填充。

7. 发明授权

US08689874B2 Visco-elastic surfactant spacers 失效
标题翻译：粘弹性表面活性剂垫片
公开(公告)号：US08689874B2
公开(公告)日：2014-04-08
申请号：US12808308
申请日：2008-12-23
申请人： Yiyan Chen , Jesse Lee , Bruno Drochon
发明人： Yiyan Chen , Jesse Lee , Bruno Drochon
IPC分类号： E21B43/16 , E21B33/00 , E21B21/00
CPC分类号： C09K8/40 , C09K8/424
摘要： A spacer for use in an oil well cementing operation comprises an aqueous solution of a visco-elastic surfactant. A method of treating a well in a cementing operation comprises pumping the spacer into a well ahead of a cement slurry, thereby minimizing or preventing commingling of drilling fluid and the cement slurry.
摘要翻译：用于油井固井操作的间隔件包括粘弹性表面活性剂的水溶液。在固井操作中处理井的方法包括将间隔件泵送到水泥浆中的井中，从而最小化或防止钻井液和水泥浆料的混合。

8. 发明授权

US07803744B2 Carbon dioxide foamed fluids 有权
标题翻译：二氧化碳发泡流体
公开(公告)号：US07803744B2
公开(公告)日：2010-09-28
申请号：US11858246
申请日：2007-09-20
申请人： Yiyan Chen , Jesse Lee , Timothy L. Pope
发明人： Yiyan Chen , Jesse Lee , Timothy L. Pope
IPC分类号： C09K8/518 , C09K8/60
CPC分类号： C09K8/706 , B01F17/0085 , C09K8/516 , C09K8/703 , C09K8/74 , C09K2208/30 , Y10S507/904
摘要： An aqueous viscoelastic surfactant (VES) fluid foamed or energized with carbon dioxide, in which the VES is more compatible with the carbon dioxide, is made by the addition of one or more than one synergistic co-surfactant. The synergist co-surfactant includes quaternary amines and ethoxylated carboxylates having a hydrophobic chain shorter than the hydrophobic chain of the VES. Improved compatibility is evidenced for a given surfactant concentration either by formation and maintenance of a foam under conditions at which the foam could not otherwise have been formed or maintained, or by either higher viscosity of the foamed fluid at a given temperature or longer foam life at a given temperature or a higher temperature at which useful fluid viscosity can be generated or maintained for a useful time. The aqueous carbon dioxide foamed fluids may be used in acidizing, acid fracturing, gravel packing, diversion, and well cleanout.
摘要翻译：通过添加一种或多种协同辅助表面活性剂，可以制备VES与二氧化碳更相容的二氧化碳发泡或赋能的含水粘弹性表面活性剂（VES）流体。增效剂助表面活性剂包括具有比VES的疏水链短的疏水链的季胺和乙氧基化羧酸盐。对于给定的表面活性剂浓度，通过在泡沫不能形成或保持的条件下形成和维持泡沫，或通过在给定温度下较高粘度的发泡流体或更长的泡沫寿命来证明给定的表面活性剂浓度的改进的相容性给定的温度或更高的温度，在该温度下可以产生或维持有用的时间。二氧化碳水溶液发泡流体可用于酸化，酸压裂，砾石填充，分流和清洁。

9. 发明授权

US07291651B2 Carbon dioxide foamed fluids 有权
标题翻译：二氧化碳发泡流体
公开(公告)号：US07291651B2
公开(公告)日：2007-11-06
申请号：US10860855
申请日：2004-06-04
申请人： Yiyan Chen , Jesse Lee , Timothy L. Pope
发明人： Yiyan Chen , Jesse Lee , Timothy L. Pope
IPC分类号： B01F3/04 , B01F17/36 , C09K8/60 , E21B21/00 , E21B43/22
CPC分类号： C09K8/706 , B01F17/0085 , C09K8/516 , C09K8/703 , C09K8/74 , C09K2208/30 , Y10S507/904
摘要： An aqueous viscoelastic surfactant (VES) fluid foamed or energized with carbon dioxide, in which the VES is more compatible with the carbon dioxide, is made by the addition of one or more than one synergistic co-surfactant. The synergist co-surfactant includes quaternary amines and ethoxylated carboxylates having a hydrophobic chain shorter than the hydrophobic chain of the VES. Improved compatibility is evidenced for a given surfactant concentration either by formation and maintenance of a foam under conditions at which the foam could not otherwise have been formed or maintained, or by either higher viscosity of the foamed fluid at a given temperature or longer foam life at a given temperature or a higher temperature at which useful fluid viscosity can be generated or maintained for a useful time. The aqueous carbon dioxide foamed fluids may be used in acidizing, acid fracturing, gravel packing, diversion, and well cleanout.
摘要翻译：通过添加一种或多种协同辅助表面活性剂，可以制备VES与二氧化碳更相容的二氧化碳发泡或赋能的含水粘弹性表面活性剂（VES）流体。增效剂助表面活性剂包括具有比VES的疏水链短的疏水链的季胺和乙氧基化羧酸盐。对于给定的表面活性剂浓度，通过在泡沫不能形成或保持的条件下形成和维持泡沫，或通过在给定温度下较高粘度的发泡流体或更长的泡沫寿命来证明给定的表面活性剂浓度的改进的相容性给定的温度或更高的温度，在该温度下可以产生或维持有用的时间。二氧化碳水溶液发泡流体可用于酸化，酸压裂，砾石填充，分流和清洁。

10. 发明申请

US20070032386A1 Internal Breaker for Oilfield Treatments 失效
标题翻译：油田治理的内部破碎机
公开(公告)号：US20070032386A1
公开(公告)日：2007-02-08
申请号：US11532553
申请日：2006-09-18
申请人： Carlos Abad , Jesse Lee , Philip Sullivan , Erik Nelson , Yiyan Chen , Belgin Baser , Lijun Lin
发明人： Carlos Abad , Jesse Lee , Philip Sullivan , Erik Nelson , Yiyan Chen , Belgin Baser , Lijun Lin
IPC分类号： C09K8/00 , E21B43/00
CPC分类号： C09K8/68 , C09K8/508 , C09K8/5751 , C09K8/76 , C09K2208/18 , C09K2208/26 , C09K2208/30 , Y10S507/922 , Y10S507/923
摘要： A composition and method for improving the fluid efficiency of many oilfield treatments is given. The composition is a solid additive, in a viscosified fluid, in a size range small enough that it enters formation pores; it optionally bridges there to form an internal filter cake, and then decomposes to provide a breaker for the viscosifying system for the fluid. Examples of suitable additives include waxes, polyesters, polycarbonates, polyacetals, polymelamines, polyvinyl chlorides, and polyvinyl acetates. Degradation of the additive may be accelerated or delayed.
摘要翻译：给出了一种用于提高许多油田处理流体效率的组合物和方法。该组合物是一种固体添加剂，在粘稠流体中，其尺寸范围足够小，使其进入地层孔; 它可选地在那里桥接以形成内部滤饼，然后分解以提供用于流体的增粘系统的断路器。合适的添加剂的实例包括蜡，聚酯，聚碳酸酯，聚缩醛，聚蜜胺，聚氯乙烯和聚乙酸乙烯酯。添加剂的降解可能会加速或延迟。

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