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1. 发明授权

US4738795A Demulsification of water-in-oil emulsions 失效
标题翻译：油包水乳液的破乳
公开(公告)号：US4738795A
公开(公告)日：1988-04-19
申请号：US781014
申请日：1985-09-27
申请人： J. Redmond Farnand
发明人： J. Redmond Farnand
IPC分类号： B01D17/04 , B01D17/05 , C09K8/60 , C10G33/04
CPC分类号： C09K8/602 , B01D17/047 , C10G33/04
摘要： Crude petroleum water-in-oil emulsions such as those produced by steam injection or water flooding in secondary oil well treatments (and other emulsions of this type) can be very effectively broken by the addition of water-insoluble, polar compounds selected from certain aliphatic carboxylic acids, alcohols, ketones including diketones, acetates, nitropropane, nitrobutane; and alkyl-substituted phenols; in small amounts up to about 8% by weight based on the emulsion. It was found that the number of carbon atoms in the aliphatic compounds and in the phenol's alkyl substituents must be within certain ranges for effective demulsification. The dispersed aqueous droplets, on treatment with the selected compound and appropriate agitation, come together to form an aqueous phase which can be separated. The additives can be recovered from the organic phase and recycled. Certain additive mixtures have been found very effective.
摘要翻译：通过在二次油井处理（和其它类型的其它乳液）中通过蒸汽注入或水驱产生的原油石油油包水乳液可以非常有效地通过加入选自某些脂肪族的水不溶性极性化合物羧酸，醇，酮，包括二酮，乙酸酯，硝基丙烷，硝基丁烷; 和烷基取代的酚; 基于乳液，其量少至多约8重量％。发现脂肪族化合物和苯酚的烷基取代基中的碳原子数必须在有效的破乳的某一范围内。分散的水滴在用所选择的化合物处理和适当的搅拌下合在一起形成可以分离的水相。添加剂可以从有机相回收再循环。已经发现某些添加剂混合物非常有效。

2. 发明授权

US4376133A Agglomeration of proteinaceous solids 失效
标题翻译：蛋白质固体聚集
公开(公告)号：US4376133A
公开(公告)日：1983-03-08
申请号：US246935
申请日：1981-03-24
申请人： J. Redmond Farnand
发明人： J. Redmond Farnand
IPC分类号： A23J3/14 , A23J3/18 , A23J3/00
CPC分类号： A23J3/14 , A23J3/18
摘要： Finely divided proteinaceous solids suspended in a non-polar organic liquid are formed into agglomerates by contacting the suspension with an immiscible polar liquid comprising selected alkanol-water mixtures, agitating the 3-phase system to effect agglomeration, separating the agglomerates and recovering the proteinaceous solids. The proteinaceous solids are usually derived from cereal grains or legume seeds, particularly those on which a milling, fractionation or solvent extraction is carried out in a non-polar organic liquid medium.
摘要翻译：悬浮在非极性有机液体中的细碎的蛋白质固体通过使悬浮液与包含选择的链烷醇 - 水混合物的不混溶的极性液体接触而形成团聚体，搅拌3相体系以实现附聚，分离附聚物并回收蛋白质固体。蛋白质固体通常衍生自谷物或豆类种子，特别是在非极性有机液体培养基中进行研磨，分馏或溶剂萃取的种子。

3. 发明授权

US4888108A Separation of fine solids from petroleum oils and the like 失效
标题翻译：从石油等分离精细固体
公开(公告)号：US4888108A
公开(公告)日：1989-12-19
申请号：US220934
申请日：1988-06-23
申请人： J. Redmond Farnand
发明人： J. Redmond Farnand
IPC分类号： C10G21/00
CPC分类号： C10G21/003
摘要： Dispersed solids, particularly fine peptized hydrophobic solids, present in some petroleum oils, bitumen solutions or concentrates, heavy oils and the like, may be removed by distributing an additive selected from resorcinol, catechol, formic acid, maleic acid or anhydride, chloral hydrate and asphaltene - precipitating solvents (preferably certain mixtures thereof) throughout the dispersion to cause small agglomerates containing the solids to form, and separating the agglomerates from the residual liquid. This residual liquid is rendered more suitable for various refining processes. Agglomerates containing asphaltenes and mineral solids may be used e.g. in hydrogen generation, for compounding roofing materials and in paving materials.
摘要翻译：存在于一些石油，沥青溶液或浓缩物，重油等中的分散固体，特别是细的胶溶疏水固体，可以通过分配选自间苯二酚，邻苯二酚，甲酸，马来酸或酸酐，水合氯醛和沥青质 - 沉淀溶剂（优选其某些混合物）在整个分散体中引起含有固体的小团聚体，并将残留物与剩余液体分离。这种残留液体更适合于各种精炼过程。含有沥青质和矿物质固体的聚集体可以被使用。在氢气生成中，用于复合屋顶材料和铺路材料。

4. 发明授权

US4057486A Separating organic material from tar sands or oil shale 失效
标题翻译：从焦油砂或油页岩中分离出有机物
公开(公告)号：US4057486A
公开(公告)日：1977-11-08
申请号：US595762
申请日：1975-07-14
申请人： F. Weldon Meadus , Bryan D. Sparks , Ira E. Puddington , J. Redmond Farnand
发明人： F. Weldon Meadus , Bryan D. Sparks , Ira E. Puddington , J. Redmond Farnand
IPC分类号： C10G1/04
CPC分类号： C10G1/045
摘要： Tar sands and like mineral solids-plus petroleum deposits are separated into a petroleum fraction and a solids fraction by contacting with an organic solvent or diluent (in one or more stages) to give a liquid slurry, providing in the system a small amount of an aqueous agglomerating liquid, mixing and agitating until discrete compact agglomerates of hydrophilic solids form, separating the solid easily-handled agglomerates and recovering the petroleum fraction and solvent or diluent. This process avoids the large volumes of aqueous effluent inherent in the "hot water" and other processes using large amounts of water. The solid agglomerates may be used as clean fill, sintered to aggregate, or modified to serve as soil amendments.
摘要翻译：沥青砂和矿物固体加上石油沉积物通过与有机溶剂或稀释剂（一个或多个阶段）接触而分离成石油馏分和固体馏分，得到液体浆料，在体系中提供少量的混合和搅拌，直到形成亲水固体的离散紧密聚集体，分离固体容易处理的附聚物并回收石油馏分和溶剂或稀释剂。该方法避免了“热水”中固有的大量含水废水和其他使用大量水的方法。固体附聚物可用作清洁填充物，烧结以聚集或修饰以用作土壤修饰物。

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