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2. 发明授权

US3954878A Synthesis of bis(2-substituted ethylthiomethyl) ethers 失效
标题翻译：双（2-取代乙硫基甲基）醚的合成
公开(公告)号：US3954878A
公开(公告)日：1976-05-04
申请号：US517133
申请日：1974-10-23
申请人： James P. Cleveland
发明人： James P. Cleveland
IPC分类号： C07C37/055 , C07C317/08 , C07C319/14 , C07C323/12 , C07C149/14
CPC分类号： C07C317/08 , C07C319/14
摘要： Process for preparing bis(2-substituted ethylthiomethyl) ethers which comprises the steps of (1) reacting 2-hydroxyethyl mercaptan, or a 2-lower-alkoxyethyl mercaptan with a bis(aryloxymethyl) ether having the formula(ArOCH.sub.2).sub.2 Owherein Ar is a negatively substituted phenyl group, said reaction being carried out in the presence of an organic solvent and a strong base at a temperature of at least 60.degree. to about 150.degree.C. in an inert atmosphere and (2) extracting said bis(2-substituted ethylthiomethyl) ether. These compounds are useful intermediates in the preparation of bis(vinylsulfonylmethyl) ethers which are effective hardening agents for hardenable materials.
摘要翻译：制备双（2-取代的乙硫基甲基）醚的方法，其包括以下步骤：（1）使2-羟乙基硫醇或2-低级烷氧基乙基硫醇与具有式（ArOCH 2）2 O的双（芳氧基甲基）醚反应，其中Ar为所述反应在有机溶剂和强碱的存在下，在惰性气氛中在至少60℃至约150℃的温度下进行，和（2）提取所述双（2- 取代的乙硫基甲基）醚。这些化合物是制备双（乙烯基磺酰基甲基）醚的有用的中间体，它们是可硬化材料的有效硬化剂。

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