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    • 2. 发明授权
    • Magnetic recording medium and a method for preparing the medium
    • 磁记录介质及其制备方法
    • US5035948A
    • 1991-07-30
    • US576103
    • 1990-08-31
    • Shinji SaitoHiroshi Ogawa
    • Shinji SaitoHiroshi Ogawa
    • C09D5/23G11B5/716
    • G11B5/716Y10S428/90Y10T428/257Y10T428/265
    • A magnetic recording medium is disclosed, comprising a nonmagnetic support having thereon an under magnetic layer and an upper magnetic layer in that order, wherein the thickness of the upper magnetic layer is less than 0.5 .mu.m and abrasive agents, which have a Mohs' hardness of 6 or more and have an average particle diameter of 0.5 .mu.m or less, are contained in the upper magnetic layer. And a method for preparing a magnetic recording medium which comprises coating a coating composition for an under magnetic layer on a running non-magnetic support, and successively coating thereon a coating composition for an upper magnetic layer containing abrasive agents, which have a Mohs' hardness of 6 or more and an average particle diameter of 0.5 .mu.m or less, in a dry thickness of less than 0.5 .mu.m while the under magnetic layer is wet.
    • 公开了一种磁记录介质,其包括其上具有下磁性层和上磁性层的非磁性载体,其中上磁性层的厚度小于0.5μm,研磨剂具有莫氏硬度 6个以上,平均粒径为0.5μm以下,含有上层磁性层。 一种磁记录介质的制备方法,其特征在于,在运行中的非磁性载体上涂布下层磁性层用涂料组合物,并依次在其上涂覆含有摩擦硬度的含有研磨剂的上层磁性层用涂料组合物 为6个以上,平均粒径为0.5μm以下,干燥厚度小于0.5μm,而在磁性层下面是湿的。
    • 5. 发明授权
    • Magnetic recording medium
    • 磁记录介质
    • US4851289A
    • 1989-07-25
    • US150860
    • 1988-02-01
    • Hiroshi OgawaShinji SaitoToshihiko MiuraNobuo YamazakiHiroaki Araki
    • Hiroshi OgawaShinji SaitoToshihiko MiuraNobuo YamazakiHiroaki Araki
    • G11B5/714G11B5/716
    • G11B5/716G11B5/714Y10S428/90Y10T428/257
    • A magnetic recording medium comprising a non-magnetic support having provided thereon plural magnetic layers containing ferromagnetic particles and binders, wherein the ferromagnetic particles contained in the uppermost magnetic layer have an average long axis length measured by a transmission electron microscope of 0.25 .mu.m or less and a crystal size measured by an X-ray deffractiometory of 300 .ANG. or less, and the ferromagnetic particles contained in the magnetic layers other than the uppermost layer have an average long axis length measured by a transmission electron microscope of 0.25 .mu.m or less and a crystal size measured by an X-ray deffractiometory of 250 .ANG. more, provided that the ferromagnetic particles of the uppermost layer have a crystal size measured by an X-ray deffractiometory smaller than the crystal size measured by an X-ray deffractiometory of the ferromagnetic particles of the magnetic layers other than the uppermost layer.
    • 一种磁记录媒体,其特征在于,具有非磁性载体,其上设有包含铁磁性粒子和粘合剂的多个磁性层,其中,所述最上层的磁性层中所含的铁磁性粒子的平均长轴长度为0.25μm以下的透射型电子显微镜 以及通过300AWG以下的X射线折射率测定的结晶尺寸,除了最上层以外的磁性层中含有的铁磁性粒子具有0.25μm以下的透射型电子显微镜测定的平均长轴长度, 通过更大的250纳米X射线衍射仪测量的晶体尺寸,条件是最上层的铁磁颗粒具有通过X射线折射率测量的晶体尺寸,该晶体尺寸小于通过铁磁性X射线分解测量的晶体尺寸 除了最上层之外的磁性层的颗粒。
    • 6. 发明授权
    • Process for producing magnetic recording medium
    • 磁记录介质的制造方法
    • US4724162A
    • 1988-02-09
    • US39878
    • 1987-04-20
    • Shinji SaitoHiroshi OgawaChiaki MizunoToshio OnoYasuo Tamai
    • Shinji SaitoHiroshi OgawaChiaki MizunoToshio OnoYasuo Tamai
    • B01F3/12G11B5/702G11B5/842H01F10/02
    • G11B5/842G11B5/7028
    • An improvement of a process for producing a magnetic recording medium comprising coating a non-magnetic support with a magnetic paint comprising a magnetic layer forming component containing ferromagnetic powder and a resin component dispersed in an organic solvent and drying the coated layer. The improvement resides in the preparation of the magnetic paint. In the improvement, the magnetic paint is obtained by kneading said magnetic layer forming component and a first solvent having a solubility parameter of not lower than 9.5[cal..multidot.cm.sup.-3 ].sup.1/2 as measured by Small method and adding a second solvent to the resulting kneaded product so that the mixed organic solvent in the magnetic paint has a solubility parameter of lower than 9.5[cal.multidot.cm.sup.-3 ].sup.1/2 to thereby disperse the magnetic layer forming component in the organic solvent.
    • 一种制造磁记录介质的方法的改进,包括用包含含有铁磁粉末的磁性层形成组分和分散在有机溶剂中的树脂组分的磁性涂料涂覆非磁性载体并干燥涂层。 改进在于磁性涂料的制备。 在此改进中,磁性涂料是通过将所述磁性层形成组分和溶解度参数不低于9.5 [cal.xcm-3] 1/2的第一种溶剂进行捏合而获得的,通过Small法测量,并将第二溶剂加入到 得到的混炼物,使得磁性涂料中的混合有机溶剂的溶解度参数低于9.5 [calxcm-3] 1/2,从而将磁性层形成组分分散在有机溶剂中。
    • 10. 发明授权
    • Method for producing a magnetic recording medium
    • 磁记录介质的制造方法
    • US5032428A
    • 1991-07-16
    • US512228
    • 1990-04-20
    • Hiroshi OgawaShinji SaitoHitoshi Noguchi
    • Hiroshi OgawaShinji SaitoHitoshi Noguchi
    • G11B5/84B05D1/26B05D1/28G11B5/71G11B5/716G11B5/842
    • G11B5/716G11B5/71Y10S428/90
    • A method for producing a magnetic recording medium is disclosed, comprising coating on a nonmagnetic support a magnetic coating composition for forming a lower magnetic layer and a magnetic coating composition for forming an upper magnetic layer using a wet-on-wet coating method, thereby forming plural magnetic layers, followed by drying, and then conducting heat treatment thereof, wherein the magnetic coating composition for the upper magnetic layer contains ferromagnetic alloy particles are ferromagnetic particles and does not contain a lubricating agent which has polar groups and has a molecular weight of 3000 or less, the magnetic coating composition for the lower magnetic layer contains ferromagnetic iron oxide particles as ferromagnetic particles, a lubricating agent having polar groups and having a molecular weight of 3000 or less, and a curing agent, the lubricating agent as well as the curing agent in the lower magnetic layer being diffused into the upper magnetic layer by the heat treatment.
    • 公开了一种制造磁记录介质的方法,其包括在非磁性载体上涂覆用于形成下磁性层的磁性涂料组合物和使用湿式湿式涂布法形成上层磁性层的磁性涂料组合物,由此形成 多个磁性层,然后干燥,然后进行热处理,其中包含铁磁性合金颗粒的上磁性层的磁性涂层组合物是铁磁性颗粒,并且不含有具有极性基团并且分子量为3000的润滑剂 以下的磁性涂料组合物含有作为铁磁性粒子的铁磁性氧化铁粒子,具有极性基团且分子量为3000以下的润滑剂,固化剂,润滑剂以及固化物 下磁性层中的试剂通过该磁性层扩散到上磁性层中 热处理。