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1. 发明授权

US09707511B2 Two-stage gas washing method 有权
公开(公告)号：US09707511B2
公开(公告)日：2017-07-18
申请号：US13368975
申请日：2012-02-08
申请人： Jan Wahlström , Juhani Aittamaa , Isto Eilos
发明人： Jan Wahlström , Juhani Aittamaa , Isto Eilos
IPC分类号： C22B3/00 , B01D53/52 , B01D53/14 , C01B17/20 , C01G3/06 , C10K1/10 , C10J3/00 , C10K1/00 , C10K1/08 , C10K1/16
CPC分类号： B01D53/526 , B01D53/1406 , B01D53/1462 , B01D2252/2021 , B01D2257/304 , B01D2257/504 , C01B17/20 , C01G3/06 , C10G2300/1011 , C10G2300/207 , C10G2300/44 , C10J3/00 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/085 , C10K1/108 , C10K1/165 , Y02C10/06 , Y02E20/18 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： The present description is related to the field of hydrocarbon production by gasification of carbonaceous material. It provides a two-stage gas washing method as a part of gas refining. More specifically it discloses a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. It introduces a use of a novel combination of wash approaches for this application. As a specific application, this process is utilized as a part of biomass to liquid (BTL) process.

2. 发明授权

US09272239B2 Two-stage gas washing method applying sulfide precipitation and alkaline absorption 有权
标题翻译：二级气体洗涤法应用硫化物沉淀和碱性吸收
公开(公告)号：US09272239B2
公开(公告)日：2016-03-01
申请号：US13601670
申请日：2012-08-31
申请人： Jan Wahlström , Juhani Aittamaa , Isto Eilos , Kari I. Keskinen , Jukka Koskinen , Marja Tiitta , Heli Vuori
发明人： Jan Wahlström , Juhani Aittamaa , Isto Eilos , Kari I. Keskinen , Jukka Koskinen , Marja Tiitta , Heli Vuori
IPC分类号： B01D47/00 , C01B17/16 , C07C27/00 , B01D53/52 , C10K1/00 , C10K1/08 , C10K1/10 , C10K1/12 , C10K3/00 , C10K3/04 , C10G2/00
CPC分类号： B01D53/526 , B01D2251/404 , B01D2257/304 , B01D2257/504 , C10G2/30 , C10G2300/1011 , C10G2300/1022 , C10G2300/207 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/08 , C10K1/105 , C10K1/106 , C10K1/108 , C10K1/12 , C10K1/122 , C10K3/006 , C10K3/04 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： Disclosed is a method relating to hydrocarbon production by gasification of carbonaceous material, for example, a two-stage gas washing method as a part of gas refining. Disclosed is a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. Disclosed is a use of a combination of two chemical wash approaches. The process can be utilized as a part of biomass to liquid (BTL) process.
摘要翻译：公开了通过碳质材料的气化，例如作为气体精炼的一部分的两级气体洗涤方法涉及碳氢化合物生产的方法。公开了从气化产生的合成气中除去硫化氢和二氧化碳的方法。公开了两种化学洗涤方法的组合的用途。该方法可用作生物量与液体（BTL）过程的一部分。

3. 发明授权

US5637777A Process and apparatus for preparing tertiary alkyl ether 失效
标题翻译：叔烷基醚的制备方法和装置
公开(公告)号：US5637777A
公开(公告)日：1997-06-10
申请号：US302837
申请日：1994-09-16
申请人： Juhani Aittamaa , Isto Eilos , Juha Jakkula , Petri Lindqvist
发明人： Juhani Aittamaa , Isto Eilos , Juha Jakkula , Petri Lindqvist
IPC分类号： B01J31/10 , B01D3/00 , C07B61/00 , C07C41/06 , C07C41/42 , C07C43/04 , C07C43/00
CPC分类号： C07C41/42 , B01D3/009 , C07C41/06 , Y02P20/127 , Y10S203/06 , Y10S203/17 , Y10S203/20
摘要： The invention concerns a process and an apparatus for preparing tertiary ethers. According to the process, C.sub.4 to C.sub.6 isoolefins and possibly heavier olefins contained in the feedstock are reacted with lower aliphatic alcohols, in particular methanol or ethanol, in a catalytic distillation reactor system in order to produce the corresponding ethers. According to the invention, the reaction between the isoolefins and the alcohols is essentially carried out in at least one reactor (5-7) of the kind, which is combined with a distillation column (3) intended for product separation, by conducting at least a part of the liquid flow of the column through the reactor and returning it to a lower tray than the one from which it was taken. At least half of cation exchange resin is placed in the side reactor (5-7). In the process according to the invention, the catalyst can be rapidly changed without stopping the process. In order to improve conversion additional alcohol can be fed to at least one of the side reactors.
摘要翻译： PCT No.PCT / FI93 / 00097 Sec。 371日期1994年9月16日 102（e）日期1994年9月16日PCT 1993年3月18日PCT公布。公开号WO93 / 19031 日期1993年9月30日本发明涉及一种制备叔醚的方法和装置。根据该方法，原料中所含的C4至C6异烯烃和可能较重的烯烃在催化蒸馏反应器系统中与低级脂族醇，特别是甲醇或乙醇反应，以产生相应的醚。根据本发明，异烯烃和醇之间的反应基本上在至少一个与用于产物分离的蒸馏塔（3）组合的反应器（5-7）中进行，至少通过至少柱的液体流的一部分通过反应器并将其返回到比从其取出的塔的下部托盘。将至少一半的阳离子交换树脂置于侧反应器（5-7）中。在根据本发明的方法中，可以快速改变催化剂而不停止该方法。为了改善转化率，另外的醇可以进料至至少一个侧反应器。

4. 发明申请

US20130053456A1 TWO-STAGE GAS WASHING METHOD APPLYING SULFIDE PRECIPITATION AND ALKALINE ABSORPTION 有权
标题翻译：应用硫化物降解和碱吸收的两阶段气体洗涤方法
公开(公告)号：US20130053456A1
公开(公告)日：2013-02-28
申请号：US13601670
申请日：2012-08-31
申请人： Jan WAHLSTRÖM , Juhani Aittamaa , lsto Eilos , Kari l. Keskinen , Jukka Koskinen , Marja Tiitta , Heli Vuori
发明人： Jan WAHLSTRÖM , Juhani Aittamaa , lsto Eilos , Kari l. Keskinen , Jukka Koskinen , Marja Tiitta , Heli Vuori
IPC分类号： C07C7/11 , C07C27/00
CPC分类号： B01D53/526 , B01D2251/404 , B01D2257/304 , B01D2257/504 , C10G2/30 , C10G2300/1011 , C10G2300/1022 , C10G2300/207 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/08 , C10K1/105 , C10K1/106 , C10K1/108 , C10K1/12 , C10K1/122 , C10K3/006 , C10K3/04 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： Disclosed is a method relating to hydrocarbon production by gasification of carbonaceous material, for example, a two-stage gas washing method as a part of gas refining. Disclosed is a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. Disclosed is a use of a combination of two chemical wash approaches. The process can be utilized as a part of biomass to liquid (BTL) process.
摘要翻译：本发明涉及一种通过碳质材料气化生产碳氢化合物的方法，例如作为气体精炼的一部分的两级气体洗涤法。公开了从气化产生的合成气中除去硫化氢和二氧化碳的方法。公开了两种化学洗涤方法的组合的用途。该方法可用作生物量与液体（BTL）过程的一部分。

5. 发明授权

US06559348B1 Process for treating gas flows of polyolefin manufacturing 失效
标题翻译：处理聚烯烃制造气流的方法
公开(公告)号：US06559348B1
公开(公告)日：2003-05-06
申请号：US09623363
申请日：2000-09-25
申请人： Juhani Aittamaa , Harri Järvelin , Timo Nyman
发明人： Juhani Aittamaa , Harri Järvelin , Timo Nyman
IPC分类号： C07C7144
CPC分类号： C08F10/00 , B01D53/229 , C01B3/501 , C08F6/001 , C08F2/01 , C08F2/34
摘要： The invention relates to a process for the treatment of a gas stream obtained from the production of polyolefins and containing unreacted compounds. According to the process, uncondensed compounds are removed from the gas stream and, when so desired, these compounds are directed to further treatment. According to the invention, the uncondensed compounds are separated from the gas stream by membrane separation. Thus the separation of gases is facilitated, since by coupling the membrane system in conjunction with distillation columns the distillation can be carried out at a substantially higher top temperature. By using the membrane system it is possible effectively to remove the lightest gases, which would otherwise accumulate in the process.
摘要翻译：本发明涉及一种处理从生产聚烯烃并含有未反应化合物得到的气流的方法。根据该方法，从气流中除去未冷凝的化合物，当需要时，将这些化合物用于进一步处理。根据本发明，通过膜分离将未冷凝的化合物与气流分离。因此，气体的分离是有利的，因为通过将膜系统与蒸馏塔结合，蒸馏可以在基本上更高的顶部温度下进行。通过使用膜系统，可以有效地去除在过程中积累的最轻的气体。

6. 发明授权

US5908964A Process for preparing alkyl ethers and mixtures thereof 失效
标题翻译：制备烷基醚及其混合物的方法
公开(公告)号：US5908964A
公开(公告)日：1999-06-01
申请号：US803177
申请日：1997-02-19
申请人： Matti Koskinen , Petri Lindqvist , Harri Jarvelin , Juhani Aittamaa
发明人： Matti Koskinen , Petri Lindqvist , Harri Jarvelin , Juhani Aittamaa
IPC分类号： C07C41/06 , C07C41/42 , C07C43/04
CPC分类号： C07C41/42 , C07C41/06
摘要： The invention concerns a process for preparing a tertiary alkyl ether product. The process comprises reacting the isoolefins of an olefinic hydrocarbon feedstock in a reaction zone (1-3) with an alkanol to form a reaction mixture, which is subjected to distillation in a first distillation zone (4). The bottoms product of the first distillation contains the ether(s), whereas the overhead stream contains unreacted alkanol and a mixture of light hydrocarbons. The overhead stream is subjected to a second distillation in a second distillation zone (15). The overhead product of the second distillation mainly contains the lightest hydrocarbons and a small amount of alkanol, and the bottoms product contains an essentially oxygenate-free hydrocarbon stream which can be used as such for alkylation. In order to increase the conversion of the process, a side drawoff is withdrawn from the second distillation zone (15) and recirculated to the reaction zone (1-3).
摘要翻译：本发明涉及一种制备叔烷基醚产物的方法。该方法包括使反应区（1-3）中的烯烃原料的异烯烃与烷醇反应以形成反应混合物，其在第一蒸馏区（4）中进行蒸馏。第一次蒸馏的塔底产物含有醚，而顶部物流含有未反应的链烷醇和轻烃的混合物。塔顶流在第二蒸馏区（15）中进行第二次蒸馏。第二次蒸馏的塔顶产物主要含有最轻的烃和少量的链烷醇，底部产物含有基本上不含氧的烃流，可用于烷基化。为了增加该方法的转化率，从第二蒸馏区（15）取出侧抽出物并再循环至反应区（1-3）。

7. 发明授权

US06660898B1 Process for dimerizing light olefins to produce a fuel component 有权
标题翻译：将轻质烯烃二聚以产生燃料组分的方法
公开(公告)号：US06660898B1
公开(公告)日：2003-12-09
申请号：US09704578
申请日：2000-11-03
申请人： Antti Pyhälahti , Juhani Aittamaa
发明人： Antti Pyhälahti , Juhani Aittamaa
IPC分类号： C07C204
CPC分类号： C07C2/08 , C07C2531/10 , C10G50/00 , C10G2300/1088 , C10G2300/1092 , C10G2400/02 , C10G2400/04 , Y02P20/582 , C07C11/02
摘要： A process for dimerizing light olefinic hydrocarbons in a reaction zone containing a solid acidic catalyst. The process comprises recovering a reaction zone effluent which contains unreacted olefinic hydrocarbons, converting the unreacted olefinic hydrocarbons into an intermediate product in the effluent and separating the intermediate product from the effluent. By decomposing the separated intermediate product the unreacted olefinic hydrocarbons can be recovered and recycled to the reaction zone. By means of the invention, the yield of the product and the lifetime of the catalyst can be improved in a direct dimerization process of light olefins.
摘要翻译：在含有固体酸性催化剂的反应区中使轻烯属烃二聚的方法。该方法包括回收含有未反应的烯烃的反应区流出物，将未反应的烯烃转化成流出物中的中间产物，并将中间产物与流出物分离。通过分解分离的中间产物，可以回收未反应的烯烃并再循环到反应区。通过本发明，可以在轻质烯烃的直接二聚过程中提高产物的产率和催化剂的使用寿命。

8. 发明授权

US5536886A Process for preparing alkyl ethers 失效
标题翻译：制备烷基醚的方法
公开(公告)号：US5536886A
公开(公告)日：1996-07-16
申请号：US305920
申请日：1994-09-16
申请人： Esa Tamminen , Juhani Aittamaa , Juha Jakkula
发明人： Esa Tamminen , Juhani Aittamaa , Juha Jakkula
IPC分类号： B01J31/10 , B01D3/00 , C07B61/00 , C07C41/06 , C07C41/42 , C07C43/04
CPC分类号： B01D3/009 , C07C41/06 , C07C41/42 , Y02P20/127
摘要： The invention relates to a process for preparing tertiary alkyl ethers. According to the process the feedstock containing hydrocarbons is fed to a catalytic distillation reactor system, in which the isoolefines, in particular the C.sub.4 to C.sub.7 isoolefines, of the feed are reacted with an alkanol in the presence of a cation exchange resin in order to produce tertiary alkyl ether products. The reaction product containing the ethers is removed from the distillation system as the bottoms product and, if necessary, it is subjected to an additional treatment for producing a gasoline component. The unreacted alkanol is removed as the overhead product of the distillation. According to the invention, the distillate withdrawn mainly contains an azeotrope of C.sub.4 hydrocarbons and alkanol, the C.sub.4 amount of which at least approximately corresponds to the C.sub.4 hydrocarbon concentration of the hydrocarbon feed, a substantial amount of the unreacted alkanol being removed in the form of said azeotrope. By means of the invention the need for a separate alkanol washing unit is eliminated in the apparatus which considerably reduces apparatus investment costs.
摘要翻译：本发明涉及一种制备叔烷基醚的方法。根据该方法，将含有烃的原料进料到催化蒸馏反应器系统中，其中进料的异烯烃，特别是C4至C7异烯烃在阳离子交换树脂的存在下与烷醇反应，以产生叔烷基醚产物。含有醚的反应产物作为塔底产物从蒸馏系统中除去，如果需要，将其进行额外处理以生产汽油组分。将未反应的链烷醇作为蒸馏塔顶产物除去。根据本发明，取出的馏出物主要含有C 4烃和链烷醇的共沸物，其C4量至少近似对应于烃进料的C 4烃浓度，大量未反应的链烷醇以说共沸物。通过本发明，在装置中消除了对单独的烷醇洗涤单元的需求，这大大降低了设备的投资成本。

9. 发明授权

US06613108B1 Process for producing a fuel component 有权
标题翻译：燃料成分的制造方法
公开(公告)号：US06613108B1
公开(公告)日：2003-09-02
申请号：US09343559
申请日：1999-06-30
申请人： Juhani Aittamaa , Juha Jakkula , Petri Lindqvist , Matti Koskinen , Juha Linnekoski , Outi Krause , Mauri Sourander , Jyrki Ignatius , Antti Pyhälahti
发明人： Juhani Aittamaa , Juha Jakkula , Petri Lindqvist , Matti Koskinen , Juha Linnekoski , Outi Krause , Mauri Sourander , Jyrki Ignatius , Antti Pyhälahti
IPC分类号： C10L118
CPC分类号： C10G50/00 , C07C2/08 , C07C9/21 , C07C11/02 , C10L1/023 , C10L1/06
摘要： The invention relates to process for dimerizing olefinic hydrocarbon feedstock, to hydrocarbon compositions and to fuel components produced by the process. According to the invention, fresh olefinic hydrocarbon feedstock is fed to a reaction zone of a system including at least one reaction zone and at least one distillation zone. The olefinic hydrocarbon feedstock is contacted with an acidic catalyst in the presence of an oxygenate at conditions in which at least a part of the olefins dimerizes. The effluent from the reaction zone is conducted to the distillation zone where dimerized reaction product is separated from effluent, and at least one flow comprising oxygenate is withdrawn from the side of at least one distillation column. The flow is circulated from distillation zone back to dimerization. The reaction mixture is recovered and optionally hydrogenated to form a parafinic reaction product.
摘要翻译：本发明涉及二烯烃烯烃原料，烃类组合物和通过该方法生产的燃料组分的方法。根据本发明，将新鲜的烯烃原料进料至包含至少一个反应区和至少一个蒸馏区的体系的反应区。在至少部分烯烃二聚的条件下，烯烃原料在含氧化合物的存在下与酸性催化剂接触。将来自反应区的流出物进入蒸馏区，其中二聚反应产物与流出物分离，并且至少一个包含含氧化合物的流从至少一个蒸馏塔的一侧排出。流量从蒸馏区循环回二聚。将反应混合物回收并任选地氢化以形成路旁反应产物。

10. 发明授权

US06458900B1 Process for preparing polyolefins 失效
标题翻译：聚烯烃的制备方法
公开(公告)号：US06458900B1
公开(公告)日：2002-10-01
申请号：US09623369
申请日：2000-09-01
申请人： Juhani Aittamaa , Harri Järvelin , Timo Nyman
发明人： Juhani Aittamaa , Harri Järvelin , Timo Nyman
IPC分类号： C08F234
CPC分类号： C08F10/00 , B01D53/225 , B01J19/2475 , B01J2219/00006 , C01B3/501 , C01B2203/0405 , C01B2203/048 , C08F210/16 , Y10S526/901 , C08F2/01 , C08F2/34 , C08F210/14
摘要： The invention relates to a process for the production of polyolefins in a reactor system which comprises at least one gas-phase reactor with at least one monomer is polymerized. According to the process, there is fed into the gas-phase reactor the monomer to be polymerized and possibly a polymer-containing fluid. According to the invention, before being fed into the gas-phase reactor, the fluid is subjected to a phase change in order to separate uncondensed compounds from liquid and possibly solid compounds. The gas including the uncondensed compound is recovered, and hydrogen is separated from the gas by membrane separation. The invention can be applied to the removal of hydrogen from the circulation gas of a gas-phase reactor, for example in order to change the polyolefin grade to be produced.
摘要翻译：本发明涉及在反应器系统中生产聚烯烃的方法，该方法包括至少一个气相反应器与至少一种单体聚合。根据该方法，向气相反应器中加入要聚合的单体和可能含有聚合物的流体。根据本发明，在进料到气相反应器之前，使流体进行相变，以将未冷凝的化合物与液体和可能的固体化合物分离。回收包含未冷凝化合物的气体，通过膜分离将氢气与气体分离。本发明可以应用于从气相反应器的循环气体中除去氢，例如为了改变要生产的聚烯烃等级。

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