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1. 发明授权

US4976943A Spherical, hydrophilic silica, method of its preparation and use 失效
标题翻译：球形，亲水性二氧化硅，其制备方法及用途
公开(公告)号：US4976943A
公开(公告)日：1990-12-11
申请号：US351054
申请日：1989-05-12
申请人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
发明人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
IPC分类号： C01B33/16 , C01B33/12 , C01B33/18 , C08K3/34 , C08K3/36
CPC分类号： C01B33/183 , C01B33/12 , C01P2002/02 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/90
摘要： A spherical, hydrophilic silica consisting of compact, massive, non-crystalline particles without inner pores with a particle size of 0.5 to 10 .mu.m, preferably 0.5 to 4 .mu.m and especially 1 to 3 .mu.m with a BET surface of
摘要翻译：一种球形的亲水性二氧化硅，其由紧凑的，块状的，非结晶的颗粒组成，没有内孔，粒径为0.5至10μm，优选0.5至4μm，特别是1至3μm，BET表面积<50m2 通过将水蒸气和气态四氯化硅分别加热至300-400℃的温度，以2:1至6.7:1的摩尔比彼此混合来制备/ g，优选1至10m 2 / g。并在600-1200℃的温度下使混合物反应。

2. 发明授权

US5061474A Amorphous aluminum oxides, methods of production and uses 失效
标题翻译：非晶铝氧化物，生产方法和用途
公开(公告)号：US5061474A
公开(公告)日：1991-10-29
申请号：US436246
申请日：1989-11-14
申请人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
发明人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
IPC分类号： B01J21/04 , C01F7/02 , C01F7/30 , C09K3/14
CPC分类号： C01F7/302 , B01J21/04 , C01F7/02 , C09K3/1409 , C01P2002/02 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/82
摘要： X-ray amorphous, aluminum oxide which exhibits a specific surface area (BET) according to DIN 66 131 of >10 m.sup.2 /g, an average particle size of .gtoreq.0.1 .mu.m and a water content of >10%. The X-ray amorphous aluminum oxide can be produced by reacting water vapor and vaporous aluminum trichloride in a molar ratio of 1.5 to 10:1, preferably 7.+-.1:1=H.sub.2 O:alCl.sub.3 at a temperature of 200.degree. to 1000.degree. C., preferably 600.degree..+-.50.degree. C. and at a dwell time of >1 sec., preferably 3.5.+-.1 sec. and a partial vacuum of 100.+-.10 mm H.sub.2 O column. By means of calcination thereof an aluminum oxide can be obtained which consists of .gtoreq.90% by weight of .alpha.-aluminum oxide and exhibits a specific surface area (BET) according to DIN 66 131 of >5 m.sup.2 /g and an average particle size of .gtoreq.0.1 .mu.m.
摘要翻译：根据DIN 66 131> 10m 2 / g的比表面积（BET），平均粒径>0.1μm，含水量> 10％的X射线无定形氧化铝。 X射线无定形氧化铝可以通过使水蒸汽和三氯化铝与摩尔比为1.5〜10:1，优选为7 +/- 1：1 = H 2 O:AlCl 3在200〜1000℃的温度下反应来制造。优选600℃±50℃，停留时间> 1秒，优选3.5 +/- 1秒。和100 +/- 10毫米H2O柱的部分真空。通过煅烧，可以获得氧化铝，其由≥/ = 90重量％的α-氧化铝组成，并且根据DIN 66 131> 5m 2 / g表现出比表面积（BET），平均颗粒大小> / = 0.1亩。

3. 发明授权

US4670101A Aqueous suspension of bentonite and its use for coating thermal insulating molded articles 失效
标题翻译：膨润土的水悬浮液及其用于涂覆绝热模制品的用途
公开(公告)号：US4670101A
公开(公告)日：1987-06-02
申请号：US749480
申请日：1985-06-27
申请人： Sabine Schmidt , Peter Kleinschmit , Rudolf Schwarz
发明人： Sabine Schmidt , Peter Kleinschmit , Rudolf Schwarz
IPC分类号： C04B30/02 , D21F11/00
CPC分类号： C04B30/02
摘要： There is prepared an aqueous suspension which in addition to water, consists of 2 to 50 weight % of a mixture of bentonite and inorganic fibers, with the portion of inorganic fiber being 1 to 30 weight % and the portion of bentonite being 1 to 30 weight % and wherein the total amount of solids does not exceed 50 weight %. With the suspension there is attained an improvement of the mechanical properties of thermal insulating molded objects which are employed for thermal insulation and which for example, contain pyrogenically produced silica as a filler by delivery of this suspension on the thermal insulating plate. The suspension can also be delivered on thermal insulating molded bodies on which there is pressed a fiber net or a fiber felt. After applying the suspension several thermal insulating molded bodies can be joined together where the coating formed consisting of bentonite and inorganic fibers acts as binder. The heat insulating molded article in addition to this layer, can have one or more additional coatings based on organic or inorganic lacquer systems, silicone compositions or low melting glazes.
摘要翻译：制备水性悬浮液，除了水之外，由2〜50重量％的膨润土和无机纤维的混合物组成，无机纤维的比例为1〜30重量％，膨润土的比例为1〜30重量％％，其中固体的总量不超过50重量％。通过悬浮液，绝热成型体的机械性能得到改善，其用于隔热，并且例如通过将该悬浮液输送到绝热板上而含有热解法生产的二氧化硅作为填料。该悬浮液也可以在其上挤压纤维网或纤维毡的隔热成型体上输送。应用悬浮液后，几个绝热成型体可以结合在一起，其中由膨润土和无机纤维组成的涂层作为粘合剂。除了该层之外，绝热模制品可以具有一种或多种基于有机或无机漆系统，硅酮组合物或低熔点釉料的附加涂层。

4. 发明授权

US4444936A Bis-(silylethyl)-oligosulphides and process for their production 失效
标题翻译：双（甲硅烷基乙基） - 二硫化物及其生产方法
公开(公告)号：US4444936A
公开(公告)日：1984-04-24
申请号：US461432
申请日：1983-01-27
申请人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
发明人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
IPC分类号： C08L7/00 , C07F7/08 , C07F7/12 , C07F7/18 , C08G75/02 , C08G75/14 , C08K5/5425 , C08K5/548 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L101/00 , C08K5/06
CPC分类号： C08K5/548 , C07F7/12 , C07F7/182 , C08G75/02 , C08G75/14
摘要： Novel bis-(silylethyl)-oligosulphides are obtained by reacting a vinyl silane of the formula (CH.sub.2 .dbd.CH).sub.m --SiR.sub.n.sup.1 R.sub.4--(m+n) in which R represents chlorine, bromine, iodine, C.sub.1 --C.sub.3 -alkoxy, 2-methoxyethoxy, 2-ethoxyethoxy or hydroxy, R.sup.1 represents C.sub.1 --C.sub.3 -alkyl, phenyl or C.sub.5 --C.sub.7 -cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m+n is 1, 2 or 3 with sulphur as well as in a given case hydrogen sulphide in molar ratios of vinyl silane to sulphur of from 1:2.5 to 1:10 and vinyl silane to hydrogen sulphide of from 1:0 to 1:5 at temperatures between about 100.degree. and 200.degree. C. under pressure of from 1 to 25 bars (total pressure at the reaction) temperature) and in the presence of sulphidation catalysts known per se, in a given case followed by hydrolysis or partial hydrolysis of the reaction products. The bis-(silylethyl)-oligosulphides are used as reinforcing additives (adhesive agents) in crosslinkable rubber mixtures containing silicate fillers and in a given case carbon black as well as in a given case sulphur and other customary constituents.
摘要翻译：通过使式（CH2 = CH）m-SiRn1R4-（m + n）的乙烯基硅烷（其中R表示氯，溴，碘，C1-C3-烷氧基，2-甲基苯基）甲氧基乙氧基，2-乙氧基乙氧基或羟基，R1代表C1-C3-烷基，苯基或C5-C7-环烷基，n是0,1或2，m是1或2，m + n是1,2或3，以及在给定情况下，在约100至200℃的温度下，乙烯基硅烷与硫的摩尔比为1:2.5至1:10的硫化氢和乙烯基硅烷至硫化氢的摩尔比为1:0至1:5 在1至25巴（反应总压力）温度的压力下，在本身已知的硫化催化剂的存在下，在给定的情况下，随后水解或部分水解反应产物。双（甲硅烷基乙基） - 二硫化物用作含有硅酸盐填料的交联性橡胶混合物中的增强添加剂（粘合剂），在给定情况下用于炭黑以及在给定情况下硫和其它常规组分。

5. 发明授权

US5362541A Shaped articles for heat insulation 失效
标题翻译：异形物品用于隔热
公开(公告)号：US5362541A
公开(公告)日：1994-11-08
申请号：US147095
申请日：1993-11-03
申请人： Gerhard Sextl , Roland Reuter , Peter Kleinschmit , Rudolf Schwarz , Ilona Sporys
发明人： Gerhard Sextl , Roland Reuter , Peter Kleinschmit , Rudolf Schwarz , Ilona Sporys
IPC分类号： C04B30/00 , B32B1/02 , B32B9/00
CPC分类号： C04B30/00 , Y10T428/231 , Y10T428/239
摘要： A preferably platelike form body for use as heat insulation, consisting of:a) a finely divided, powdery or fibrous material,b) a microporous casing andc) a gas and watertight casing.The form body is produced by optionally drying the powdery or fibrous material, optionally placing it into a microporous casing, optionally pressing it and then optionally drying it. Then, the powdery material is placed with the microporous casing into a gas and watertight casing. This gas and watertight casing is optionally evacuated and sealed.
摘要翻译：用作隔热材料的优选板状体，由以下部分组成：a）细碎的粉状或纤维状材料，b）微孔套管，c）气体和水密套管。通过任选地干燥粉末或纤维材料，任选地将其置于微孔壳体中，任选地将其压制，然后任选地将其干燥来制造成形体。然后，将粉状材料与微孔套管一起放入气体和水密套管中。该气体和水密外壳可选择地抽真空并密封。

6. 发明授权

US5120701A Titanium dioxide compacts, method of their production and a catalyst coated on a carrier of titanium dioxide 失效
标题翻译：二氧化钛溶液，其生产方法和涂覆在二氧化钛载体上的催化剂
公开(公告)号：US5120701A
公开(公告)日：1992-06-09
申请号：US676176
申请日：1991-03-28
申请人： Reinhold Brand , Bernd Engler , Martin Foerster , Werner Hartmann , Peter Kleinschmit , Edgar Koberstein , Johannes Ohmer , Rudolf Schwarz
发明人： Reinhold Brand , Bernd Engler , Martin Foerster , Werner Hartmann , Peter Kleinschmit , Edgar Koberstein , Johannes Ohmer , Rudolf Schwarz
IPC分类号： B01J21/06 , B01J35/10 , B01J37/00 , B28B3/20 , C04B35/46
CPC分类号： B01J21/063 , B01J35/1014 , B01J35/1038 , B01J35/1052 , B01J35/1061 , B01J37/0009 , C04B35/46
摘要： Titanium dioxide compacts are produced by intensively mixing pyrogenically produced titanium dioxide in the presence of deionized water with a wetting agent and/or with a base and/or optionally with a binder and/or optionally with an auxiliary deformation agent and/or optionally with a pore former, extruding the mass thus obtained at pressures between 5 and 100 bars to form shaped articles, drying the shaped articles at temperatures between 50.degree. and 120.degree. C. and subsequently calcining the shaped articles in the ambient air at temperatures of 400.degree. to 700.degree. C. for 1 to 5 hours.
摘要翻译：二氧化钛压块是通过在去离子水的存在下与润湿剂和/或与基底和/或任选地与粘合剂和/或任选地与辅助变形剂和/或任选地与在50至100巴之间的压力下挤出由此获得的物料以形成成型制品，在50至120℃的温度下干燥成形制品，随后在400℃至400℃的温度下在环境空气中煅烧成型制品 700℃下1〜5小时。

7. 发明授权

US4286990A Temperature stabilized, pyrogenically produced aluminum oxide-mixed oxide, the process for its production and use 失效
标题翻译：温度稳定，热解生成的氧化铝 - 混合氧化物，其生产和使用的过程
公开(公告)号：US4286990A
公开(公告)日：1981-09-01
申请号：US174342
申请日：1980-07-31
申请人： Peter Kleinschmit , Rudolf Schwarz
发明人： Peter Kleinschmit , Rudolf Schwarz
IPC分类号： C01B13/22 , C01F7/00 , C01F7/06 , C01F7/30 , C04B14/30 , C04B30/00 , C04B35/10
CPC分类号： C01B13/22 , C01F7/00 , C01F7/302 , C04B14/30 , C04B30/00 , C04B35/10 , C01P2004/03 , C01P2004/50 , C01P2004/61 , C01P2006/12
摘要： There is provided temperature stabilized pyrogenically produced aluminum oxide-mixed oxide having a BET surface area of 50 to 200 m.sup.2 /g which contains 0.5 to 20 weight % silicon dioxide as a constituent thereof. Because of the silicon dioxide constituent the aluminum oxide does not change into the .alpha.-Al.sub.2 O.sub.3 phase until 1350.degree. C. The temperature stabilized aluminum oxide-mixed oxide is suitable for the production of thermal insulation compositions.
摘要翻译：提供温度稳定的热解法生产的氧化铝混合氧化物，其BET表面积为50〜200m 2 / g，其含有0.5〜20重量％的二氧化硅作为其成分。由于二氧化硅组分，氧化铝直到1350℃才改变为α-Al2O3相。温度稳定的氧化铝混合氧化物适用于生产隔热组合物。

8. 发明授权

US5316816A Form body for heat insulation and vacuum insulation panel with asymmetric design 失效
标题翻译：隔热型绝热面板和非对称设计的真空绝热面板
公开(公告)号：US5316816A
公开(公告)日：1994-05-31
申请号：US7129
申请日：1993-01-22
申请人： Gerhard Sextl , Hans Strack , Roland Reuter , Ilona Fuss , Peter Kleinschmit , Rudolf Schwarz
发明人： Gerhard Sextl , Hans Strack , Roland Reuter , Ilona Fuss , Peter Kleinschmit , Rudolf Schwarz
IPC分类号： F16L59/02 , B32B1/06 , B32B5/16
CPC分类号： F16L59/028 , Y10T428/231 , Y10T428/237 , Y10T428/238 , Y10T428/239
摘要： A shaped body, preferably plate-shaped, for use as heat insulation, formed of (a) a finely distributed, powdery or fibrous substance, (b) a microporous casing, and (c) a gastight and watertight, metal-free casing. The shaped body is produced by drying a powdery or fibrous substance if necessary, optionally placing it into a microporous casing, optionally pressing and then optionally drying. Thereafter, the powdery substance is placed with the microporous casing into a gastight and watertight, metal-free casing. This gastight and watertight casing is optionally evacuated and sealed. Furthermore, a shaped article, preferably plate-shaped, for use as heat insulation, produced from (a) a finely distributed, powdery or fibrous substance with a water absorption capacity of 4 to 50% by weight at 23.degree. C. and 85% relative humidity, (b) a casing of two parts with asymmetric design which contains this finely distributed, powdery or fibrous substance, the first part of the casing being metal-free and concave in such a manner that it is completely filled by the preferably plate-like shaped article and the second part being metal-free or metallic and planar and connected to the trough in such a manner that a gastight and water-vapor-tight seal is assured and both parts having water-vapor-permeabilities between 0 and 0.2 g/m.sup.2 /d at 23.degree. C. and 85% relative humidity and gas permeabilities for N.sub.2, O.sub.2 and CO.sub.2 of in sum 0 to 0.5 cm.sup.3 /m.sup.2 d/bar at 23.degree. C.; the shaped article having the property of absorbing water up to an amount of 2 to 15% by weight without its thermal conductivity deteriorating more than 25%.
摘要翻译：由（a）精细分布的粉状或纤维状物质形成的成型体，优选为板状，（b）微孔外壳，（c）气密和水密的无金属外壳。如果需要，通过干燥粉末或纤维状物质，任选地将其置于微孔套管中，任选地按压然后任选地干燥而制成成形体。此后，将粉状物质与微孔套管一起置于气密和防水，无金属的外壳中。这种气密和防水外壳可选择地抽真空并密封。此外，用作绝热的成型制品，优选为板状，由（a）精细分布的粉末状或纤维状物质制成，其吸水量在23℃下为4〜50重量％，85重量％相对湿度，（b）具有不对称设计的两部分的壳体，其包含这种精细分布的粉状或纤维状物质，壳体的第一部分是无金属和凹入的，使得其被优选板完全填充并且第二部分是无金属的或金属的和平面的，并且以这样的方式连接到槽，使得保证气密和水蒸气密封，并且两个部分的水蒸汽渗透性在0和0.2之间在23℃和85％相对湿度下的g / m 2 / d和在23℃下为0至0.5cm 3 / m 2d / bar的N 2，O 2和CO 2的气体渗透性。该成型制品具有吸水量至多2至15重量％的特性，而其导热率不会降低25％以上。

9. 发明授权

US5089247A Process for producing zirconium-doped pseudoboehmite 失效
标题翻译：生产ZIRCONIUM-DOPED PSEUDOBOEHMITE的方法
公开(公告)号：US5089247A
公开(公告)日：1992-02-18
申请号：US489795
申请日：1990-03-05
申请人： Anh T. Liu , Rudolf Schwarz , Peter Kleinschmit
发明人： Anh T. Liu , Rudolf Schwarz , Peter Kleinschmit
IPC分类号： B01J21/06 , B01J35/10 , B01J37/00 , C01F7/00 , C01F7/34 , C01G25/00
CPC分类号： B01J21/066 , B01J37/0045 , C01F7/00 , C01F7/34 , C01G25/00 , B01J35/1019 , B01J35/1038 , C01P2002/52 , C01P2002/72 , C01P2006/12
摘要： Zirconium-doped pseudoboehmite with the following properties: zirconium content of 0.5 to 10 mol % relative to Al water content of 20 to 35 weight percent total of the anionic impurities less than 0.5 weight percent. It is synthesized by a process wherein zirconium salt is added in calculated quantity to an aqueous aluminum sulfate solution, the resulting mixture is fed simultaneously with a sodium aluminate liquor into a water pool having a temperature of 50.degree. to 100.degree. C., thereby precipitating zirconium-doped alumina gel while a pH of 3.5 to 8 is maintained, the pH of the suspension is adjusted after addition of the aluminum sulfate solution to 8.5 to 10.5 by further addition of sodium aluminate liquor, the suspension is digested if necessary at the pH of 8.5 to 10.5 and the temperature of 50.degree. to 100.degree. C. for a period of up to 24 hours, the formed pseudoboehmite crystals are filtered off, the filter cake is redispersed with water and the suspension is sprayed-dried. By calcining at 700.degree. to 1100.degree. C., preferably at 850.degree. to 950.degree. C., the pseudoboehmite is further processed to zirconium-doped gamma-alumina suitable for automobile exhaust catalysts.

10. 发明授权

US4529532A Process for the production of binder-free press-molded heat-insulating parts 失效
标题翻译：用于生产无粘合剂的压模绝热部件的方法
公开(公告)号：US4529532A
公开(公告)日：1985-07-16
申请号：US579913
申请日：1984-02-13
申请人： Sabine Gliem , Peter Kleinschmit , Rudolf Schwarz
发明人： Sabine Gliem , Peter Kleinschmit , Rudolf Schwarz
IPC分类号： C04B30/02 , C04B43/00
CPC分类号： C04B30/02
摘要： Binder-free mixtures of heat-insulating material are mixed with substances showing a basic reaction in aqueous solution during the mixing process and are then press-molded to press-molded heat-insulating parts.
摘要翻译：将混合绝热材料的无粘合剂与在混合过程中在水溶液中显示出碱性反应的物质混合，然后将其压模到压模式绝热部件上。

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