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1. 发明授权

US06174852B1 High-density powdered detergent composition 失效
标题翻译：高密度粉末洗涤剂组合物
公开(公告)号：US06174852B1
公开(公告)日：2001-01-16
申请号：US09117026
申请日：1998-07-22
申请人： Hiromitsu Hayashi , Toshiharu Noguchi , Masaki Tsumadori , Masaaki Yamamura , Noboru Moriyama
发明人： Hiromitsu Hayashi , Toshiharu Noguchi , Masaki Tsumadori , Masaaki Yamamura , Noboru Moriyama
IPC分类号： C11D326
CPC分类号： C11D1/83 , C11D1/04 , C11D1/146 , C11D1/22 , C11D1/28 , C11D1/72 , C11D3/128 , C11D3/33 , C11D17/065
摘要： A high-density powdered detergent composition which has a bulk density of 0.6 to 1.2 g/ml and which comprises 0.5 to 30% by weight of (a) a glycine-N,N-diacetic acid derivative, 20 to 50% by weight of (b) an anionic surfactant, 0.5 to 5% by weight of (c) an ether-type nonionic surfactant having an HLB value of 10.5 to 15.0 and 1 to 30% by weight of (d) an aluminosilcate, each percentage being based on the total weight of the composition, and the component (c) being contained in an amount of 0.5 to 10.0 parts by weight per 100 parts by weight of the component (b). This composition contains both a glycine-N,N-diacetic acid derivative which is a builder excellent in biodegradability and sequestering power and an inorganic builder such as zeolite or crystalline silicate, and exhibits high detergency.
摘要翻译：一种高密度粉末状洗涤剂组合物，其堆密度为0.6〜1.2g / ml，含有0.5〜30重量％的（a）甘氨酸-N，N-二乙酸衍生物，20〜50重量％（b）阴离子表面活性剂，0.5〜5重量％的（c）HLB值为10.5〜15.0的醚型非离子表面活性剂和1〜30重量％的（d）铝硅酸盐，每个百分比基于组合物的总重量和组分（c）的含量为每100重量份组分（b）0.5至10.0重量份。该组合物含有作为生物降解性和螯合能力优异的助洗剂的甘氨酸-N，N-二乙酸衍生物和沸石或结晶性硅酸盐等无机助洗剂，并且显示出高洗涤性。

2. 发明授权

US06211141B1 High-density powdered detergent composition 失效
标题翻译：高密度粉末洗涤剂组合物
公开(公告)号：US06211141B1
公开(公告)日：2001-04-03
申请号：US09101510
申请日：1998-07-13
申请人： Shu Yamaguchi , Hiromitsu Hayashi , Masaki Tsumadori , Masaaki Yamamura , Noboru Moriyama
发明人： Shu Yamaguchi , Hiromitsu Hayashi , Masaki Tsumadori , Masaaki Yamamura , Noboru Moriyama
IPC分类号： C11D183
CPC分类号： C11D17/065 , C11D1/04 , C11D1/146 , C11D1/22 , C11D1/72 , C11D1/83 , C11D3/128 , C11D3/33
摘要： A high-density powdered detergent composition which has a bulk density of 0.6 to 1.2 g/ml and which comprises 0.5 to 30% by weight of (a) a glycine-N,N-diacetic acid derivative, 5 to 45% by weight of (b) a nonionic surfactant having an HLB value of 10.5 to 15.0, 0.5 to 18% by weight of (c) an anionic surfactant and 1 to 30% by weight of (d) an aluminosilicate, each percentage being based on the total weight of the composition, and the weight ratio of the component (b) to the component (c) lying between 90:1 and 60:40. This composition contains both a glycine-N,N-diacetic acid derivative which is a builder excellent in biodegradability and sequestering power and an inorganic builder such as zeolite or crystalline silicate, and exhibits high detergency.
摘要翻译：一种高密度粉末状洗涤剂组合物，其堆积密度为0.6〜1.2g / ml，含有0.5〜30重量％的（a）甘氨酸-N，N-二乙酸衍生物，5〜45重量％（b）HLB值为10.5〜15.0，0.5〜18重量％（c）阴离子表面活性剂和1〜30重量％（d）铝硅酸盐的非离子性表面活性剂，各自以总重量计的组分，和组分（b）与组分（c）的重量比在90:1和60:40之间。该组合物含有作为生物降解性和螯合能力优异的助洗剂的甘氨酸-N，N-二乙酸衍生物和沸石或结晶性硅酸盐等无机助洗剂，并且显示出高洗涤性。

3. 发明授权

US5980580A Washing method and detergent compositions 失效
标题翻译：洗涤方法和洗涤剂组合物
公开(公告)号：US5980580A
公开(公告)日：1999-11-09
申请号：US817999
申请日：1997-05-01
申请人： Shu Yamaguchi , Katsuhiko Kasai , Yoko Yamaguchi , Shigeru Tamura , Masaki Tsumadori , Hiroyuki Yamashita
发明人： Shu Yamaguchi , Katsuhiko Kasai , Yoko Yamaguchi , Shigeru Tamura , Masaki Tsumadori , Hiroyuki Yamashita
IPC分类号： C11D3/08 , C11D3/10 , C11D3/12 , C11D11/00 , C11D17/00 , D06L1/16
CPC分类号： C11D3/08 , C11D11/0017 , C11D17/0039 , C11D3/10 , C11D3/126
摘要： A washing method characterized in that washing is carried out under conditions that a pH of a washing liquid starts increasing after a water hardness of the washing liquid starts decreasing; a detergent composition characterized by containing particles capable of delayed-exerting an alkalizing effect of a washing liquid, wherein a pH of a washing liquid starts increasing after a water hardness of the washing liquid starts decreasing; and a detergent composition comprising an alkalizing agent coated with an organic material, or organic and inorganic materials, the alkalizing agent occupying an amount of 70% by weight or more of the entire alkalizing agents in the detergent composition. In the washing method and the detergent composition of the present invention, since washing is carried out under conditions that a pH of a washing liquid starts increasing after a water hardness of the washing liquid starts decreasing, excellent detergency can be achieved even at a low surfactant concentration in a washing liquid.
摘要翻译： PCT No.PCT / JP96 / 02485第 371日期1997年5月1日 102（e）日期1997年5月1日PCT PCT 1996年9月2日PCT公布。公开号WO97 / 09414 日期1997年3月13日一种洗涤方法，其特征在于，在洗涤液的水硬度开始下降后，洗涤液的pH开始增加的条件下进行洗涤; 一种洗涤剂组合物，其特征在于含有能够延迟施用洗涤液的碱化效果的颗粒，其中在洗涤液的水硬度开始降低之后，洗涤液的pH开始增加; 以及包含涂覆有机材料的碱化剂或有机和无机材料的洗涤剂组合物，所述碱化剂占所述洗涤剂组合物中的全部碱化剂的70重量％以上。在本发明的洗涤方法和洗涤剂组合物中，由于在洗涤液的水硬度开始下降后，在洗涤液的pH开始增加的条件下进行洗涤，即使在低表面活性剂在洗涤液中的浓度。

4. 再颁专利

USRE38411E1 Washing method and clothes detergent composition 有权
标题翻译：洗涤方法和衣物洗涤剂组成
公开(公告)号：USRE38411E1
公开(公告)日：2004-02-03
申请号：US09970688
申请日：2001-10-05
申请人： Shu Yamaguchi , Noriaki Ushio , Akiko Ishikura , Katsuhiko Kasai , Masaki Tsumadori , Hiroyuki Yamashita
发明人： Shu Yamaguchi , Noriaki Ushio , Akiko Ishikura , Katsuhiko Kasai , Masaki Tsumadori , Hiroyuki Yamashita
IPC分类号： C11D308
CPC分类号： C11D3/128 , C11D3/126 , C11D3/1273 , C11D3/33 , C11D3/361 , C11D3/364 , C11D3/365 , C11D3/3761 , C11D11/0017
摘要： A washing method is described which has excellent washing power and a low surfactant concentration. The described clothes washing method comprises the use of a phosphorus-free clothes detergent composition comprising (a) one or more surfactants, (b) one or more alkali metal silicates, and (c) one or more metal ion capturing agents other than the alkali metal silicate (b). The above detergent composition is added to water in an amount sufficient to produce a washing liquid having the following washing conditions (1) a pH of not less than 10.60; (2) containing a material having an ion capturing capacity in an amount sufficient for theoretically changing the water hardness of said water to be not more than 0.5° DH; and (3) having a surfactant concentration of from 0.07 to 0.17 g/L.

5. 发明授权

US5013485A Liquid detergent composition containing terpene and calcium or magnesium salts 失效
标题翻译：含有萜烯和钙或镁盐的液体洗涤剂组合物
公开(公告)号：US5013485A
公开(公告)日：1991-05-07
申请号：US373278
申请日：1989-06-28
申请人： Kazunori Tsukuda , Masakazu Toda , Masami Saito , Masaki Tsumadori
发明人： Kazunori Tsukuda , Masakazu Toda , Masami Saito , Masaki Tsumadori
IPC分类号： C11D3/43 , C11D3/02 , C11D3/18 , C11D3/60
CPC分类号： C11D3/046 , C11D3/18
摘要： A liquid detergent composition for household use is disclosed. It comprises, as essential components, (A) 0.01-1.0% by weight of an anionic surface active agent, (B) 0.01-1.0% by weight of a terpene-type hydrocarbon solvent selected from monoterpenes and sesquiterpenes, and (C) 0.001-0.1% by weight of a water-soluble divalent metallic salt. The composition has superior detergency, exhibits a minimum adverse effect on surfaces which it contacts and a high degree of safety when in contact with the human body, and does not require rinsing.
摘要翻译：公开了一种家用液体洗涤剂组合物。作为必需成分，以（A）0.01〜1.0重量％的阴离子表面活性剂，（B）0.01〜1.0重量％的选自单萜烯和倍半萜烯的萜烯型烃溶剂，（C）0.001 -0.1重量％的水溶性二价金属盐。该组合物具有优异的去污力，对与其接触的表面具有最小的不利影响，并且在与人体接触时具有高度的安全性，并且不需要漂洗。

6. 发明授权

US6114297A Detergent composition for clothing 有权
标题翻译：衣物洗涤剂组成
公开(公告)号：US6114297A
公开(公告)日：2000-09-05
申请号：US142433
申请日：1998-09-09
申请人： Shu Yamaguchi , Hitoshi Tanimoto , Masaki Tsumadori
发明人： Shu Yamaguchi , Hitoshi Tanimoto , Masaki Tsumadori
IPC分类号： C11D1/14 , C11D1/22 , C11D1/37 , C11D1/66 , C11D1/83 , C11D3/08 , C11D3/12 , C11D17/06 , C11D17/00
CPC分类号： C11D1/37 , C11D1/83 , C11D17/065 , C11D3/08 , C11D3/1273 , C11D1/146 , C11D1/22 , C11D1/66
摘要： The detergent composition for clothes washing includes (I) surfactant components including:A) one or more sulfonate-type anionic surfactants; and B) at least one of nonionic surfactants and sulfate-type anionic surfactants, wherein a weight ratio of Component B to Component A is B/A=1/10 to 2/1; and(II) components including:C) one or more alkali metal silicates; and D) one or more metal ion capturing agents other than component C), wherein a weight ratio of Component C to Component D is C/D=1/15 to 5/1. Here, a total amount of the components (I) is from 20 to 50% by weight, and a total amount of the components (II) is from 30 to 80% by weight, and the detergent composition has a bulk density of 0.6 g/cc or more.
摘要翻译： PCT No.PCT / JP97 / 00750 Sec。 371 1998年9月9日第 102（e）1998年9月9日PCT 1997年3月10日PCT公布。公开号WO97 / 33969 日本1997年9月18日洗涤用洗涤剂组合物包括（I）表面活性剂组分，包括：A）一种或多种磺酸盐型阴离子表面活性剂; 和B）至少一种非离子表面活性剂和硫酸盐型阴离子表面活性剂，其中组分B与组分A的重量比为B / A = 1/10〜2/1; 和（II）组分，包括：C）一种或多种碱金属硅酸盐; 和D）组分C）以外的一种或多种金属离子捕获剂，其中组分C与组分D的重量比为C / D = 1/15〜5/1。这里，组分（I）的总量为20至50重量％，组分（II）的总量为30至80重量％，洗涤剂组合物的堆积密度为0.6g / cc或更多。

7. 发明授权

US5961662A Washing method and clothes detergent composition 失效
标题翻译：洗涤方法和衣物洗涤剂组成
公开(公告)号：US5961662A
公开(公告)日：1999-10-05
申请号：US793870
申请日：1997-03-11
申请人： Shu Yamaguchi , Noriaki Ushio , Akiko Ishikura , Katsuhiko Kasai , Masaki Tsumadori , Hiroyuki Yamashita
发明人： Shu Yamaguchi , Noriaki Ushio , Akiko Ishikura , Katsuhiko Kasai , Masaki Tsumadori , Hiroyuki Yamashita
IPC分类号： C11D3/08 , C11D3/12 , C11D3/33 , C11D3/36 , C11D3/37
CPC分类号： C11D3/365 , C11D3/08 , C11D3/126 , C11D3/1273 , C11D3/128 , C11D3/33 , C11D3/361 , C11D3/364 , C11D3/3761
摘要： A washing method is described which has excellent washing power and a low surfactant concentration. The described clothes washing method comprises the use of a phosphorus-free clothes detergent composition comprising (a) one or more surfactants, (b) one or more alkali metal silicates, and (c) one or more metal ion capturing agents other than the alkali metal silicate (b). The above detergent composition is added to water in an amount sufficient to produce a washing liquid having the following washing conditions (1) a pH of not less than 10.60; (2) containing a material having an ion capturing capacity in an amount sufficient for theoretically changing the water hardness of said water to be not more than 0.5.degree. DH; and (3) having a surfactant concentration of from 0.07 to 0.17 g/L.
摘要翻译： PCT No.PCT / JP95 / 01750 Sec。 371日期1997年3月10日 102（e）1997年3月10日PCT PCT 1995年9月1日PCT公布。公开号WO96 / 08552 日期：1996年3月21日描述了具有优异洗涤力和低表面活性剂浓度的洗涤方法。所描述的衣物洗涤方法包括使用无磷衣物洗涤剂组合物，其包含（a）一种或多种表面活性剂，（b）一种或多种碱金属硅酸盐，和（c）除碱之外的一种或多种金属离子捕获剂金属硅酸盐（b）。将上述洗涤剂组合物以足以产生具有以下洗涤条件的洗涤液的量加入到水中（1）pH不小于10.60; （2）含有足以使所述水的理论上将所述水的硬度变化为0.5℃以下的离子捕捉能力的材料; 和（3）表面活性剂浓度为0.07至0.17g / L。

8. 发明授权

US06214787B1 Granular detergent composition for clothing 有权
标题翻译：颗粒洗涤剂组合物为服装
公开(公告)号：US06214787B1
公开(公告)日：2001-04-10
申请号：US09142555
申请日：1998-09-11
申请人： Shu Yamaguchi , Shigeru Tamura , Futoshi Teranishi , Noriaki Ushio , Masaki Tsumadori , Hiroyuki Yamashita
发明人： Shu Yamaguchi , Shigeru Tamura , Futoshi Teranishi , Noriaki Ushio , Masaki Tsumadori , Hiroyuki Yamashita
IPC分类号： C11D308
CPC分类号： C11D3/046 , C11D3/08 , C11D3/1273 , C11D17/065
摘要： The granular detergent composition for clothes washing including a surfactant, a metal ion capturing agent, a crystalline alkali metal silicate, and an acidic ingredient, wherein the granular detergent composition includes at least two different granules: a first granule containing the crystalline alkali metal silicate, and a second granule, which is an acidic granule, containing the acidic ingredient. In the granular detergent composition, the crystalline alkali metal silicate and the acidic ingredient are being present in different granules, and the granular detergent composition shows alkaline property in distilled water at 25° C. and has a bulk density of 650 g/L or more. Since each of an acidic ingredient and a crystalline alkali metal silicate is included in a different granule, the initial rise in the pH at initial washing can be adjusted, so that a further improved detergency against the sebum dirt stains is exhibited.
摘要翻译：包含表面活性剂，金属离子捕获剂，结晶性碱金属硅酸盐和酸性成分的衣物用洗涤剂组合物，其中所述颗粒状洗涤剂组合物包含至少两种不同的颗粒：含有结晶性碱金属硅酸盐的第一颗粒，和含有酸性成分的酸性颗粒的第二颗粒。在颗粒状洗涤剂组合物中，结晶性碱金属硅酸盐和酸性成分存在于不同的颗粒中，粒状洗涤剂组合物在25℃的蒸馏水中显示碱性，堆积密度为650g / L以上由于酸性成分和结晶性碱金属硅酸盐中的每一种都包含在不同的颗粒中，因此可以调节初始洗涤时的pH的初始上升，从而显示出对皮脂污垢的去污力的进一步改善。

9. 发明授权

US6159919A Bleaching detergent composition 失效
标题翻译：漂白洗涤剂组合物
公开(公告)号：US6159919A
公开(公告)日：2000-12-12
申请号：US633698
申请日：1996-04-19
申请人： Shu Yamaguchi , Nobuyosi Yamaguchi , Muneo Aoyagi , Noriaki Ushio , Shigeru Tamura , Masaki Tsumadori
发明人： Shu Yamaguchi , Nobuyosi Yamaguchi , Muneo Aoyagi , Noriaki Ushio , Shigeru Tamura , Masaki Tsumadori
IPC分类号： C11D3/12 , C11D3/39 , C11D3/395
CPC分类号： C11D3/3907 , C11D3/1246 , C11D3/3942
摘要： The bleaching detergent composition in a form of granules or powders containing an organic peracid precursor which produces an organic peracid upon reaction with hydrogen peroxide in water, the organic peracid having an alkyl group with 7 to 19 carbon atoms, and a hydrogen peroxide releasing material, wherein the bleaching detergent composition comprises the following components a) to c): a) one or more surfactants; b) one or more crystalline alkali metal silicates; and c) one or more agents for capturing metal ions other than the crystalline alkali metal silicates b), wherein a total amount of the above a), b), and c) components in the bleaching detergent composition occupies from 70 to 99% by weight, and wherein the weight ratio of component b) to component a) is b/a=90/10 to 45/55, and the weight ratio of component b) to component c) is b/c=7/93 to 75/25, and wherein the weight ratio of the organic peracid precursor to nonionic surfactants used as component a) is from 10/90 to 70/30.
摘要翻译：漂白洗涤剂组合物为颗粒或粉末形式，其含有有机过酸前体，其与水中的过氧化氢反应产生有机过酸，具有7至19个碳原子的烷基的有机过酸和过氧化氢释放物质，其中所述漂白洗涤剂组合物包含以下组分a）至c）：a）一种或多种表面活性剂; b）一种或多种结晶碱金属硅酸盐; 和c）一种或多种用于捕获除结晶性碱金属硅酸盐b）之外的金属离子的试剂，其中漂白洗涤剂组合物中上述a），b）和c）组分的总量占70-99％成分b）与成分a）的重量比为b / a = 90/10〜45/55，成分b）与成分c）的重量比为b / c = 7/93〜75 / 25，其中有机过酸前体与用作组分a）的非离子表面活性剂的重量比为10/90至70/30。

10. 发明授权

US5545349A Bleaching composition 失效
标题翻译：漂白成分
公开(公告)号：US5545349A
公开(公告)日：1996-08-13
申请号：US210418
申请日：1994-03-18
申请人： Jun Kurii , Noboru Nomura , Masami Itoh , Kozo Ohira , Masaki Tsumadori , Akira Matsunaga , Akio Kimura , Shigetoshi Suzue
发明人： Jun Kurii , Noboru Nomura , Masami Itoh , Kozo Ohira , Masaki Tsumadori , Akira Matsunaga , Akio Kimura , Shigetoshi Suzue
IPC分类号： C11D3/39 , C09K3/00 , C01B15/10
CPC分类号： C11D3/391
摘要： A bleaching composition comprising:(a) Hydrogen peroxide or peroxide that produces hydrogen peroxide in aqueous solution; and(b) An organic acid peroxide precursor that produces organic acid peroxide by reacting with said hydrogen peroxide or peroxide that produces hydrogen peroxide in aqueous solution, wherein said organic acid peroxide is represented by general formula (I): ##STR1## wherein R.sup.1 represents a straight chain or branched chain alkyl or alkenyl group having 1-5 carbon atoms, R.sup.2 represents a straight chain or branched chain alkylene group having 1-8 carbon atoms or a phenylene group that may be substituted with a straight chain or branched chain alkyl group having 1-5 carbon atoms, A represent identical or different alkylene groups having from 2 to 4 carbon atoms, and n represents an integer from 0-100.
摘要翻译：一种漂白组合物，其包含：（a）在水溶液中产生过氧化氢的过氧化氢或过氧化物; （b）通过与在水溶液中产生过氧化氢的所述过氧化氢或过氧化物反应产生有机过氧化氢的有机过氧化氢前体，其中所述有机过氧化物由通式（I）表示：其中R1表示具有1-5个碳原子的直链或支链烷基或烯基，R2表示具有1-8个碳原子的直链或支链亚烷基或可以被直链或支链取代的亚苯基具有1-5个碳原子的链烷基，A表示具有2至4个碳原子的相同或不同的亚烷基，n表示0-100的整数。

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