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1. 发明授权

US08895675B2 Block copolymer 有权
标题翻译：嵌段共聚物
公开(公告)号：US08895675B2
公开(公告)日：2014-11-25
申请号：US12159143
申请日：2006-12-25
申请人： Daisuke Fukushima , Hideyuki Higashimura , Akihiko Okada , Kazuei Ohuchi , Makoto Anryu
发明人： Daisuke Fukushima , Hideyuki Higashimura , Akihiko Okada , Kazuei Ohuchi , Makoto Anryu
IPC分类号： C08G79/02 , C08G79/08 , C08L53/00 , C08G61/00 , C08G61/10 , C08G61/12 , C09K11/06 , H01L51/00 , H05B33/14 , C08L85/02 , C08L85/04 , C08F283/00
CPC分类号： C08L53/00 , C08G61/00 , C08G61/10 , C08G61/12 , C08G61/124 , C08G61/125 , C08G61/126 , C09K11/06 , C09K2211/14 , H01L51/0026 , H01L51/0035 , H01L51/0036 , H01L51/0037 , H01L51/0039 , H01L51/0043 , H01L2251/308 , H05B33/14 , C08L2666/02
摘要： A block copolymer comprising two or more of blocks of the following formula (1), wherein at least two of a plurality of m's present in the copolymer represent a number of 5 or more, Ar's in adjacent two blocks in the copolymer are mutually different, and the copolymer has two Ar's when composed of 2 blocks of the formula (1), has two or more Ar's when composed of 3 blocks of the formula (1) and has four or more Ar's when composed of 4 or more blocks of the formula (1): (in the formula (1), Ar represents a conjugative divalent group and represents the same divalent group in an identical block, and m represents a number of 1 or more showing the number average polymerization degree of Ar present in one block).
摘要翻译：包含两个或更多个下式（1）的嵌段的嵌段共聚物，其中共聚物中存在的多个m中的至少两个表示5个或更多个，共聚物中相邻的两个嵌段中的Ar相互不同，并且当由2个式（1）的嵌段组成时，该共聚物具有两个Ar，当由3个式（1）的嵌段组成时具有两个或更多个Ar，并且当由4个或更多个式（1）表示（式（1）中，Ar表示共轭二价基，在同一嵌段中表示相同的二价基，m表示一个嵌段中存在Ar的数均聚合度的1以上的数）。

2. 发明申请

US20100219399A1 BLOCK COPOLYMER 有权
标题翻译：嵌段共聚物
公开(公告)号：US20100219399A1
公开(公告)日：2010-09-02
申请号：US12159143
申请日：2006-12-25
申请人： Daisuke Fukushima , Hideyuki Higashimura , Akihiko Okada , Kazuei Ohuchi , Makoto Anryu
发明人： Daisuke Fukushima , Hideyuki Higashimura , Akihiko Okada , Kazuei Ohuchi , Makoto Anryu
IPC分类号： H01L51/54 , C08G79/08 , C08L85/04 , B05D5/00
CPC分类号： C08L53/00 , C08G61/00 , C08G61/10 , C08G61/12 , C08G61/124 , C08G61/125 , C08G61/126 , C09K11/06 , C09K2211/14 , H01L51/0026 , H01L51/0035 , H01L51/0036 , H01L51/0037 , H01L51/0039 , H01L51/0043 , H01L2251/308 , H05B33/14 , C08L2666/02
摘要： A block copolymer comprising two or more of blocks of the following formula (1), wherein at least two of a plurality of m's present in the copolymer represent a number of 5 or more, Ar's in adjacent two blocks in the copolymer are mutually different, and the copolymer has two Ar's when composed of 2 blocks of the formula (1), has two or more Ar's when composed of 3 blocks of the formula (1) and has four or more Ar's when composed of 4 or more blocks of the formula (1): (in the formula (1), Ar represents a conjugative divalent group and represents the same divalent group in an identical block, and m represents a number of 1 or more showing the number average polymerization degree of Ar present in one block.).
摘要翻译：包含两个或更多个下式（1）的嵌段的嵌段共聚物，其中共聚物中存在的多个m中的至少两个表示5个或更多个，共聚物中相邻的两个嵌段中的Ar相互不同，并且当由2个式（1）的嵌段组成时，该共聚物具有两个Ar，当由3个式（1）的嵌段组成时具有两个或更多个Ar，并且当由4个或更多个式（1）表示（式（1）中，Ar表示共轭二价基，在同一嵌段中表示相同的二价基，m表示一个嵌段中存在Ar的数均聚合度的1以上的数。）。

3. 发明申请

US20090045725A1 POLYARYLENE 审中-公开
标题翻译：聚氨酯
公开(公告)号：US20090045725A1
公开(公告)日：2009-02-19
申请号：US11916464
申请日：2006-06-09
申请人： Daisuke Fukushima , Akihiko Okada , Takeshi Yamada , Kazuei Ohuchi , Hideyuki Higashimura , Nozomi Kogure
发明人： Daisuke Fukushima , Akihiko Okada , Takeshi Yamada , Kazuei Ohuchi , Hideyuki Higashimura , Nozomi Kogure
IPC分类号： H01J1/63 , C08G61/04 , C09K11/00 , H01L51/05
CPC分类号： H01L51/0035 , C08G61/02 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , C09K2211/1029 , C09K2211/1033 , C09K2211/1037 , C09K2211/104 , C09K2211/1044 , C09K2211/1048 , C09K2211/1051 , C09K2211/1059 , C09K2211/1088 , C09K2211/1092 , C09K2211/1096 , C09K2211/185 , H01L51/0039 , H01L51/5012
摘要： A high-molecular compound, characterized by containing a chain consisting of repeating units represented by the general formula (1) and having an average number of repeating units constituting the chain of 3 or above and a ratio of bonds formed between the head and the tail to all the bonds formed between repeating units of 85% or above: (1) wherein Ar1 is a divalent aromatic group whose aromatic ring is an aromatic hydrocarbon ring; R1 is a substituent on Ar1; n is an integer of 0 to 30; when n is 2 or above, plural R1's may be the same or different from each other, when the carbon atoms of a repeating unit of the general formula (1) are numbered as a divalent group according to Nomenclature of Organic Chemistry by IUPAC, between the two carbon atoms having free valencies, the carbon atom with a smaller number is defined as the head and the carbon atom with a larger number is defined as the tail; and no repeating unit of the general formula (1) has a two-fold axis of symmetry intersecting the straight line joining the head and the tail at right angles at the middle point.
摘要翻译：一种高分子化合物，其特征在于，含有由通式（1）表示的重复单元构成的链，构成上述3以上链的重复单元的平均数以及头部和尾部之间形成的键的比例对于85重量％以上的重复单元之间形成的全部键;（1）其中Ar1为芳香环为芳香烃环的二价芳香族基团; R1是Ar1上的取代基; n为0〜30的整数，当n为2以上时，当通式（1）的重复单元的碳原子根据IUPAC的有机化学命名法被编号为二价基团时，多个R 1可以相同或不同，在具有自由价的两个碳原子，具有较小数目的碳原子被定义为头部，并且具有较大数量的碳原子被定义为尾部; 并且没有通式（1）的重复单元具有与在中点处以直角连接头部和尾部的直线相交的双重对称轴。

4. 发明申请

US20090099391A1 Novel Aryl Compound 审中-公开
标题翻译：新型芳基化合物
公开(公告)号：US20090099391A1
公开(公告)日：2009-04-16
申请号：US11921796
申请日：2006-06-09
申请人： Kazuei Ohuchi , Hideyuki Higashimura , Daisuke Fukushima
发明人： Kazuei Ohuchi , Hideyuki Higashimura , Daisuke Fukushima
IPC分类号： C07C209/18
CPC分类号： C07F5/025 , C07C211/56
摘要： A novel aryl compound represented by the formula (1) in which the characteristic groups represented by X1 and X2 are different from each other: wherein X1 and X2 are characteristic groups which are different from each other and each of which is selected from the group consisting of a chlorine, bromine or iodine atom, —OSO2Q1, —B(OQ2)2, —Si(OQ3)3, —Sn(Q4)3, Z1 (Z2)m, a metal acetylide group and a terminal acetylene group (where Q represents a hydrocarbon group; Q2 represents a hydrogen atom or a hydrocarbon group; two Q2's may be the same as or different from each other or may together form a ring; Q3 represents a hydrocarbon group and three Q3's may be the same as or different from one another; Q4 represents a hydrocarbon group and three Q4's may be the same as different from one another; Z1 represents a metal atom or a metal ion; Z2 represents a counter anion; and m is an integer of 0 or higher); Ar1 and Ar2 independently represent an arylene group and Ar3 represetns an aryl group, provided that any two of Ar1, Ar2 and Ar3 may be bound to each other via a substituent or directly; Y represents a trivalent atomic group having a nitrogen, carbon, boron or silicon atom to which a hydrogen atom or a hydrocarbon group may be added if required; J represents an arylene group; and n is an integer of 0 or higher; provided that, when each of J, Y and Ar3 is present in the molecule in plural number, they may be the same as or different from each other or one another.
摘要翻译：由式（1）表示的由X1和X2表示的特征基团彼此不同的式（1）表示的新型芳基化合物：其中X1和X2是彼此不同的特征基团，其各自选自的氯，溴或碘原子，-OSO 2 Q 1，-B（OQ 2）2，-Si（OQ 3）3，-Sn（Q 4）3，Z 1（Z 2）m，金属乙炔基和末端乙炔基 Q表示烃基; Q2表示氢原子或烃基;两个Q2可以相同或不同，也可以一起形成环; Q3表示烃基，三个Q3可以相同或不同 Q4表示烃基，3个Q4可以相同，Z1表示金属原子或金属离子，Z2表示抗衡阴离子，m表示0以上的整数）表示的化合物。 Ar1和Ar2独立地表示亚芳基，Ar3表示芳基，只要Ar1，Ar2和Ar3中的任意两个可以通过取代基彼此结合或直接键合; Y表示如果需要，可以加入氢原子或烃基的具有氮原子，碳原子，硼原子或硅原子的三价原子团; J表示亚芳基; n为0以上的整数，条件是，当分子中存在多个数量的J，Y和Ar 3中的每一个时，它们可以彼此相同或不同。

5. 发明授权

US08048982B2 Method for producing aromatic compound polymer 有权
标题翻译：芳香族化合物聚合物的制备方法
公开(公告)号：US08048982B2
公开(公告)日：2011-11-01
申请号：US11571280
申请日：2005-06-24
申请人： Hideyuki Higashimura , Daisuke Fukushima , Kazuei Ohuchi
发明人： Hideyuki Higashimura , Daisuke Fukushima , Kazuei Ohuchi
IPC分类号： C08G65/00 , C08G65/34 , C07F9/00
CPC分类号： C08G61/12 , C07C49/92 , C07F9/005 , C08G61/02 , C08G61/10
摘要： A method for producing an aromatic compound polymer comprising oxidatively polymerizing one or more of aromatic compound(s) having two or more hydrogen atoms directly connected to aromatic ring(s), in the presence of an oxidizing agent, wherein the method employs a catalyst composed of a transition metal complex or a catalyst prepared from a transition metal complex and an activating agent, and said catalyst has a parameter P defined by the following formula (A) of 0.50 or more, and a parameter Eo defined by the following formula (B) of 0.50 [V] or more: P=Af/Ai (A) and Eo=(Epa+Epc)/2 [V] (B).
摘要翻译：一种芳族化合物聚合物的制造方法，其特征在于，在氧化剂的存在下，使直接与芳香环连接的2个以上的氢原子的一种以上的芳香族化合物氧化聚合，的过渡金属络合物或由过渡金属络合物和活化剂制备的催化剂，所述催化剂具有下式（A）定义的参数P为0.50以上，以及由下式（B ）为0.50 [V]以上：P = Af / Ai（A），Eo =（Epa + Epc）/ 2 [V]（B）。

6. 发明申请

US20090209715A1 Process for producing polymer 审中-公开
标题翻译：生产聚合物的方法
公开(公告)号：US20090209715A1
公开(公告)日：2009-08-20
申请号：US11921767
申请日：2006-06-09
申请人： Kazuei Ohuchi , Daisuke Fukushima , Hideyuki Higashimura
发明人： Kazuei Ohuchi , Daisuke Fukushima , Hideyuki Higashimura
IPC分类号： C08F232/00 , C08F226/06 , C08F24/00
CPC分类号： C08G61/125 , C08G73/10 , C09K11/06 , C09K2211/1416 , C09K2211/145 , H01L51/0035 , H01L51/0039 , H01L51/5012 , H05B33/14
摘要： A process for producing a polymer, characterized by comprising the following step (A) and step (B). (A) A step in which a polymer having repeating units represented by the general formula (1): —Ar1— (wherein Ar1 represents an arylene, divalent heterocyclic, or divalent aromatic amine group having at least one C—H bond on the aromatic ring) is used as a raw material and one or more of the C—H bond(s) on the aromatic ring are converted to thereby produce a polymer having repeating units which have one or more characteristic groups X and are represented by the general formula (2): (wherein X represents a characteristic group; Ar2 represents an arylene group, heterocyclic group, or aromatic amine group which each has a valence of n+2 and in each of which n of the C—H bonds on the aromatic ring of Ar1 have been converted into a C—X bond; and n is an integer of 1-4) (hereinafter, this polymer is referred to as polymer having the characteristic group (X)). (B) A step in which the polymer having the characteristic group (X) produced in the step (A) is reacted with a compound having a characteristic group (Y) which reacts with the characteristic group (X) to form a bond.
摘要翻译：一种制备聚合物的方法，其特征在于包括以下步骤（A）和步骤（B）。（A）具有由通式（1）表示的重复单元的聚合物：-Ar1-（其中Ar1表示亚芳基，二价杂环，或芳香环上具有至少一个CH键的二价芳香族胺基）用作原料，将芳环上的一个或多个CH键转化成由具有一个或多个特征基团X并由通式（2）表示的重复单元的聚合物：（其中X表示特征基团; Ar 2表示各自具有n + 2的化合价的亚芳基，杂环基或芳香族胺基，并且其中Ar1芳香环上的n个nN都已转化为 CX键; n为1-4的整数）（以下，将该聚合物称为具有特征基团（X）的聚合物）。（B）将具有在步骤（A）中制造的特征基团（X）的聚合物与具有与特征基团（X）反应的特征基团（Y）的化合物反应以形成键的步骤。

7. 发明申请

US20090018309A1 Method for Producing Aromatic Compound Polymer 有权
标题翻译：生产芳香族化合物聚合物的方法
公开(公告)号：US20090018309A1
公开(公告)日：2009-01-15
申请号：US11571280
申请日：2005-06-24
申请人： Hideyuki Higashimura , Daisuke Fukushima , Kazuei Ohuchi
发明人： Hideyuki Higashimura , Daisuke Fukushima , Kazuei Ohuchi
IPC分类号： C08G65/00 , C07F9/00
CPC分类号： C08G61/12 , C07C49/92 , C07F9/005 , C08G61/02 , C08G61/10
摘要： A method for producing an aromatic compound polymer comprising oxidatively polymerizing one or more of aromatic compound(s) having two or more hydrogen atoms directly connected to aromatic ring(s), in the presence of an oxidizing agent, wherein the method employs a catalyst composed of a transition metal complex or a catalyst prepared from a transition metal complex and an activating agent, and said catalyst has a parameter P defined by the following formula (A) of 0.50 or more, and a parameter Eo defined by the following formula (B) of 0.50 [V] or more: P=Af/Ai (A) and Eo=(Epa+Epc)/2[V] (B).
摘要翻译：一种芳族化合物聚合物的制造方法，其特征在于，在氧化剂的存在下，使直接与芳香环连接的2个以上的氢原子的一种以上的芳香族化合物氧化聚合，的过渡金属络合物或由过渡金属络合物和活化剂制备的催化剂，所述催化剂具有下式（A）定义的参数P为0.50以上，以及由下式（B ）0.50 [V]以上：<？in-line-formula description =“In-line Formulas”end =“lead”？> P = Af / Ai（A）<？in-line-formula description =“In -line公式“end =”tail“？> <？in-line-formula description =”In-line Formulas“end =”lead“？>和<？in-line-formula description =”In-line Formulas“end =“tail”？> <？in-line-formula description =“In-line formula”end =“lead”？> Eo =（Epa + Epc）/ 2 [V]（B）公式描述=“内联公式”end =“tail”？>

8. 发明申请

US20090096355A1 Aromatic Graft Polymer 审中-公开
标题翻译：芳族接枝聚合物
公开(公告)号：US20090096355A1
公开(公告)日：2009-04-16
申请号：US11921766
申请日：2006-06-09
申请人： Kazuei Ohuchi , Hideyuki Higashimura , Makoto Anryu
发明人： Kazuei Ohuchi , Hideyuki Higashimura , Makoto Anryu
IPC分类号： C08L85/04 , B05D5/00 , H01B1/12 , H01L51/30 , H01L51/54
CPC分类号： H01L51/5012 , C08G61/00 , C08G61/02 , C08G61/12 , C08G2261/1434 , C08G2261/3142 , C08G2261/3162 , C08G2261/411 , C08G2261/5222 , C08G2261/77 , C08G2261/92 , H01L51/0039 , H01L51/0043 , H01L51/0059 , H01L51/5048
摘要： An aromatic graft polymer containing one or more kinds of repeating units represented by the following formula (1). (In the formula, Ar1 represents a divalent residue of a π-conjugated cyclic compound having a side chain represented by the following formula (2), the side chain being bonded to a carbon atom which is included in the ring structure of the divalent π-conjugated-cyclic-compound residue represented by Ar1 and has an sp2 hybrid orbital: (wherein Ar2 represents a divalent group having a residue of a π-conjugated cyclic compound; X1 represents a direct bond or a divalent group selected from the group consisting of NQ1-, —PQ2-, and —BQ3-, wherein Q1 to Q3 each independently represents a substituent; Z represents a direct bond or a divalent connecting group; k is an integer of 3 or larger; and E1 represents hydrogen, halogeno, or a monovalent organic group, provided that when two or more Ar2's, X1's, and Z's are present, then they each may be the same or different and when two or more side chains represented by the formula (2) are present, then they may be the same or different.))
摘要翻译：含有下述式（1）所示的一种以上的重复单元的芳香族接枝聚合物。（式中，Ar 1表示具有由下式（2）表示的侧链的π-共轭环状化合物的二价残基，该侧链与包含在二价p 1的环结构中的碳原子键合由Ar1表示的共轭环化合物残基，并具有sp2杂环轨道：（其中Ar2表示具有π-共轭环状化合物的残基的二价基团; X1表示直接键或选自以下的二价基团： NQ1-，-PQ2-和-BQ3-，其中Q1至Q3各自独立地表示取代基; Z表示直接键或二价连接基团; k表示3以上的整数，E1表示氢，卤素或一个有机基团，条件是当存在两个或更多个Ar 2，X 1和Z时，它们各自可以相同或不同，并且当存在由式（2）表示的两个或更多个侧链时，则它们可以是相同或不同）））

9. 发明授权

US09109081B2 Method for producing aromatic polymer 有权
标题翻译：芳族聚合物的制备方法
公开(公告)号：US09109081B2
公开(公告)日：2015-08-18
申请号：US11816195
申请日：2006-02-15
申请人： Tsutomu Yokozawa , Kazuei Ohuchi , Yasuhiro Kubota , Hideyuki Higashimura
发明人： Tsutomu Yokozawa , Kazuei Ohuchi , Yasuhiro Kubota , Hideyuki Higashimura
IPC分类号： C08G79/00 , C08G61/02 , C08G61/10 , B01J31/22 , B01J31/24
CPC分类号： C08G61/02 , B01J31/2295 , B01J31/24 , B01J2531/824 , C08G61/10 , C08G2261/312 , C08G2261/3142 , C08G2261/411
摘要： A method for producing an aromatic polymer comprising polycondensing an aromatic compound of the following formula (I) in the presence of a palladium complex containing a phosphine compound of the following formula (II): (wherein, Ar represents an aromatic ring-containing bi-functional organic group. X represents a halogen atom, nitro group or group of the formula —SO3Q (wherein, Q represents an optionally substituted hydrocarbon group). Y represents an oxygen atom, sulfur atom or the like, and n represents 0 or 1. M represents a hydrogen atom, —B(OQ1)2 or the like (Q1 represents a hydrogen atom or hydrocarbon group.) P(R1)3 (II) (wherein, R1 represents a group of the following formula (III) or a group of the following formula (IV) and three R1s may be the same or different, providing at least one of three R1s is a group of the following formula (III)) —C(R2)3 (III) (wherein, R2 represents a hydrogen atom or an optionally substituted hydrocarbon group) (wherein, R3 to R7 represent each independently a hydrogen atom, optionally substituted hydrocarbon group or the like).
摘要翻译：一种芳香族聚合物的制造方法，其特征在于，在含有下述式（II）的膦化合物的钯络合物的存在下，使下式（I）的芳香族化合物缩聚：（式中，Ar表示含芳环的双 - X表示卤素原子，硝基或式-SO 3 Q基团（其中，Q表示任选取代的烃基），Y表示氧原子，硫原子等，n表示0或1。 M表示氢原子，-B（OQ1）2等（Q1表示氢原子或烃基）P（R1）3（Ⅱ）（式中，R1表示下式（III）的基团或 -C（R2）3（III）（其中，R2表示（R））表示的基团，可以相同或不同，提供三个R 1中的至少一个为下式（III）氢原子或任选取代的烃基）（其中，R3至R 7独立地表示氢原子，任选取代的烃基等）。

10. 发明申请

US20100144999A1 METHOD FOR PRODUCING AROMATIC POLYMER 有权
标题翻译：生产芳族聚合物的方法
公开(公告)号：US20100144999A1
公开(公告)日：2010-06-10
申请号：US11816195
申请日：2006-02-15
申请人： Tsutomu Yokozawa , Kazuei Ohuchi , Yasuhiro Kubota , Hideyuki Higashimura
发明人： Tsutomu Yokozawa , Kazuei Ohuchi , Yasuhiro Kubota , Hideyuki Higashimura
IPC分类号： C08G61/00
CPC分类号： C08G61/02 , B01J31/2295 , B01J31/24 , B01J2531/824 , C08G61/10 , C08G2261/312 , C08G2261/3142 , C08G2261/411
摘要： Disclosed is a method for producing an aromatic polymer characterized in that an aromatic compound represented by the formula (I) below is polycondensed in the presence of a palladium complex containing a phosphine compound represented by the formula (II) below. (I) (In the formula (I), Ar represents a bifunctional organic group containing an aromatic ring; X represents a halogen atom, a nitro group or a group expressed as —SO3Q (wherein Q is an optionally substituted hydrocarbon group); Y represents an oxygen atom, a sulfur atom or the like; n is 0 or 1; and M represents a hydrogen atom, a —B(OQ1)2 group (wherein Q1 is a hydrogen atom or a hydrocarbon group) or the like.) P(R1)3 (II) (In the formula (II), R1 represents a group represented by the formula (III) below or a group represented by the formula (IV) below, and three R1s may be the same as or different from one another, provided that at least one of R1s is a group represented by the formula (III) below.) —C(R2)3 (III) (In the formula (III), R2 represents a hydrogen atom or an optionally substituted hydrocarbon group.) (IV) (In the formula (IV), R3-R7 independently represent a hydrogen atom, an optionally substituted hydrocarbon group or the like.)
摘要翻译：公开了一种芳族聚合物的制造方法，其特征在于，在下述式（II）表示的膦化合物的钯络合物的存在下，将下述式（I）表示的芳香族化合物进行缩聚。（I）（式（I）中，Ar表示含有芳香环的双官能性有机基团，X表示卤素原子，硝基或-SO 3 Q表示的基团（Q表示可以具有取代基的烃基），Y表示表示氧原子，硫原子等; n为0或1; M表示氢原子，-B（OQ1）2基（其中Q1为氢原子或烃基）等）。 P（R 1）3（II）（式（II）中，R 1表示由下式（III）表示的基团或下述式（IV）表示的基团，3个R 1可以相同或不同前提条件是R 1中的至少一个是由下式（III）表示的基团）-C（R 2）3（III）（在式（III）中，R 2表示氢原子或任选取代的烃基）（Ⅳ）（式（Ⅳ）中，R 3 -R 7分别表示氢原子，可以具有取代基的烃基等）。

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