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1. 发明授权

US06740702B2 Coating liquid for forming ink-receiving layer 失效
标题翻译：用于形成油墨接收层的涂布液
公开(公告)号：US06740702B2
公开(公告)日：2004-05-25
申请号：US10172916
申请日：2002-06-17
申请人： Hiroyasu Nishida , Mitsuru Nakai , Michio Komatsu
发明人： Hiroyasu Nishida , Mitsuru Nakai , Michio Komatsu
IPC分类号： C08K336
CPC分类号： B41M5/5218 , Y10T428/24802 , Y10T428/259
摘要： The invention provides a recording sheet having an ink-receiving layer, which comprises a substrate sheet and an ink-receiving layer formed thereon, said ink-receiving layer comprising oxide particles, wherein the ink-receiving layer has pores having a diameter in the range of 3.4 to 2,000 nm, the pore volume of pores having a diameter of 3.4 to 30 nm is in the range of 0.2 to 1.8 ml/g, and the pore volume of pores having a diameter of 30 to 2,000 nm is in the range of 0.1 to 1.5 ml/g. It is preferable that the oxide particles have an average particle diameter of 2 to 1,000 nm and are a mixture of hydrophobic oxide particles and hydrophilic oxide particles. This recording sheet shows sufficient strength, has excellent printability such that images of uniform density and high sharpness can be printed thereon without bleeding, and is excellent in water resistance, weathering resistance and fading resistance.
摘要翻译：本发明提供了一种具有油墨接收层的记录纸，其包括基板和形成在其上的油墨接收层，所述油墨接收层包括氧化物颗粒，其中油墨接收层具有直径在该范围内的孔为3.4〜2000nm，直径为3.4〜30nm的孔的孔体积为0.2〜1.8ml / g，直径为30〜2000nm的孔的孔体积为 0.1〜1.5ml / g。优选氧化物粒子的平均粒径为2〜1000nm，是疏水性氧化物粒子和亲水性氧化物粒子的混合物。该记录片材具有足够的强度，具有优异的可印刷性，使得能够在不渗色的情况下在其上印刷均匀的密度和高锐度的图像，并且具有优异的耐水性，耐候性和抗褪色性。

2. 发明授权

US06680040B1 Sol having fine particles dispersed and method for preparing 有权
标题翻译：具有分散细颗粒的溶胶和制备方法
公开(公告)号：US06680040B1
公开(公告)日：2004-01-20
申请号：US09868860
申请日：2001-06-21
申请人： Hiroyasu Nishida , Mitsuru Nakai , Michio Komatsu , Hiroo Yoshitome
发明人： Hiroyasu Nishida , Mitsuru Nakai , Michio Komatsu , Hiroo Yoshitome
IPC分类号： C01B3312
CPC分类号： C08K9/02 , C03C17/007 , C03C2217/425 , C03C2217/475 , C04B41/009 , C04B41/4584 , C04B41/81 , C04B2111/80 , C08K9/04 , C04B41/4537 , C04B41/4582 , C04B41/5035 , C04B41/526 , C04B41/5037 , C04B35/14 , C04B35/16 , C04B35/18
摘要： The porous composite oxide particle is coated with a porous silica-based inorganic oxide layer, and also a substrate has a coating film with the fine particles thereon, which has a low refractive index and excellent in adhesion with a resin or the like, strength, the ability to reduce reflection and the like. The fine particles include porous composite oxide with silica and an inorganic oxide other than silica, wherein the fine particles are coated with a porous silica-based inorganic oxide layer having a thickness from 0.5 to 20 nm. The fine particles include preferably an organic group directly bonded to silicon, and SR/ST, the ratio of the molar amount of silicon having the organic group directly bonded thereto (SR) vs the molar amount of the total silicon (ST), is preferably in the range from 0.001 to 0.9.
摘要翻译：多孔复合氧化物粒子涂布有多孔二氧化硅系无机氧化物层，并且基板也具有其上具有低折射率和与树脂等的粘合性优异的其上的微粒的涂膜，强度，减少反射等的能力。细颗粒包括具有二氧化硅的多孔复合氧化物和除二氧化硅之外的无机氧化物，其中细颗粒涂覆有厚度为0.5至20nm的多孔二氧化硅基无机氧化物层。微粒优选包括与硅直接键合的有机基团，SR / ST（直接键合有机基团的硅的摩尔量（SR））与总硅的摩尔量（ST）的比例优选为在0.001至0.9的范围内。

3. 发明授权

US06447881B1 Recording sheet having ink-receiving layer 有权
标题翻译：具有油墨接收层的记录纸
公开(公告)号：US06447881B1
公开(公告)日：2002-09-10
申请号：US09220134
申请日：1998-12-23
申请人： Hiroyasu Nishida , Mitsuru Nakai , Michio Komatsu
发明人： Hiroyasu Nishida , Mitsuru Nakai , Michio Komatsu
IPC分类号： B41M500
CPC分类号： B41M5/5218 , Y10T428/24802 , Y10T428/259
摘要： The invention provides a recording sheet having an ink-receiving layer, which comprises a substrate sheet and an ink-receiving layer formed thereon, said ink-receiving layer comprising oxide particles, wherein the ink-receiving layer has pores having a diameter in the range of 3.4 to 2,000 nm, the pore volume of pores having a diameter of 3.4 to 30 nm is in the range of 0.2 to 1.8 ml/g, and the pore volume of pores having a diameter of 30 to 2,000 nm is in the range of 0.1 to 1.5 ml/g. It is preferable that the oxide particles have an average particle diameter of 2 to 1,000 nm and are a mixture of hydrophobic oxide particles and hydrophilic oxide particles. This recording sheet shows sufficient strength, has excellent printability such that images of uniform density and high sharpness can be printed thereon without bleeding, and is excellent in water resistance, weathering resistance and fading resistance.
摘要翻译：本发明提供了一种具有油墨接收层的记录纸，其包括基板和形成在其上的油墨接收层，所述油墨接收层包括氧化物颗粒，其中油墨接收层具有直径在该范围内的孔为3.4〜2000nm，直径为3.4〜30nm的孔的孔体积为0.2〜1.8ml / g，直径为30〜2000nm的孔的孔体积为 0.1〜1.5ml / g。优选氧化物粒子的平均粒径为2〜1000nm，是疏水性氧化物粒子和亲水性氧化物粒子的混合物。该记录片材具有足够的强度，具有优异的可印刷性，使得能够在不渗色的情况下在其上印刷均匀的密度和高锐度的图像，并且具有优异的耐水性，耐候性和抗褪色性。

4. 发明申请

US20070249736A1 Titanium-Containing Silica Sol and Process for Producing the Same, Antifouling Film and Base Material with Ink-Receptive Layer, and Method for Reproducing Recording Base Material 审中-公开
标题翻译：含钛二氧化硅溶胶及其制造方法，具有油墨接受层的防污膜和基材以及用于再现记录基材的方法
公开(公告)号：US20070249736A1
公开(公告)日：2007-10-25
申请号：US11661799
申请日：2005-09-01
申请人： Manabu Watanabe , Tatsuo Ogawa , Hiroyasu Nishida , Michio Komatsu
发明人： Manabu Watanabe , Tatsuo Ogawa , Hiroyasu Nishida , Michio Komatsu
IPC分类号： C01G23/047 , B41M5/00 , B41M5/50 , B41M5/52 , C01B33/149
CPC分类号： C01B33/146 , B41M5/5218 , B82Y30/00 , C01B33/149 , C01P2002/30 , C01P2004/34 , C01P2004/64 , C01P2006/12 , C01P2006/40 , C08K3/22 , C08K3/36 , C08K7/26 , C08K9/04 , C09C1/3054 , C09C1/3607 , C09D1/00 , C09D5/1618 , C09D7/62 , C09D7/67 , Y02P20/582
摘要： It is an object of the present invention to provide a material which is applied to substrates by an easy and simple process, is applicable to substrates of a wide range and is capable of forming an antifouling film exhibiting excellent antifouling performance, and a substrate with an ink-receiving layer having excellent decoloring property. The titanium-containing silica sol of the invention includes (a) the following fine particles (a1) or the following fine particles (a2) and (b) a dispersion medium: (a1) titania fine particles having a mean particle diameter of 2 to 50 nm and porous silica fine particles having a mean particle diameter of 5 to 100 nm and a specific surface area, as determined by BET method, of not less than 300 m2/g, or (a2) porous silica fine particles obtained by surface-modifying surfaces of porous silica fine particles having a mean particle diameter of 5 to 100 nm and a specific surface area, as determined by BET method, of not less than 300 m2/g with a titanate compound.
摘要翻译：本发明的目的是提供一种通过简单和简单的方法施加到基材上的材料，可应用于宽范围的基材，并且能够形成显示出优异的防污性能的防污膜，以及具有油墨接收层具有优异的脱色性能。本发明的含钛硅溶胶包含（a）下述细颗粒（a1）或以下微粒（a2）和（b）分散介质：（a1）平均粒径为2〜 50nm，通过BET法测定的平均粒径为5〜100nm，比表面积为300μm2 / g以上的多孔二氧化硅微粒，或（a2）通过BET法测定的平均粒径为5〜100nm的多孔二氧化硅微粒表面改性比表面积为300μm2以上的多孔二氧化硅微粒 > / g与钛酸盐化合物。

5. 发明申请

US20050037201A1 Inorganic compound particle and process for preparation thereof 有权
标题翻译：无机化合物颗粒及其制备方法
公开(公告)号：US20050037201A1
公开(公告)日：2005-02-17
申请号：US10898894
申请日：2004-07-26
申请人： Toshiharu Hirai , Hiroyasu Nishida , Michio Komatsu
发明人： Toshiharu Hirai , Hiroyasu Nishida , Michio Komatsu
IPC分类号： C03C17/00 , C03C17/34 , C03C17/36 , C01B15/14 , B32B5/16
CPC分类号： C03C17/3655 , C03C17/007 , C03C17/34 , C03C17/36 , C03C17/3676 , C03C2217/425 , C03C2217/445 , C03C2217/475 , C03C2217/76 , C03C2217/78 , Y10T428/249953 , Y10T428/249962 , Y10T428/249998 , Y10T428/25 , Y10T428/2982 , Y10T428/2984 , Y10T428/2991 , Y10T428/2993 , Y10T428/2995 , Y10T428/2996 , Y10T428/2998
摘要： Inorganic compound particles constituted of a shell, a porous matter or a cavity enclosed therein, and the porous matter or the cavity being kept unchanged in a subsequently formed transparent coating film.
摘要翻译：由外壳，多孔物质或其中包围的空腔构成的无机化合物颗粒，并且多孔物质或空腔在随后形成的透明涂膜中保持不变。

6. 发明授权

US5935700A Thermoplastic resin film containing composite oxide particles 失效
标题翻译：含复合氧化物颗粒的热塑性树脂薄膜
公开(公告)号：US5935700A
公开(公告)日：1999-08-10
申请号：US737937
申请日：1996-12-05
申请人： Naoyuki Enomoto , Hiroyasu Nishida , Michio Komatsu
发明人： Naoyuki Enomoto , Hiroyasu Nishida , Michio Komatsu
IPC分类号： B29D7/01 , C08J5/18 , G11B5/73 , G11B5/733 , B32B27/18 , B32B27/36
CPC分类号： C08J5/18 , B29D7/01 , G11B5/733 , B29K2067/00 , B29K2105/16 , B29K2995/0087 , C08J2367/02 , Y10T428/256 , Y10T428/257 , Y10T428/258 , Y10T428/259 , Y10T428/31786
摘要： A thermoplastic resin film excellent in slipperiness, wear resistance and transparency contains 0.05 to 0.5 wt. % of specified fine particles of composite oxide comprising silica, alkali metal oxide, and at least one inorganic oxide other than silica, wherein the fine particles satisfies the following expression (I):S .gtoreq.10,000/(Dp*SG) (I)wherein S indicates the specific surface area (m.sup.2 /g) of the fine particles of composite oxide, Dp indicates the average diameter (nm) of the fine particles, and SG indicates the true specific gravity thereof. The film is preferably a polyester film having a hazing value of 5% or less. It is suitable for use as magnetic tape, capacitor, photographic film and pressure-sensitive adhesive tape. The film is manufactured by adding a silicate of alkali metals, ammonium or organic bases and an alkali-soluble inorganic compound simultaneously to an alkali solution with pH 9 or above, generating fine particles of composite oxide without any control of the pH of this reaction solution, adding the obtained sol to a thermoplastic resin and/or the reaction system thereof, and processing of a film.
摘要翻译： PCT No.PCT / JP95 / 01093 Sec。 371日期：1996年12月5日 102（e）日期1996年12月5日PCT提交1995年6月5日PCT公布。公开号WO95 / 33787 日期1995年12月14日耐滑性，耐磨性和透明性优异的热塑性树脂膜含有0.05〜0.5重量％％的包含二氧化硅，碱金属氧化物和除二氧化硅以外的至少一种无机氧化物的复合氧化物的特定细颗粒，其中所述细颗粒满足以下表达式（I）：S> = 10,000 /（Dp * SG）（I ）其中S表示复合氧化物微粒的比表面积（m2 / g），Dp表示细颗粒的平均直径（nm），SG表示其真比重。该膜优选为具有5％以下的雾度值的聚酯膜。适用于磁带，电容器，照相胶片和压敏胶带。该膜通过将碱金属，铵或有机碱的硅酸盐和碱溶性无机化合物同时加入到pH9或更高的碱溶液中来制备，产生复合氧化物的微粒，而无需控制该反应溶液的pH值将所得溶胶加入到热塑性树脂和/或其反应体系中，加工薄膜。

7. 发明授权

US5785892A Organo-antimony oxide sols and coating compositions thereof 失效
标题翻译：有机氧化锑溶胶及其涂料组合物
公开(公告)号：US5785892A
公开(公告)日：1998-07-28
申请号：US137140
申请日：1994-03-22
申请人： Hiroyasu Nishida , Yoshichika Tanaka , Michio Komatsu , Teruo Migita
发明人： Hiroyasu Nishida , Yoshichika Tanaka , Michio Komatsu , Teruo Migita
IPC分类号： B01J13/00 , C01G30/00 , H01B1/08 , H01B1/20 , C08K3/20
CPC分类号： C01G30/005 , B01J13/0021 , B01J13/0026 , H01B1/08 , H01B1/20 , C01P2002/36 , C01P2004/80 , C01P2006/40 , C01P2006/60 , Y10T428/2995
摘要： An organo-antimony oxide sol capable of affording an electrical conductivity property and a photo-setting coating composition containing such a sol are provided. The particulate colloidal antimony oxide, i.e. a dispersoid in the sol, has a pyrochlore structure and is surface-treated with an organo-silicon compound of the formula ##STR1## wherein R.sup.2 is hydrogen or a C.sub.1 -C.sub.5 alkyl group; R.sup.3 is hydrogen or a C.sub.1 -C.sub.5 alkyl group; R.sup.4 is a C.sub.1 -C.sub.8 alkylene group; R.sup.5 is hydrogen or a C.sub.1 -C.sub.8 alkyl group; i is an integer of 1-3; j is an integer of 0-2; and k is an integer of 1-3 equal to i+j.
摘要翻译： PCT No.PCT / JP92 / 00536 Sec。 371日期：1994年3月22日 102（e）1994年3月22日PCT提交1992年4月24日PCT公布。出版物WO92 / 日期：1992年11月12日提供能够提供导电性的有机 - 氧化锑溶胶和含有这种溶胶的光固化涂料组合物。颗粒状胶体氧化锑，即溶胶中的分散质，具有烧绿石结构，并用下式的有机硅化合物（1）进行表面处理，其中R2是氢或C1-C5烷基; R3是氢或C1-C5烷基; R4是C1-C8亚烷基; R5是氢或C1-C8烷基; 我是1-3的整数; j是0-2的整数; 并且k是等于i + j的1-3的整数。

8. 发明授权

US4925704A Processes for preparing mono-dispersed particles 失效
标题翻译：制备单分散颗粒的方法
公开(公告)号：US4925704A
公开(公告)日：1990-05-15
申请号：US206863
申请日：1988-06-13
申请人： Goro Sato , Michio Komatsu , Hiroyasu Nishida , Yoshichika Tanaka , Tsuguo Koyanagi , Kei Mihara
发明人： Goro Sato , Michio Komatsu , Hiroyasu Nishida , Yoshichika Tanaka , Tsuguo Koyanagi , Kei Mihara
IPC分类号： C01B13/32 , C01B33/16 , C01G23/053 , C01G25/02 , G02F1/1339
CPC分类号： C01B33/163 , C01B13/32 , C01G23/053 , C01G25/02 , G02F1/13392 , C01P2004/03 , C01P2004/32 , C01P2004/52 , C01P2004/61 , C01P2004/62 , C01P2006/22 , C01P2006/60 , Y10T428/2998
摘要： In a process for preparing spherical particles of a metal oxide or hydroxide having a particle size of from 0.1 to 10 .mu.m by adding a corresponding metal alkoxide to a dispersion of water-alcohol system having dispersed therein a metal oxide or hydroxide as a seed, under alkaline conditions and allowing a decomposition product from said metal alkoxide to attach onto said seed to effect particle growth of the seed, the improvement which comprises maintaining said dispersion at a substantially constant pH within the range between 10 and 13 during the addition of the metal alkoxide to said dispersion and the subsequent particle growth of the seed, thereby to prepare mono-dispersed particles substantially free from particle aggregation having a sharp particle size distribution of a standard deviation of not greater than 0.5. The white particles so prepared may be, after separation, heat treated to provide black particles. The white or black particles may be coated with a synthetic resin in the surface. The products are useful particularly as spacers for liquid crystal display devices.
摘要翻译：在通过向其中分散有金属氧化物或氢氧化物作为种子的水 - 醇体系的分散体中加入相应的金属醇盐来制备粒径为0.1至10μm的金属氧化物或氢氧化物的球形颗粒的方法中，在碱性条件下并允许来自所述金属醇盐的分解产物附着在所述种子上以实现种子的颗粒生长，其改进包括在添加金属期间将所述分散体保持在10至13之间的基本恒定的pH值在10和13之间的范围内所述分散体和随后的种子颗粒生长，从而制备基本上不具有标准偏差不大于0.5的尖锐粒度分布的颗粒聚集的单分散颗粒。如此制备的白色颗粒可以在分离后进行热处理以提供黑色颗粒。白色或黑色颗粒可以在表面上涂覆合成树脂。该产品特别用作液晶显示装置的间隔物。

9. 发明授权

US06669748B2 Dispersion liquid of silica particles for polishing, method of producing the same, and polishing agent 有权
标题翻译：用于抛光的二氧化硅颗粒的分散液，其制造方法和抛光剂
公开(公告)号：US06669748B2
公开(公告)日：2003-12-30
申请号：US10254992
申请日：2002-09-26
申请人： Hiroyasu Nishida , Yoshinori Wakamiya , Manabu Watanabe , Michio Komatsu
发明人： Hiroyasu Nishida , Yoshinori Wakamiya , Manabu Watanabe , Michio Komatsu
IPC分类号： C09K314
CPC分类号： C09K3/1463 , C09G1/02 , C09K3/1409 , H01L21/31053 , H01L21/3212
摘要： The present invention provides a dispersion liquid of silica particles for polishing with a low content of Na ions and also with a content of ions other than Na ions in a prespecified range. This dispersion liquid is a dispersion liquid of silica particles in which the silica particles having the average particle diameter in the range from 5 to 300 nm is dispersed, and a content of Na ions in the silica particle is less than 100 ppm, while a contents of ions other than Na ions is in the range from 300 ppm to 2 weight %.
摘要翻译：本发明提供了一种二氧化硅颗粒的分散液，其用于以低含量的Na离子进行抛光，并且在预定范围内提供除Na离子之外的其他离子的含量。该分散液是分散平均粒径为5〜300nm的二氧化硅粒子的二氧化硅粒子的分散液，二氧化硅粒子中的Na离子的含量小于100ppm，的Na离子之外的离子在300ppm至2重量％的范围内。

10. 发明授权

US06849112B2 Inorganic particles as a dental material and a method of producing the same 有权
标题翻译：作为牙科用材料的无机粒子及其制造方法
公开(公告)号：US06849112B2
公开(公告)日：2005-02-01
申请号：US10291550
申请日：2002-11-12
申请人： Hiroyasu Nishida , Noboru Senju , Michio Komatsu
发明人： Hiroyasu Nishida , Noboru Senju , Michio Komatsu
IPC分类号： A61K6/027 , A61K6/02 , A61K6/04 , A61K6/06 , C01B33/12 , C04B38/00 , A61K6/08
CPC分类号： C04B35/63 , A61K6/0008 , A61K6/0076 , A61K6/0088 , A61K6/0235 , A61K6/024 , A61K6/0245 , A61K6/0255 , C04B35/62655 , C04B38/009 , C04B2111/00836 , C04B2235/3213 , C04B2235/3215 , C04B2235/3217 , C04B2235/3225 , C04B2235/3227 , C04B2235/3232 , C04B2235/3244 , C04B2235/3284 , C04B2235/3409 , C04B2235/3418 , C04B2235/5409 , C04B2235/5436 , C04B2235/9646 , C04B12/04 , C04B22/08 , C04B28/24 , C04B40/0082 , A61K6/083 , C08L43/04 , C08L33/14 , C08L33/10
摘要： Amorphous inorganic particles as a dental material includes silica and inorganic oxide(s) other than silica and has high x-ray impermeability. The inorganic particles as a dental material includes silica with the content in the range from 70 to 98 weight % and oxide(s) of one or more elements selected from the group of Zr, Ti, La, Ba, Sr, Hf, Y, Zn, AL, and B, wherein 5 to 70 weight % of the silica is originated from an acidic silicic acid solution and 30 to 95 weight % of the silica is originated from a sol of silica. The inorganic particles as a dental material have an average particle diameter in the range from 1 to 10 μm, specific surface area in the range from 50 to 350 m2/g, pore volume in the range from 0.05 to 0.5 ml/g, amorphous crystallinity as observed by x-ray diffraction, and the refractive index in the range from 1.47 to 1.60.
摘要翻译：作为牙科材料的无定形无机颗粒包括除二氧化硅之外的二氧化硅和无机氧化物，并且具有高x射线不渗透性。作为牙科用材料的无机粒子包含含量为70〜98重量％的二氧化硅和选自Zr，Ti，La，Ba，Sr，Hf，Y， Zn，AL和B，其中5至70重量％的二氧化硅来自酸性硅酸溶液，30至95重量％的二氧化硅源自二氧化硅溶胶。作为牙科用材料的无机粒子的平均粒径为1〜10μm，比表面积为50〜350m 2 / g，孔体积为0.05〜0.5ml / g ，通过x射线衍射观察到的无定形结晶度，折射率在1.47至1.60的范围内。

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