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1. 发明授权

US5024775A Alkyl phenol stabilizer compositions for fuels and lubricants 失效
标题翻译：用于燃料和润滑剂的烷基酚稳定剂组合物
公开(公告)号：US5024775A
公开(公告)日：1991-06-18
申请号：US432164
申请日：1989-11-06
申请人： J. Vincent Hanlon , Scott A. Culley
发明人： J. Vincent Hanlon , Scott A. Culley
IPC分类号： C10L1/183 , C09K15/08 , C10L10/08 , C10L10/14 , C10M129/10 , C10N30/10 , C10N40/08
CPC分类号： C10L1/1832 , C09K15/08 , C10M129/10 , C10M2207/023 , C10M2207/026 , C10M2207/027 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/201 , C10N2240/202
摘要： Liquid mixtures of alkyl phenols composed of from 1 to 8 wt % 2-tert-butylphenol; from 4 to 12 wt % of 2,6-di-tert-butylphenol; from 4 to 12 wt % of 2-tri-tert-butylphenol; and from 65 to 80 wt % of 2,6-di-tert-butyl-4-n-butylphenol have a balance of properties rendering them ideally suited for use as stabilizers for middle distillate fuels. Such mixtures can be readily produced by an aldehyde-catalyzed alkylation procedure using n-butanol, an appropriate mixture of tertiary butylated phenols, and a strong base (e.g., NaOH, KOH, etc.).

2. 发明授权

US5076814A Stabilizer compositions 失效
标题翻译：稳定剂组合物
公开(公告)号：US5076814A
公开(公告)日：1991-12-31
申请号：US622648
申请日：1990-12-05
申请人： J. Vincent Hanlon , Scott A. Culley
发明人： J. Vincent Hanlon , Scott A. Culley
IPC分类号： C09K15/08 , C10M129/10
CPC分类号： C09K15/08 , C10L1/1832 , C10M129/10 , C10M2207/023 , C10M2207/026 , C10M2207/027 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/06 , C10N2240/08 , C10N2240/201 , C10N2240/202
摘要： Liquid mixtures of alkyl phenols composed of from 1 to 8 wt % of 2-tert-butylphenol; from 4 to 12 wt % of 2,6-di-tert-butylphenol; from 4 to 12 wt % of 2-tert-butyl-4-n-butylphenol; from 4 to 12 wt % of 2,4,6-tri-tert-butylphenol; and from 65 to 89 wt % of 2,6-di-tert-butyl-4-n-butylphenol having a balance of properties rendering them ideally suited for use as stabilizers for middle distillate fuels. Such mixtures can be readily produced by an aldehyde-catalytzed alkylation procedure using n-butanol, an appropriate mixture of tertiary butylated phenols, and a strong base (e.g., NaOH, KOH, etc.).
摘要翻译：由1至8重量％的2-叔丁基苯酚组成的烷基酚的液体混合物; 4〜12重量％的2,6-二叔丁基苯酚; 4-12重量％的2-叔丁基-4-正丁基苯酚; 4至12重量％的2,4,6-三叔丁基苯酚; 和65至89重量％的具有平衡性能的2,6-二叔丁基-4-正丁基苯酚，使其理想地适合用作中间馏分燃料的稳定剂。这种混合物可以通过使用正丁醇，叔丁基化酚和强碱（例如NaOH，KOH等）的合适混合物的醛催化的烷基化方法容易地制备。

3. 发明授权

US4849544A 1,3-Diaminocyclohexanes 失效
标题翻译： 1,3-二氨基环己烷
公开(公告)号：US4849544A
公开(公告)日：1989-07-18
申请号：US181045
申请日：1988-04-13
申请人： Scott A. Culley , Kestutis A. Keblys , Christopher J. Nalepa
发明人： Scott A. Culley , Kestutis A. Keblys , Christopher J. Nalepa
IPC分类号： C07C211/36
CPC分类号： C07C211/36 , C07C2101/14
摘要： Sterically hindered 1,3-diaminocyclohexanes which can be used in the preparation of polyurethane, polyurea, polyurethaneurea, and epoxy resins are prepared by hydrogenating a metaphenylenediamine having alkyl substituents of 1-6 carbons in the 4- and 6-positions and optionally also in the 2-position, at least one of the alkyl substituents containing at least two carbons, and the total number of carbons in the alkyl substituents being at least five, at a temperature of about 170.degree.-200.degree. C. and a pressure of at least about 6.9 MPa, preferably about 20-30 MPa, in the presence of a supported ruthenium catalyst and an activating amount of a modifier selected from alkali metal hydroxides and alkoxides and alkali metal amide salts of the meta-phenylenediamine to form the corresponding 1,3-diaminocyclohexane.
摘要翻译：可用于制备聚氨酯，聚脲，聚氨酯脲和环氧树脂的可受阻的1,3-二氨基环己烷是通过在4-和6-位上氢化具有1-6个碳烷基取代基的间苯二胺制备的， 2-位，至少一个含有至少两个碳的烷基取代基，烷基取代基中的碳总数至少为五个，温度为约170℃-200℃，压力为在负载的钌催化剂和活化量的选自碱金属氢氧化物和醇盐的改性剂和间苯二胺的碱金属酰胺盐的存在下，至少约6.9MPa，优选约20-30MPa，形成相应的1， 3-二氨基环己烷。

4. 发明授权

US5180510A Antioxidant additive and lubricating oil containing same 失效
标题翻译：含有抗氧化添加剂和润滑油
公开(公告)号：US5180510A
公开(公告)日：1993-01-19
申请号：US175522
申请日：1988-03-31
申请人： Edward F. Zaweski , Scott A. Culley
发明人： Edward F. Zaweski , Scott A. Culley
IPC分类号： C07G99/00 , C10M133/00 , C10M135/18
CPC分类号： C07G17/006 , C10M133/00 , C10M135/18 , C10M2219/00 , C10M2219/022 , C10M2219/066 , C10M2219/068 , C10M2219/082 , C10M2219/083 , C10N2210/01 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106
摘要： An additive for improving the antioxidation properties of lubricating oil is made by reacting a sulfur halide selected from sulfur monochloride or sulfur dichloride with an aliphatic monoolefin (e.g. isobutene) to form an adduct, reacting the adduct thus formed with an alkali metal salt of an organocarbamodithioic acid in an aqueous alkanol medium and recovering the reaction product.When added to lubricating oil, the additive products of the invention improve the antioxidation properties of the lubricating oil.
摘要翻译：用于提高润滑油的抗氧化性能的添加剂是通过使选自一氯化硫或二氯化硫的卤化硫与脂族单烯烃（例如异丁烯）反应形成加合物，使由此形成的加合物与有机羧基二硫代硫酸的碱金属盐反应酸在烷基醇水溶液中并回收反应产物。当添加到润滑油中时，本发明的添加剂产品提高润滑油的抗氧化性能。

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