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1. 发明授权

US5942651A Process for converting C.sub.9 + aromatic hydrocarbons to lighter aromatic products by transalkylation in the prescence of two zeolite-containing catalysts 失效
标题翻译：在两种含沸石的催化剂的情况下，通过烷基转移将C9 +芳族烃转化成较轻的芳香族产物的方法
公开(公告)号：US5942651A
公开(公告)日：1999-08-24
申请号：US874875
申请日：1997-06-13
申请人： James H. Beech, Jr. , Stuart Damon Hellring , Terry Eugene Helton , Timothy Frederick Kinn , Sadi Mizrahi , Norman J. Rouleau
发明人： James H. Beech, Jr. , Stuart Damon Hellring , Terry Eugene Helton , Timothy Frederick Kinn , Sadi Mizrahi , Norman J. Rouleau
IPC分类号： C07C4/18 , C07B61/00 , C07C6/12 , C07C15/02 , C07C15/04 , C10G11/05 , C07C5/22
CPC分类号： C07C6/126 , C07C2529/06 , C07C2529/70 , Y02P20/52
摘要： A process for converting a heavy aromatics feed to lighter aromatic products, such as benzene and xylene, by reacting C.sub.9+ aromatic hydrocarbons and toluene or benzene under transalkylation reaction conditions, over a first catalyst composition including a zeolite having a constraint index ranging from 0.5 to 3 and a hydrogenation component and a second catalyst composition including an intermediate pore size zeolite having a constraint index ranging from 3 to 12 and a silica to alumina ratio of at least about 5, to produce a transalkylation reaction product containing benzene or toluene and xylene. The benzene or toluene from the reaction product can then be distilled to obtain a benzene or toluene product.
摘要翻译：通过在烷基转移反应条件下使C9 +芳族烃和甲苯或苯反应，在包含约0.5到3的约束指数的沸石的第一种催化剂组合物上，将重质芳族化合物进料转化成较轻的芳香族产物如苯和二甲苯的方法以及氢化组分和第二催化剂组合物，其包含约3至12的约束指数和至少约5的二氧化硅与氧化铝的中等孔径的沸石，以产生含有苯或甲苯和二甲苯的烷基转移反应产物。然后可以将来自反应产物的苯或甲苯蒸馏得到苯或甲苯产物。

2. 发明申请

US20100285949A1 Process for Rejuvenating a Catalyst Composition 有权
标题翻译：催化剂组合物再生方法
公开(公告)号：US20100285949A1
公开(公告)日：2010-11-11
申请号：US12738061
申请日：2008-10-07
申请人： Terry Eugene Helton , Vijav Nanda , Wei-Ping Tai , Teresa Ann Jurgens-Kowal , Kathleen Marie Keville
发明人： Terry Eugene Helton , Vijav Nanda , Wei-Ping Tai , Teresa Ann Jurgens-Kowal , Kathleen Marie Keville
IPC分类号： B01J38/10 , B01J38/04
CPC分类号： B01J38/02 , B01J29/041 , B01J29/08 , B01J29/18 , B01J29/7007 , B01J29/90 , B01J38/04
摘要： This disclosure relates to a method for rejuvenating a catalyst, comprising contacting the catalyst with a gaseous feedstock at rejuvenation conditions for at least one hour to form a rejuvenated catalyst and a gaseous product, wherein the catalyst comprises at least 10 wt. % of a molecular sieve, wherein the catalyst prior to the contacting step comprises from 0.001 wt. % to 45 wt. % of hydrocarbons and 0.001 to 10 wt. % nitrogen containing components based on the total weight of the catalyst prior to the contacting step, wherein the molecular sieve comprises at least one of a MCM-22 family molecular sieve, a molecular sieve having a framework type of *BEA, a molecular sieve having a framework type of FAU, and a molecular sieve having a framework type of MOR, wherein the gaseous feedstock comprises at least one of N2, H2, alkane, He, Ar, CO, and CO2, wherein the gaseous product has at least a portion of the gaseous feedstock and at least a portion of the hydrocarbons of the catalyst and at least a portion of the nitrogen containing components of the catalyst, wherein the rejuvenation conditions comprise a temperature in the range from about 400 to 600° C., a pressure in the range from about 101.3 kPa-a to 10130 kPa-a, a space hourly velocity in the range of from 0.05 to 10 hr−1.
摘要翻译：本公开涉及一种用于使催化剂再生的方法，包括在再生条件下将催化剂与气态原料接触至少1小时，以形成复原的催化剂和气态产物，其中催化剂包含至少10wt。％的分子筛，其中在接触步骤之前的催化剂包含0.001重量％％至45重量％％的烃和0.001至10wt。％的含氮组分基于在接触步骤之前的催化剂的总重量，其中分子筛包括MCM-22族分子筛，具有骨架类型为* BEA的分子筛中的至少一种，分子筛具有骨架类型的FAU和具有骨架类型MOR的分子筛，其中气态原料包括N 2，H 2，烷烃，He，Ar，CO和CO 2中的至少一种，其中气态产物具有至少一部分的气态原料和催化剂的烃的至少一部分和催化剂的至少一部分含氮组分，其中再生条件包括约400-600℃的温度，压力在约101.3kPa-a至10130kPa-a的范围内，空间时速在0.05至10小时-1的范围内。

3. 发明授权

US07241930B2 Transalkylation of aromatic fluids 有权
标题翻译：芳烃流体的烷基转移
公开(公告)号：US07241930B2
公开(公告)日：2007-07-10
申请号：US10414658
申请日：2003-04-16
申请人： Richard Henry Schlosberg , Edmund John Mozeleski , Francisco M. Benitez , Steven M. Silverberg , Terry Eugene Helton
发明人： Richard Henry Schlosberg , Edmund John Mozeleski , Francisco M. Benitez , Steven M. Silverberg , Terry Eugene Helton
IPC分类号： C07C5/22
CPC分类号： C07C6/126 , C07C7/14883 , C10G2400/30 , C07C15/02
摘要： A process for making an ethylated polycyclic aromatic compound in a mixed aromatic fluid, the process comprising contacting the mixed aromatic fluid containing a polycyclic aromatic compound and a monocyclic aromatic compound having an ethyl substituent in the presence of an acid catalyst under conditions sufficient to effect transalkylation to form the ethylated polycyclic compound and a de-ethylated monocyclic aromatic compound and removal of the de-ethylated monocyclic aromatic compound. A process for decreasing naphthalene concentration in a naphthalene-containing aromatic fluid by acid catalyzed transalkylation of an alkylbenzene and naphthalene to form benzene and an alkylnaphthalene.
摘要翻译：一种在混合芳族流体中制备乙基化多环芳族化合物的方法，该方法包括在酸催化剂存在下，在足以实现烷基转移的条件下使含有多环芳族化合物的混合芳族流体和具有乙基取代基的单环芳族化合物形成乙基化多环化合物和脱乙基化单环芳香族化合物，除去脱乙基单环芳香族化合物。通过烷基苯和萘的酸催化烷基转移来降低含萘芳族流体中萘浓度以形成苯和烷基萘的方法。

4. 发明授权

US07396969B2 Process for preparing short chain alkyl aromatic compounds 失效
标题翻译：制备短链烷基芳族化合物的方法
公开(公告)号：US07396969B2
公开(公告)日：2008-07-08
申请号：US11104858
申请日：2005-04-14
申请人： Jane Chi-Ya Cheng , Terry Eugene Helton , Dominick Nicholas Mazzone , Dennis E. Walsh
发明人： Jane Chi-Ya Cheng , Terry Eugene Helton , Dominick Nicholas Mazzone , Dennis E. Walsh
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C15/073
摘要： A process for producing alkyl aromatic compounds which comprises contacting at least one aromatic compound with at least one alkylating agent or transalkylating agent possessing at least one aliphatic group having from 1 to 5 carbon atoms under alkylation or transalkylation reaction conditions and in the presence of an alkylation or transalkylation catalyst, to provide an alkylated aromatic product possessing at least one alkyl group derived from said alkylating agent or transalkylating agent, said catalyst comprising a binder-free molecular sieve having an X-ray diffraction pattern that includes the lines set forth in Table A.
摘要翻译：一种制备烷基芳族化合物的方法，其包括在烷基化或烷基转移反应条件下和在烷基化存在下使至少一种芳族化合物与至少一种具有至少一个具有1-5个碳原子的脂肪族基团的烷基化剂或烷基转移剂接触或烷基转移催化剂，以提供具有至少一种衍生自所述烷基化剂或烷基转移剂的烷基的烷基化芳族产物，所述催化剂包含具有X射线衍射图的无粘合剂分子筛，其包括表A所示的线。

5. 发明授权

US09545622B2 Activation and use of hydroalkylation catalysts 有权
标题翻译：加氢烷基化催化剂的活化和使用
公开(公告)号：US09545622B2
公开(公告)日：2017-01-17
申请号：US13821957
申请日：2011-09-20
申请人： Teng Xu , Edward Andrew Lemon, Jr. , Terry Eugene Helton , Tan-Jen Chen , Charles Morris Smith
发明人： Teng Xu , Edward Andrew Lemon, Jr. , Terry Eugene Helton , Tan-Jen Chen , Charles Morris Smith
IPC分类号： B01J29/06 , B01J29/74 , B01J29/068 , B01J29/76 , B01J29/072 , B01J29/064 , B01J29/70 , B01J29/72 , B01J37/18 , C07C2/74 , B01J37/08
CPC分类号： B01J29/7476 , B01J29/061 , B01J29/064 , B01J29/068 , B01J29/072 , B01J29/7088 , B01J29/7276 , B01J29/7676 , B01J37/088 , B01J37/18 , B01J2229/20 , B01J2229/40 , B01J2229/42 , C07C2/74 , C07C2529/70 , C07C2529/74 , C07C2529/76 , C07C2601/14 , Y02P20/52 , C07C13/28
摘要： A hydroalkylation catalyst comprising a molecular sieve and a compound of a hydrogenation metal is activated by treating the catalyst at a temperature of less than about 250° C. in the presence of hydrogen.
摘要翻译：包含分子筛和氢化金属化合物的加氢烷基化催化剂通过在氢气存在下在小于约250℃的温度下处理催化剂来活化。

6. 发明授权

US08704025B2 Molecular sieve composition EMM-12, a method of making and a process of using the same 有权
标题翻译：分子筛组合物EMM-12，其制备方法和使用方法
公开(公告)号：US08704025B2
公开(公告)日：2014-04-22
申请号：US12999585
申请日：2009-07-15
申请人： Wieslaw J. Roth , Douglas L. Dorset , Gordon J. Kennedy , Thomas Yorke , Terry Eugene Helton
发明人： Wieslaw J. Roth , Douglas L. Dorset , Gordon J. Kennedy , Thomas Yorke , Terry Eugene Helton
IPC分类号： C07C2/68
CPC分类号： B01J29/70 , B01J29/7038 , B01J2229/42 , C01B39/46 , C01B39/48 , C07C2/66 , C07C6/123 , C07C6/126 , C07C29/36 , C07C37/11 , C07C37/20 , C07C41/06 , C07C45/53 , C07C51/235 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/12 , C07C2521/14 , C07C2523/02 , C07C2529/70 , Y02P20/52 , C07C15/085 , C07C15/107 , C07C33/20 , C07C39/06 , C07C39/16 , C07C43/04 , C07C49/10 , C07C57/30
摘要： This disclosure relates to an EMM-12 molecular sieve having, in its as-synthesized form and in calcined form, an X-ray diffraction pattern including peaks having a d-spacing maximum in the range of 14.17 to 12.57 Angstroms, a d-spacing maximum in the range of 12.1 to 12.56 Angstroms, and non-discrete scattering between about 8.85 to 11.05 Angstroms or exhibit a valley in between the peaks having a d-spacing maximum in the range of 10.14 to 12.0 Angstroms and a d-spacing maximum in the range from 8.66 to 10.13 Angstroms with measured intensity corrected for background at the lowest point being not less than 50% of the point at the same XRD d-spacing on the line connecting maxima in the range of 10.14 to 12.0 Angstroms and in the range from 8.66 to 10.13 Angstroms.
摘要翻译：本公开涉及一种EMM-12分子筛，其以其合成形式和煅烧形式具有X射线衍射图，其包括d-间距最大值在14.17至12.57埃范围内的峰，d-间距在12.1至12.56埃的范围内的最大值，以及在约8.85至11.05埃之间的非离散散射，或在具有10.14至12.0埃范围内的d间距最大值的峰之间呈现出谷值，在最低点处校正背景的测量强度的8.66至10.13埃的范围不小于连接最大值在10.14至12.0埃范围内的线上的相同XRD d间距处的点的50％从8.66到10.13埃。

7. 发明授权

US08623777B2 Process for rejuvenating a catalyst composition 有权
标题翻译：催化剂组合物再生方法
公开(公告)号：US08623777B2
公开(公告)日：2014-01-07
申请号：US12738061
申请日：2008-10-07
申请人： Terry Eugene Helton , Vijay Nanda , Wei-Ping Tai , Teresa Ann Jurgens-Kowal , Kathleen Marie Keville
发明人： Terry Eugene Helton , Vijay Nanda , Wei-Ping Tai , Teresa Ann Jurgens-Kowal , Kathleen Marie Keville
IPC分类号： B01J38/04 , B01J38/10 , B01J38/06 , B01J38/02
CPC分类号： B01J38/02 , B01J29/041 , B01J29/08 , B01J29/18 , B01J29/7007 , B01J29/90 , B01J38/04
摘要： This disclosure relates to a method for rejuvenating a catalyst, comprising contacting the catalyst with a gaseous feedstock at rejuvenation conditions for at least one hour to form a rejuvenated catalyst and a gaseous product, wherein the catalyst comprises at least 10 wt. % of a molecular sieve, wherein the catalyst prior to the contacting step comprises from 0.001 wt. % to 45 wt. % of hydrocarbons and 0.001 to 10 wt. % nitrogen containing components based on the total weight of the catalyst prior to the contacting step, wherein the molecular sieve comprises at least one of a MCM-22 family molecular sieve, a molecular sieve having a framework type of *BEA, a molecular sieve having a framework type of FAU, and a molecular sieve having a framework type of MOR, wherein the gaseous feedstock comprises at least one of N2, H2, alkane, He, Ar, CO, and CO2, wherein the gaseous product has at least a portion of the gaseous feedstock and at least a portion of the hydrocarbons of the catalyst and at least a portion of the nitrogen containing components of the catalyst, wherein the rejuvenation conditions comprise a temperature in the range from about 400 to 600° C., a pressure in the range from about 101.3 kPa-a to 10130 kPa-a, a space hourly velocity in the range of from 0.05 to 10 hr−1.
摘要翻译：本公开涉及一种用于使催化剂再生的方法，包括在再生条件下将催化剂与气态原料接触至少1小时，以形成复原的催化剂和气态产物，其中催化剂包含至少10wt。％的分子筛，其中在接触步骤之前的催化剂包含0.001重量％％至45重量％％的烃和0.001至10wt。％的含氮组分基于在接触步骤之前的催化剂的总重量，其中分子筛包括MCM-22族分子筛，具有骨架类型为* BEA的分子筛中的至少一种，分子筛具有骨架类型的FAU和具有骨架类型MOR的分子筛，其中气态原料包括N 2，H 2，烷烃，He，Ar，CO和CO 2中的至少一种，其中气态产物具有至少一部分的气态原料和催化剂的烃的至少一部分和催化剂的至少一部分含氮组分，其中再生条件包括约400-600℃的温度，压力在约101.3kPa-a至10130kPa-a的范围内，空间时速在0.05至10小时-1的范围内。

8. 发明申请

US20130289323A1 Activation and Use of Hydroalkylation Catalysts 有权
标题翻译：氢化烷基化催化剂的活化和使用
公开(公告)号：US20130289323A1
公开(公告)日：2013-10-31
申请号：US13821957
申请日：2011-09-20
申请人： Teng Xu , Edward Andrew Lemon, JR. , Terry Eugene Helton , Tan-Jen Chen , Charles Morris Smith
发明人： Teng Xu , Edward Andrew Lemon, JR. , Terry Eugene Helton , Tan-Jen Chen , Charles Morris Smith
IPC分类号： B01J29/74
CPC分类号： B01J29/7476 , B01J29/061 , B01J29/064 , B01J29/068 , B01J29/072 , B01J29/7088 , B01J29/7276 , B01J29/7676 , B01J37/088 , B01J37/18 , B01J2229/20 , B01J2229/40 , B01J2229/42 , C07C2/74 , C07C2529/70 , C07C2529/74 , C07C2529/76 , C07C2601/14 , Y02P20/52 , C07C13/28
摘要： A hydroalkylation catalyst comprising a molecular sieve and a compound of a hydrogenation metal is activated by treating the catalyst at a temperature of less than about 250° C. in the presence of hydrogen.
摘要翻译：包含分子筛和氢化金属化合物的加氢烷基化催化剂通过在氢气存在下在小于约250℃的温度下处理催化剂来活化。

9. 发明授权

US09580368B2 Dehydrogenation process 有权
标题翻译：脱氢工艺
公开(公告)号：US09580368B2
公开(公告)日：2017-02-28
申请号：US14006338
申请日：2011-12-02
申请人： Tan-Jen Chen , Jihad Mohammed Dakka , Terry Eugene Helton , Francisco Manuel Benitez , Charles Morris Smith , Lorenzo Cophard DeCaul
发明人： Tan-Jen Chen , Jihad Mohammed Dakka , Terry Eugene Helton , Francisco Manuel Benitez , Charles Morris Smith , Lorenzo Cophard DeCaul
IPC分类号： C07C5/367 , C07C5/32
CPC分类号： C07C5/367 , C07C5/325 , C07C2523/14 , C07C2523/42 , C07C2523/62 , C07C13/20
摘要： Disclosed herein is a process for dehydrogenating a saturated cyclic hydrocarbon and/or 5-membered ring compound with a dehydrogenation catalyst. The dehydrogenation catalyst comprises: (i) 0.05 wt % to 5 wt % of a metal selected from Group 14 of the Periodic Table of Elements; and (ii) 0.1 wt % to 10 wt % of a metal selected from Groups 6 to 10 of the Periodic Table of Elements. The process is conducted under dehydrogenation conditions effective to dehydrogenate at least a portion saturated cyclic hydrocarbon and/or 5-membered ring compound.
摘要翻译：本文公开了一种使用脱氢催化剂使饱和环烃和/或五元环化合物脱氢的方法。脱氢催化剂包括：（i）0.05重量％至5重量％的选自元素周期表第14族的金属; 和（ii）0.1重量％至10重量％的选自元素周期表第6至10族的金属。该方法在有效使至少一部分饱和环烃和/或五元环化合物脱氢的脱氢条件下进行。

10. 发明申请

US20140323782A1 Dehydrogenation Process 有权
标题翻译：脱氢工艺
公开(公告)号：US20140323782A1
公开(公告)日：2014-10-30
申请号：US14006338
申请日：2011-12-02
申请人： Tan-Jen Chen , Jihad Mohammed Dakka , Terry Eugene Helton , Francisco Manuel Benitez , Charles Morris Smith , Lorenzo Cophard DeCaul
发明人： Tan-Jen Chen , Jihad Mohammed Dakka , Terry Eugene Helton , Francisco Manuel Benitez , Charles Morris Smith , Lorenzo Cophard DeCaul
IPC分类号： C07C5/367
CPC分类号： C07C5/367 , C07C5/325 , C07C2523/14 , C07C2523/42 , C07C2523/62 , C07C13/20
摘要： Disclosed herein is a process for dehydrogenating a saturated cyclic hydrocarbon and/or 5-membered ring compound with a dehydrogenation catalyst. The dehydrogenation catalyst comprises: (i) 0.05 wt % to 5 wt % of a metal selected from Group 14 of the Periodic Table of Elements; and (ii) 0.1 wt % to 10 wt % of a metal selected from Groups 6 to 10 of the Periodic Table of Elements. The process is conducted under dehydrogenation conditions effective to dehydrogenate at least a portion saturated cyclic hydrocarbon and/or 5-membered ring compound.
摘要翻译：本文公开了一种使用脱氢催化剂使饱和环烃和/或五元环化合物脱氢的方法。脱氢催化剂包括：（i）0.05重量％至5重量％的选自元素周期表第14族的金属; 和（ii）0.1重量％至10重量％的选自元素周期表第6至10族的金属。该方法在有效使至少一部分饱和环烃和/或五元环化合物脱氢的脱氢条件下进行。

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