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    • 9. 发明授权
    • Apparatus and method for monitoring corrosion and cracking of alloys during live well testing
    • 在活井试验过程中监测合金的腐蚀和开裂的装置和方法
    • US09033036B2
    • 2015-05-19
    • US13106036
    • 2011-05-12
    • Christian WilkinsonIndranil RoyStephane Hiron
    • Christian WilkinsonIndranil RoyStephane Hiron
    • E21B47/00
    • E21B47/00Y10S166/902
    • Embodiments may take the form of a tool string sub. The tool string sub may include a longitudinally extending tubular housing having an outside surface and an inside surface. A stepped circumferential portion of the inside surface of the housing bisects the interior surface of the housing. A degradation part is connected adjacent to the stepped portion of the housing and is supported by the housing and at least one moveable support part protruding inward and beyond the inner surface of the housing. The support part has a first position where the degradation part is at first stress and a second position where the degradation part is at a second stress greater than the first stress. At least one end of the tool string sub is adapted to connect with a tool string.
    • 实施例可以采用工具串子的形式。 工具串sub可以包括具有外表面和内表面的纵向延伸的管状外壳。 壳体内表面的台阶周向部分将壳体的内表面平分。 劣化部分与壳体的阶梯部分相邻地连接并且由壳体支撑并且至少一个可移动的支撑部分向内突出并超出壳体的内表面。 支撑部分具有第一位置,其中劣化部分处于第一应力,第二位置处劣化部分处于比第一应力大的第二应力。 工具串子的至少一端适于与工具串连接。
    • 10. 发明授权
    • Diamondoid stabilized fine-grained metals
    • 金刚石稳定细粒金属
    • US08628599B2
    • 2014-01-14
    • US12204763
    • 2008-09-04
    • James C. EarthmanFarghalli A. MohamedRahul K. MishraIndranil Roy
    • James C. EarthmanFarghalli A. MohamedRahul K. MishraIndranil Roy
    • B22F1/00B22F1/02C22C1/05
    • B22F1/0044B22F2999/00C22C1/1084C22C32/0084B22F2202/03B22F1/0085
    • Thermal stability of cryomilled Al+1% diamantane was investigated in the temperature range of 423 to 773K. Diamantane is a nanosized hydrocarbon molecule with a 14 carbon atom diamond cubic framework that is terminated by hydrogen atoms. Following the cryomilling of the Al powders and diamantane cages, the average grain size characterized using transmission electron microscopy (TEM) and X-ray diffraction (XRD). The as-cryomilled grain sized was found to be of the order of 22 nm, essentially the same as that for Al cryomilled without diamantane. To determine thermal stability, the powders were sealed in glass tubes in an Ar atmosphere to avoid oxidation and contamination and annealed at different temperatures between 423 and 773K for different holding times. Following these treatments, the grain size of cryomilled Al+1% diamantane was consistently less than that for cryomilled Al by about a factor of two. Preliminary investigations indicate that the grain growth exponent n decreased with increasing temperature, reaching a value of approximately 35 at 423 K. Such a high value of n suggests the operation of strong pinning forces on boundaries during annealing treatment. The thermal stability data were found to be consistent with Burke's model based on drag forces exerted by dispersion particles.
    • 在423〜773K的温度范围内研究了冷冻Al + 1%的金刚烷的热稳定性。 金刚烷是具有14个碳原子的金刚石立方体骨架的纳米级烃分子,其由氢原子终止。 在Al粉末和金刚烷笼的冷冻冷却之后,使用透射电子显微镜(TEM)和X射线衍射(XRD)表征的平均晶粒尺寸。 发现低密度颗粒大小为22nm的量级,基本上与没有金刚烷的低温冷却的Al一样。 为了确定热稳定性,将粉末在Ar气氛中的玻璃管中密封,以避免氧化和污染,并在不同的保持时间在423和773K之间的不同温度下退火。 在这些处理之后,冷冻Al + 1%二金刚的晶粒尺寸一直低于低温Al的晶粒大约二分之一。 初步研究表明,晶粒生长指数n随着温度的升高而降低,在423K时达到约35的值。这样高的n值表明在退火处理过程中边界强的钉扎力的作用。 发现热稳定性数据与基于分散粒子施加的阻力的伯克模型一致。