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1. 发明授权

US07462228B2 Water-base black ink composition and colored product 有权
标题翻译：水性黑色油墨组合物和有色产品
公开(公告)号：US07462228B2
公开(公告)日：2008-12-09
申请号：US10547850
申请日：2004-03-04
申请人： Hiroaki Ohno , Toru Yamaguchi , Takahiko Matsui , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki , Kazunobu Nagasaki
发明人： Hiroaki Ohno , Toru Yamaguchi , Takahiko Matsui , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki , Kazunobu Nagasaki
IPC分类号： C09D11/00 , C09D11/02 , C09B31/30
CPC分类号： C09D11/32 , C09B33/28 , C09D11/38
摘要： The present invention relates to a water-based black ink composition comprising a water-soluble black dye (A) exhibiting ozone fastness and a condensate compound (B) of 4,4′-dinitrostilbene-2,2′-disulfonic acid and aminobenzenes or a reduction product (C) thereof. Said ink composition is suitable for use in ink-jet recording, and realizes neutral hue and black color of high printing density. Further, a printed matter obtained is excellent in ozone gas fastness, light fastness, moisture fastness and color rendering properties. Still further, storage stability as a recording liquid is excellent.
摘要翻译：本发明涉及一种水性黑色油墨组合物，其包含显示出耐臭氧性的水溶性黑色染料（A）和4,4'-二硝基茋-2,2'-二磺酸和氨基苯的缩合物（B）或还原产物（C）。所述油墨组合物适用于喷墨记录，并实现高印刷密度的中性色调和黑色。此外，得到的印刷品的臭氧气体牢度，耐光性，耐湿牢度和显色性优异。此外，作为记录液体的储存稳定性优异。

2. 发明申请

US20060144288A1 Water-base black ink composition and colored material 有权
标题翻译：水底黑色油墨组合物和着色材料
公开(公告)号：US20060144288A1
公开(公告)日：2006-07-06
申请号：US10547850
申请日：2004-03-04
申请人： Hiroaki Ohno , Toru Yamaguchi , Takahiko Matsui , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki , Kazunobu Nagasaki
发明人： Hiroaki Ohno , Toru Yamaguchi , Takahiko Matsui , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki , Kazunobu Nagasaki
IPC分类号： C09D11/00 , C09B33/18 , C07C245/02
CPC分类号： C09D11/32 , C09B33/28 , C09D11/38
摘要： The present invention relates to a water-based black ink composition comprising a water-soluble black dye (A) exhibiting ozone fastness and a condensate compound (B) of 4,4′-dinitrostilbene-2,2′-disulfonic acid and aminobenzenes or a reduction product (C) thereof. Said ink composition is suitable for use in ink-jet recording, and realizes neutral hue and black color of high printing density. Further, a printed matter obtained is excellent in ozone gas fastness, light fastness, moisture fastness and color rendering properties. Still further, storage stability as a recording liquid is excellent.
摘要翻译：本发明涉及一种水性黑色油墨组合物，其包含显示出耐臭氧性的水溶性黑色染料（A）和4,4'-二硝基茋-2,2'-二磺酸和氨基苯的缩合物（B）或还原产物（C）。所述油墨组合物适用于喷墨记录，并实现高印刷密度的中性色调和黑色。此外，得到的印刷品的臭氧气体牢度，耐光性，耐湿牢度和显色性优异。此外，作为记录液体的储存稳定性优异。

3. 发明授权

US07326288B2 Trisazo compound, ink composition, and colored object 失效
标题翻译：三唑烷化合物，油墨组合物和有色物体
公开(公告)号：US07326288B2
公开(公告)日：2008-02-05
申请号：US10581469
申请日：2004-11-26
申请人： Takahiko Matsui , Hiroaki Ohno , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki
发明人： Takahiko Matsui , Hiroaki Ohno , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki
IPC分类号： C09D11/00 , C09D11/02 , C09B31/16 , B41J2/01
CPC分类号： C09D11/328 , C09B33/22
摘要： [PROBLEMS] To provide: a black compound which is for use in ink-jet recording or writing utensils, is excellent in ozone resistance, light resistance, moisture resistance, and color rendering, and gives a recording fluid having satisfactory storage stability; and an ink composition containing the compound. [MEANS FOR SOLVING PROBLEMS] The black compound is a trisazo compound represented by the following formula (1) or a salt thereof. (1) [In the formula (1), R1 and R2 each independently represents hydrogen, carboxy, sulfo, hydroxy, a C1-4 alkyl, C1-4 alkoxy, or sulfo group optionally substituted by C1-4 alkoxy, an optionally carboxylated C1-4 alkoxy group, etc.; and A represents phenyl or naphthyl (provided that the phenyl and naphthyl groups may be substituted by halogeno, carboxy, sulfo, sulfamonyl optionally substituted by alkyl or phenyl, nitro, etc.).]
摘要翻译：提供：用于喷墨记录或书写用具的黑色化合物，具有优异的耐臭氧性，耐光性，耐湿性和显色性，并且得到具有令人满意的储存稳定性的记录液; 和含有该化合物的油墨组合物。解决问题的方法黑色化合物是由下式（1）表示的三偶氮化合物或其盐。（1）[式（1）中，R 1和R 2各自独立地表示氢，羧基，磺基，羟基，C 1-4烷基， C 1-4烷氧基或任选被C 1-4烷氧基取代的磺基，任选羧基化的C 1-4烷基烷氧基等。并且A表示苯基或萘基（条件是苯基和萘基可以被卤素，羧基，磺基，任选被烷基或苯基，硝基等取代的磺酰氨基取代）。

4. 发明申请

US20070227388A1 Tetrakisazo Compound, Coloring Matter for Recording, Ink Composition and Colored Article 审中-公开
标题翻译：四氮唑化合物，着色剂用于记录，油墨组合物和彩色制品
公开(公告)号：US20070227388A1
公开(公告)日：2007-10-04
申请号：US11579289
申请日：2005-05-09
申请人： Hiroaki Ohno , Takahiko Matsui , Takashi Yoneda , Yasuo Shirasaki , Yoshiaki Kawaida
发明人： Hiroaki Ohno , Takahiko Matsui , Takashi Yoneda , Yasuo Shirasaki , Yoshiaki Kawaida
IPC分类号： C09B31/02 , B41M3/00 , C09D11/00
CPC分类号： C09B33/28 , C09D11/322
摘要： The present invention relates to black coloring matter, and relates to a compound represented by the following formula (1): (wherein A and D independently represent an optionally substituted phenyl group or naphthyl group, respectively, and m and n represent 1 or 2, respectively), and the coloring matter for recording and an ink comprising the same. Said compound exhibits high solubility in a medium containing water as a main component, is stable even when an aqueous dye solution or an ink having a high concentration is prepared therefrom and is stored for a long period of time, has low color rendering property, exhibits colorless and neutral black, provides a printed image having high density and also provides a black recorded image being excellent in moisture fastness, light fastness and an ozone gas fastness, and further can be synthesized easily and can be produced at a low cost.
摘要翻译：本发明涉及黑色色素，涉及由下式（1）表示的化合物：其中A和D分别独立地表示任选取代的苯基或萘基，m和n表示1或2，分别）和用于记录的着色剂和包含其的油墨。所述化合物在以水为主要成分的介质中表现出高溶解度，即使制备高浓度的水性染料溶液或长时间储存的色素溶液或显色性低，也是稳定的无色和中性黑色，提供了高密度的印刷图像，并且还提供了耐湿牢度，耐光性和耐臭氧气体牢度优异的黑色记录图像，并且还可以容易地合成并且可以以低成本制造。

5. 发明申请

US20070107628A1 Trisazo compound, ink composition, and colored object 失效
标题翻译：三唑烷化合物，油墨组合物和有色物体
公开(公告)号：US20070107628A1
公开(公告)日：2007-05-17
申请号：US10581469
申请日：2004-11-26
申请人： Takahiko Matsui , Hiroaki Ohno , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki
发明人： Takahiko Matsui , Hiroaki Ohno , Takashi Yoneda , Yoshiaki Kawaida , Yasuo Shirasaki
IPC分类号： C09D11/00 , C09D11/02 , C07C245/02
CPC分类号： C09D11/328 , C09B33/22
摘要： [PROBLEMS] To provide: a black compound which is for use in ink-jet recording or writing utensils, is excellent in ozone resistance, light resistance, moisture resistance, and color rendering, and gives a recording fluid having satisfactory storage stability; and an ink composition containing the compound. [MEANS FOR SOLVING PROBLEMS] The black compound is a trisazo compound represented by the following formula (1) or a salt thereof. (1) [In the formula (1), R1 and R2 each independently represents hydrogen, carboxy, sulfo, hydroxy, a C1-4 alkyl, C1-4 alkoxy, or sulfo group optionally substituted by C1-4 alkoxy, an optionally carboxylated C1-4 alkoxy group, etc.; and A represents phenyl or naphthyl (provided that the phenyl and naphthyl groups may be substituted by halogeno, carboxy, sulfo, sulfamonyl optionally substituted by alkyl or phenyl, nitro, etc.).]
摘要翻译：提供：用于喷墨记录或书写用具的黑色化合物，具有优异的耐臭氧性，耐光性，耐湿性和显色性，并且得到具有令人满意的储存稳定性的记录液; 和含有该化合物的油墨组合物。解决问题的方法黑色化合物是由下式（1）表示的三偶氮化合物或其盐。（1）[式（1）中，R 1和R 2各自独立地表示氢，羧基，磺基，羟基，C 1-4烷基， C 1-4烷氧基或任选被C 1-4烷氧基取代的磺基，任选羧基化的C 1-4烷基烷氧基等。并且A表示苯基或萘基（条件是苯基和萘基可以被卤素，羧基，磺基，任选被烷基或苯基，硝基等取代的磺酰氨基取代）。

6. 发明申请

US20110050787A1 TRISAZO COMPOUND, INK COMPOSITION, RECORDING METHOD AND COLORED BODY 有权
标题翻译： TRISAZO化合物，墨水组合物，记录方法和着色体
公开(公告)号：US20110050787A1
公开(公告)日：2011-03-03
申请号：US12989784
申请日：2009-04-28
申请人： Takashi Yoshimoto , Yoshiaki Kawaida , Takahiko Matsui
发明人： Takashi Yoshimoto , Yoshiaki Kawaida , Takahiko Matsui
IPC分类号： B41J2/015 , C09B39/00
CPC分类号： B41M5/0023 , C09B31/28 , C09D11/328
摘要： Disclosed is a dye compound for black ink which has high solubility in media composed mainly of water and which is stable even when a high-concentration aqueous solution and ink are stored over a long term. The density of printed images is very high, and even if a high-concentration solution is used for printing, no bronzing occurs in the images, and black recorded images are provided with which all aspects of printed image durability, particularly light resistance and ozone gas resistance, are excellent. Also disclosed is an ink composition thereof. Trisazo compounds represented by general formula (1) or tautomers thereof or salts thereof are used as said dye compound for black ink. In formula (1), group A represents a 2-naphthothiazolyl group, R1 represents a substitutable C1 to C4 alkyl group or the like, R2 represents a cyano group or the like, R3 and R4 independently represent a hydrogen atom, a sulfo group, or the like, R5 to R7 independently represent a hydrogen atom, a substitutable C1 to C4 alkyl group, or a substitutable C1 to C4 alkoxy group, or the like, and R8 to R10 independently represent a hydrogen atom, a substitutable C1 to C4 alkyl group, a substitutable C1 to C4 alkoxy group, a substitutable C1 to C4 alkylthio group, or the like.
摘要翻译：公开了一种黑色油墨用染料化合物，其在主要由水组成的介质中的溶解度高，即使长期储存高浓度水溶液和油墨也是稳定的。印刷图像的浓度非常高，即使使用高浓度溶液进行印刷，也不会在图像中发生烫伤，并且黑色记录图像具有印刷图像耐久性，特别是耐光性和臭氧气体的所有方面阻力很好。还公开了其油墨组合物。作为黑色油墨的染料化合物，使用由通式（1）表示的三唑并
化合物或其互变异构体或其盐。式（1）中，A组表示2-萘并噻唑基，R 1表示可取代的C 1〜C 4烷基等，R 2表示氰基等，R 3和R 4分别表示氢原子， R 5〜R 7独立地表示氢原子，可取代的C 1〜C 4烷基或可取代的C 1至C 4烷氧基等，R 8至R 10独立地表示氢原子，可取代的C 1至C 4烷基基团，可取代的C 1至C 4烷氧基，可取代的C 1至C 4烷硫基等。

7. 发明授权

US08080100B2 Trisazo compound, ink composition, recording method and colored body 有权
标题翻译：三唑类化合物，油墨组合物，记录方法和着色体
公开(公告)号：US08080100B2
公开(公告)日：2011-12-20
申请号：US12989784
申请日：2009-04-28
申请人： Takashi Yoshimoto , Yoshiaki Kawaida , Takahiko Matsui
发明人： Takashi Yoshimoto , Yoshiaki Kawaida , Takahiko Matsui
IPC分类号： C09D11/02 , C09B31/16
CPC分类号： B41M5/0023 , C09B31/28 , C09D11/328
摘要： Disclosed is a dye compound for black ink which has high solubility in media composed mainly of water and which is stable even when a high-concentration aqueous solution and ink are stored over a long term. The density of printed images is very high, and even if a high-concentration solution is used for printing, no bronzing occurs in the images, and black recorded images are provided with which all aspects of printed image durability, particularly light resistance and ozone gas resistance, are excellent. Also disclosed is an ink composition thereof. Trisazo compounds represented by general formula (1) or tautomers thereof or salts thereof are used as said dye compound for black ink. In formula (1), group A represents a 2-naphthothiazolyl group, R1 represents a substitutable C1 to C4 alkyl group or the like, R2 represents a cyano group or the like, R3 and R4 independently represent a hydrogen atom, a sulfo group, or the like, R5 to R7 independently represent a hydrogen atom, a substitutable C1 to C4 alkyl group, or a substitutable C1 to C4 alkoxy group, or the like, and R8 to R10 independently represent a hydrogen atom, a substitutable C1 to C4 alkyl group, a substitutable C1 to C4 alkxy group, a substitutable C1 to C4 alkylthio group, or the like.
摘要翻译：公开了一种黑色油墨用染料化合物，其在主要由水组成的介质中的溶解度高，即使长期储存高浓度水溶液和油墨也是稳定的。印刷图像的浓度非常高，即使使用高浓度溶液进行印刷，也不会在图像中发生烫伤，并且黑色记录图像具有印刷图像耐久性，特别是耐光性和臭氧气体的所有方面阻力很好。还公开了其油墨组合物。作为黑色油墨的染料化合物，使用由通式（1）表示的三唑并
化合物或其互变异构体或其盐。式（1）中，A组表示2-萘并噻唑基，R 1表示可取代的C 1〜C 4烷基等，R 2表示氰基等，R 3和R 4分别表示氢原子， R 5〜R 7独立地表示氢原子，可取代的C 1〜C 4烷基或可取代的C 1至C 4烷氧基等，R 8至R 10独立地表示氢原子，可取代的C 1至C 4烷基基团，可取代的C1至C4烷氧基，可取代的C1-C4烷硫基等。

8. 发明申请

US20090151599A1 Porphyrazine Coloring Matter, Ink, Ink Set and Colored Product 有权
标题翻译：紫菜色素，油墨，油墨和有色产品
公开(公告)号：US20090151599A1
公开(公告)日：2009-06-18
申请号：US12226043
申请日：2007-04-05
申请人： Takafumi Fujii , Takashi Yoneda , Yoshiaki Kawaida , Hiroyuki Tsukui
发明人： Takafumi Fujii , Takashi Yoneda , Yoshiaki Kawaida , Hiroyuki Tsukui
IPC分类号： C09B47/04 , C09B62/016 , C09D11/02 , B05D5/00
CPC分类号： C09B47/00 , C09B47/0675 , C09B47/0678 , C09B47/26 , C09D11/328 , C09D11/40
摘要： The present invention relates to a porphyrazine coloring matter represented by the following formula (1): (wherein, A, B, C and D independently represents a 6-membered ring having aromaticity, at least one or more is a benzene ring, at least one or more contains a nitrogen-containing heteroaromatic ring; in addition, E represents alkylene and each of X and Y independently represents a substituted or unsubstituted anilino group or a substituted or unsubstituted naphthylamino group; and b is 0 to 2.9, c is 0.1 to 3 and the sum of b and c is 1 to 3) which has a good hue as a cyan ink, is excellent in light fastness, ozone fastness and moisture fastness, and does not cause bronze phenomenon, as well as is thus suitable for inkjet recording.
摘要翻译：本发明涉及由下式（1）表示的四氮杂卟啉色素：（其中，A，B，C和D独立地表示具有芳香性的6元环，至少一个或多个为苯环，至少一个或多个含有含氮杂芳环;此外，E表示亚烷基，X和Y各自独立地表示取代或未取代的苯胺基或取代或未取代的萘基氨基; b为0〜2.9，c为0.1〜 3，b和c之和为1〜3）作为青色墨水具有良好的色相，耐光性，耐臭氧性和耐湿牢度优异，不会引起青铜现象，因此适用于喷墨记录。

9. 发明授权

US07854797B2 Porphyrazine coloring matter, ink, ink set, and colored product 有权
标题翻译：紫菜色素，油墨，油墨和彩色产品
公开(公告)号：US07854797B2
公开(公告)日：2010-12-21
申请号：US12450127
申请日：2008-03-13
申请人： Takafumi Fujii , Takashi Yoneda , Yasuo Kuroda , Yoshiaki Kawaida
发明人： Takafumi Fujii , Takashi Yoneda , Yasuo Kuroda , Yoshiaki Kawaida
IPC分类号： C09D11/02 , C07D487/22 , B41J2/01
CPC分类号： C09D11/328 , B41M5/0023 , C07D487/22 , C09B47/26 , C09D11/32
摘要： The present invention relates to a porphyrazine coloring matter represented by the following formula (1) or a salt thereof; wherein, each of the rings A to D independently represents a benzene ring or a 6-membered nitrogen-containing heteroaromatic ring, at least one or more thereof is a benzene ring, at least one of the rest is a nitrogen-containing heteroaromatic ring, E represents alkylene, X is an anilino group having a substituent and the like, Y represents an amino group; a hydroxy group; a mono- or di-alkylamino group or a nitrogen-containing heterocyclic group which may have a substituent, excepting for the combination in which Y is an amino group or a hydroxy group and X is a substituted anilino group, b is 0 to 2.9, c is 0.1 to 3, and the sum of b and c is 1 to 3. According to the present invention, a porphyrazine coloring matter suitable for inkjet recording which has a good hue as a cyan ink, is excellent in light fastness, ozone fastness and moisture fastness, and causes no bronze phenomenon can be provided.
摘要翻译：本发明涉及由下式（1）表示的四氮杂卟啉色素或其盐; 其中，环A至D各自独立地表示苯环或6元含氮杂芳环，其中至少一个为苯环，其余至少一个为含氮杂芳环， E表示亚烷基，X表示具有取代基的苯胺基等，Y表示氨基。羟基; 除了Y为氨基或羟基，X为取代苯胺基的组合外，b为0〜2.9，可以具有取代基的单 - 或二 - 烷基氨基或含氮杂环基， c为0.1〜3，b和c之和为1〜3。根据本发明，适用于具有良好色调的青色墨水的喷墨记录用四氮杂卟啉色素具有优异的耐光性，耐臭氧性并具有耐湿牢度，并且不会产生青铜现象。

10. 发明申请

US20100112218A1 NOVEL PORPHYRAZINE COLORING MATTER, INK, INK SET, AND COLORED PRODUCT 有权
标题翻译：新颖的PORPHYRAZINE COLORING MATTER，INK，INK SET和COLORED PRODUCT
公开(公告)号：US20100112218A1
公开(公告)日：2010-05-06
申请号：US12450127
申请日：2008-03-13
申请人： Takafumi Fujii , Takashi Yoneda , Yasuo Kuroda , Yoshiaki Kawaida
发明人： Takafumi Fujii , Takashi Yoneda , Yasuo Kuroda , Yoshiaki Kawaida
IPC分类号： C09B67/50 , B05D5/00 , C09D11/02 , C09B47/04
CPC分类号： C09D11/328 , B41M5/0023 , C07D487/22 , C09B47/26 , C09D11/32
摘要： The present invention relates to a porphyrazine coloring matter represented by the following formula (1) or a salt thereof; (wherein, each of the rings A to D independently represents a benzene ring or a 6-membered nitrogen-containing heteroaromatic ring, at least one or more thereof is a benzene ring, at least one of the rest is a nitrogen-containing heteroaromatic ring, E represents alkylene, X is an anilino group having a substituent and the like, Y represents an amino group; a hydroxy group; a mono- or di-alkylamino group or a nitrogen-containing heterocyclic group which may have a substituent, excepting for the combination in which Y is an amino group or a hydroxy group and X is a substituted anilino group, b is 0 to 2.9, c is 0.1 to 3, and the sum of b and c is 1 to 3). According to the present invention, a porphyrazine coloring matter suitable for inkjet recording which has a good hue as a cyan ink, is excellent in light fastness, ozone fastness and moisture fastness, and causes no bronze phenomenon can be provided.
摘要翻译：本发明涉及由下式（1）表示的四氮杂卟啉色素或其盐; （其中，环A至D各自独立地表示苯环或6元含氮杂芳环，其中至少一个或多个为苯环，其余至少一个为含氮杂芳环 E表示亚烷基，X表示具有取代基的苯胺基等，Y表示氨基，羟基，可以具有取代基的单 - 或二 - 烷基氨基或含氮杂环基，除了 Y为氨基或羟基，X为取代苯胺基的组合，b为0〜2.9，c为0.1〜3，b与c的和为1〜3）。根据本发明，适用于喷墨记录的四氮杂卟啉色素具有良好的色相作为青色油墨，耐光性，耐臭氧性和耐湿牢度优异，不会产生青铜现象。

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