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1. 发明授权

US4085099A Water-insoluble nitrophenylazophenyl compounds containing a terminal --N--(C.sub.2).sub.n --O--CO-- or --CO--O--CH.sub.2 --CH.sub.2 --C.sub.3 F.sub.5 group 失效
标题翻译：含有末端{13 N {13（CH {HD 2 {B）{HD n {b {13 N {13 CO {13 {0或{13 CO {13 O {13 CH {HD 2 { B {13 CH {HD 2 {B {13 C {HD 3 {BF {HD 5 {B {0 group
公开(公告)号：US4085099A
公开(公告)日：1978-04-18
申请号：US457681
申请日：1974-04-03
申请人： Jean Marie Louis Leroy , Jacques Pierre Edmond Pechmeze
发明人： Jean Marie Louis Leroy , Jacques Pierre Edmond Pechmeze
IPC分类号： C09B29/08 , C09B31/043 , C09B31/047 , C09B43/20 , C09B43/30 , C09B29/00 , C09B29/26 , C09B31/04
CPC分类号： C09B31/043 , C09B29/08 , C09B29/0802 , C09B29/0809 , C09B29/0838 , C09B31/047 , C09B43/202 , C09B43/30 , Y10S8/922
摘要： Dyestuffs falling within the formula: ##STR1## in which A represents the residue of a diazotizable amine free from substituents giving rise to an acid dissociation, m is 0 or 1, the benzene nucleus B may be substituted by methyl or methoxy groups, X represents a hydrogen atom or a methyl, methoxy or ethoxy group, Y represents a hydrogen or chlorine atom or a methyl, methoxy or acylamino group, n is 1, 2 or 3, Z represents --O--CO--CH.sub.2 CH.sub.2 C.sub.2 F.sub.5 or --CO--O--CH.sub.2 CH.sub.2 C.sub.2 F.sub.5 or, provided that Y is --NHCO--CH.sub.2 CH.sub.2 C.sub.2 F.sub.5, a hydrogen atom or a hydroxy, cyano, alkoxycarbonyl or acyloxy group, and R represents a substituted or unsubstituted alkyl group of low molecular weight or --(CH.sub.2).sub.n --Z wherein n and Z have the meanings given above; mixture of such dyestuffs; processes for their preparation; process for the coloration of hydrophobic fibres in which the coloring agent is a dyestuff of the formula given above or a mixture thereof; textile materials dyed or printed with a dyestuff of the formula given above or with a mixture thereof and intermediate products of the formula: ##STR2##
摘要翻译：落在式中的染料：其中A表示不含引发酸解离的取代基的重氮化胺的残基，m为0或1，苯核B可被甲基或甲氧基取代 X表示氢原子或甲基，甲氧基或乙氧基，Y表示氢或氯原子或甲基，甲氧基或酰氨基，n为1,2或3，Z表示-O-CO-CH2CH2C2F5或-CO -O-CH 2 CH 2 C 2 F 5，或者Y为-NHCO-CH 2 CH 2 C 2 F 5，氢原子或羟基，氰基，烷氧基羰基或酰氧基，R为取代或未取代的低分子量烷基或 - （CH 2）n Z，其中n Z具有上述含义; 这种染料的混合物; 其准备过程; 疏水性纤维的着色方法，其中着色剂是上述式所示的染料或其混合物; 用上面给出的式子的染料或其混合物染色或印刷的纺织品材料和下式的中间产物：（III）

2. 发明授权

US4010151A Water insoluble mono azo and disazo dyes containing cinnamonitrile group 失效
标题翻译：含有肉桂腈基团的水不溶性单偶氮和双偶氮染料
公开(公告)号：US4010151A
公开(公告)日：1977-03-01
申请号：US459147
申请日：1974-04-08
申请人： Claude Marie Henri Emile Brouard , Jean Marie Louis Leroy , Jean-Pierre Henry Stiot
发明人： Claude Marie Henri Emile Brouard , Jean Marie Louis Leroy , Jean-Pierre Henry Stiot
IPC分类号： C09B29/01 , C09B29/46 , C09B29/50 , C09B31/02 , C09B31/14 , C09B62/82 , C09B29/08 , C09B29/36 , C09B29/38 , C09B33/12
CPC分类号： C09B31/14 , C09B29/0003 , C09B29/3652 , C09B29/366 , C09B31/02 , C09B62/82
摘要： Dyestuffs of the general formula: ##STR1## IN WHICH THE RADICAL --CH=--CN is fixed in the 4- or 5-position, X represents a hydrogen or chlorine atom, the benzene nucleus A is unsubstituted or substituted by at least one chlorine atom or alkyl, alkoxy or acylamino group, m is the number 0 or 1, and B represents the residue of a coupling compound containing no sulphonic or carboxylic acid group.The dyestuffs in which m represents zero may be prepared by diazotizing a base of the formula: ##STR2## and coupling the diazo derivative with a coupling compound BH wherein X and B have the same significance as set out above.The dyestuffs in which m is equal to 1 may be prepared by coupling the diazo derivative of a base of the formula: ##STR3## with an amine of the formula: ##STR4## diazotizing the amino-monoazo dyestuff thus obtained and coupling with a coupling compound BH wherein ##STR5## have the same significance as set out above. The dyestuffs may be used for the coloration of synthetic fibres.3-amino-cinnamonitrile or 3-amino-4-chloro-cinnamonitrile or 4-amino-3-chloro-cinnamonitrile. These may be prepared by Meerwein's reaction between acrylonitrile and a diazonium chloride of m- or p-nitraniline, dehydrohalogenation by means of an alkali and then reduction of the nitro group.
摘要翻译：具有以下通式的染料：其中R = -CN固定在4-或5-位上的，X表示氢或氯原子，苯核A未被取代或被至少一个氯原子或烷基，烷氧基或酰氨基，m为数0或1，B表示不含磺酸基或羧酸基的偶合化合物的残基。

3. 发明授权

US4101543A Benzene-azo-heterocyclic dyestuffs derived from alkyl aminocinnamates or aminocinnamide 失效
标题翻译：衍生自氨基肉桂酸烷基酯或氨基辛酰胺的苯 - 偶氮 - 杂环染料
公开(公告)号：US4101543A
公开(公告)日：1978-07-18
申请号：US441791
申请日：1974-02-12
申请人： Jean-Pierre Henri Stiot , Claude Marie Henri Emile Brouard , Jean Marie Louis Leroy
发明人： Jean-Pierre Henri Stiot , Claude Marie Henri Emile Brouard , Jean Marie Louis Leroy
IPC分类号： C09B29/01 , C09B29/34 , C09B31/00 , C09B31/02 , C09B62/82 , C09B29/36 , C09B29/38 , C09B31/14 , C09B33/02
CPC分类号： C09B31/02 , C09B29/0003 , C09B62/82
摘要： A dyestuff of the formula: ##STR1## IN WHICH --CH.dbd.CH--CO--Y is fixed in the 4 or 5 position, X is hydrogen or chlorine, Y is amino or alkoxy containing 1 to 4 carbon atoms, the p-phenylene nucleus A is unsubstituted or substituted by chlorine, alkyl containing 1 to 4 carbon atoms, alkoxy containing 1 to 4 carbon atoms, formylamino, acetylamino, propanoylamino, benzoylamino or cinnamoylamino, m is 0 or 1, and B represents the radical N-methyl (or ethyl)-4-hydroxy-2-oxo-quinolyl, 2-hydroxy-carbazolyl, 3-hydroxy-dibenzofuranyl, 2-phenylindolyl, N-methyl (or ethyl)-2-hydroxy-3-cyano-4-methyl-6-oxopyridyl, 3,6-dimethyl-4-hydroxy-1-phenyl-(4,5,-b)pyrazolopyridyl or the radical of formula: ##STR2## wherein R.sub.3 is hydrogen, methyl, alkoxycarbonyl, carbonamido or alkyl-substituted carbonamido and R.sub.4 is hydrogen, chlorine, nitro, methyl, cyano or, but only in the 3 or 4 position of the phenyl nucleus, sulphonamido, carbonamido, alkyl-substituted sulphonamido or alkyl-substituted carbonamido, the alkyl and alkoxy groups containing 1 to 4 carbon atoms. Such a dyestuff is used in the coloration of synthetic fibres.
摘要翻译：一种下式的染料：其中-CH = CH-CO-Y的固定在4或5位，X是氢或氯，Y是氨基或含有1至4个碳原子的烷氧基，对亚苯基核A是未取代的或被氯取代，含有1至4个碳原子的烷基，含1至4个碳原子的烷氧基，甲酰氨基，乙酰氨基，丙酰氨基，苯甲酰氨基或肉桂酰氨基，m是0或1，B代表基团N-甲基或乙基）-4-羟基-2-氧代 - 喹啉基，2-羟基 - 咔唑基，3-羟基 - 二苯并呋喃基，2-苯基吲哚基，N-甲基（或乙基）-2-羟基-3-氰基-4-甲基 - 6-氧代吡啶基，3,6-二甲基-4-羟基-1-苯基 - （4,5，-b）吡唑并吡啶基或下式的基团：其中R3是氢，甲基，烷氧基羰基，碳酰氨基或烷基取代的碳酰氨基和R 4是氢，氯，硝基，甲基，氰基或仅在苯基核的3或4位，磺酰氨基，碳酰胺基，烷基取代的磺酰胺基或烷基取代的碳酰氨基，烷基和含有1至4个碳原子的烷氧基。这种染料用于合成纤维的着色。

4. 发明授权

US4008213A Azo dyestuffs containing a cinnamonitrile residue 失效
标题翻译：含有肉桂腈残留物的偶氮染料
公开(公告)号：US4008213A
公开(公告)日：1977-02-15
申请号：US123414
申请日：1971-03-11
申请人： Claude Marie Henri Emile Brouard , Jean Marie Louis Leroy , Jean-Pierre Henri Stiot
发明人： Claude Marie Henri Emile Brouard , Jean Marie Louis Leroy , Jean-Pierre Henri Stiot
IPC分类号： C07C255/34 , C09B23/14 , C09B31/02 , C09B62/82 , D06P1/18 , C09B29/08 , C09B29/10 , C09B29/26 , C09B29/28
CPC分类号： C07C255/00 , C09B31/02 , C09B62/82
摘要： Dyestuffs of the general formula: ##STR1## in which the radical --CH=CH--CN is fixed in the 4- or 5- position, X represents a hydrogen or chlorine atom, the benzene nucleus A is unsubstituted or substituted by at least one chlorine atom or alkyl, alkoxy or acylamino group, m is the number 0 or 1, and B represents the residue of a coupling compound containing no sulphonic or carboxylic acid group.The dyestuffs in which m represents zero may be prepared by diazotizing a base of the formula: ##STR2## and coupling the diazo derivative with a coupling compound BH wherein X and B have the same significance as set out above.The dyestuffs in which m is equal to 1 may be prepared by coupling the diazo derivative of a base of the formula: ##STR3## with an amine of the formula: ##STR4## diazotizing the amino-monoazo dyestuff thus obtained and coupling with a coupling compound BH wherein ##STR5## have the same significance as set out above. The dyestuffs may be used for the coloration of synthetic fibers such as fibers based on cellulose diacetate, cellulose triacetate and, more particularly aromatic polyesters and polyamides.3-amino-cinnamonitrile or 3-amino-4-chloro-cinnamonitrile or 4-amino-3-chloro-cinnamonitrile. These may be prepared by Meerwein's reaction between acrylonitrile and a diazonium chloride of m- or p-nitraniline, dehydrohalogenation by means of an alkali and then reduction of the nitro group.
摘要翻译：其中基团-CH = CH-CN固定在4-或5-位的通式为的染料，X表示氢或氯原子，苯核A未被取代或被至少一个氯原子或烷基，烷氧基或酰氨基，m为数0或1，B表示不含磺酸基或羧酸基的偶合化合物的残基。

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