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1. 发明申请

US20060151311A1 Electroconductive 12ca0.7al203 and compound of same type, and method for preparation thereof 有权
标题翻译：导电性12ca0.7al203和同型化合物及其制备方法
公开(公告)号：US20060151311A1
公开(公告)日：2006-07-13
申请号：US10561968
申请日：2004-02-12
申请人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi , Isao Tanaka
发明人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi , Isao Tanaka
IPC分类号： C01B13/00
CPC分类号： H01B1/08 , C01F7/164 , C01F7/166 , C01P2006/40 , C04B35/44 , C04B35/653 , C04B2235/3208 , C04B2235/3213 , C04B2235/604 , C04B2235/6587 , C04B2235/664 , C04B2235/787 , C04B2235/94
摘要： In a solid solution system of Al2O3 and CAO or SrO, it has been difficult to obtain a material having a high electrical conductivity (>10−4 S·cm−) at room temperature. A compound is provided in which electrons at a high concentration are introduced into a 12CaO.7Al2O3 compound, a 12SrO.7Al2O3 compound, or a mixed crystal compound containing 12CaO.7Al2O3 and 12SrO.7Al2O3. The compound formed by substituting all the free oxygen ions with electrons is regarded as an electride compound in which [Ca24Al28O64]4+(4e−) or [Sr24Al28O64]4+(4e−) serves as a cation and electrons serve as anions. When a single crystal or a hydrostatic pressure press molded material of a fine powder thereof is held at approximately 700° C. in an alkaline metal vapor or an alkaline earth metal vapor, melt of a hydrostatic pressure press molded material of a powder is held at approximately 1,600° C. in a carbon crucible, followed by slow cooling for solidification, or a thin film of the compound held at approximately 600° C. is implanted with rare gas ions, a great number of the free oxygen ions can be substituted with electrons.
摘要翻译：在Al 2 N 3 O 3和CAO或SrO的固溶体系中，难以获得具有高导电性的材料（> 10 -4 S.cm ）在室温下。提供了一种化合物，其中将高浓度的电子引入12CaO7Al 2 O 3 O 3化合物，12SrO·7H 2 O 2 或者含有12CaO.7Al 2 O 3 3和12SrO 7 Al 2 O 3的混合晶体化合物， SUB> 3 。通过用电子代替全部游离氧离子而形成的化合物被认为是电化学化合物，其中[Ca 2 H 12 O 12 O 64] （4e-sup） - 或[Sr 2 O 2] 28 O 64] SUP + 4 +（4e - - ）用作阳离子，电子用作阴离子。当在碱金属蒸气或碱土金属蒸气中将其细粉末的单晶或静水压成型材料保持在约700℃时，将粉末的流体静压加压成型材料的熔体保持在在碳坩埚中约1600℃，然后缓慢冷却固化，或者在约600℃保持的化合物薄膜注入稀有气体离子，大量的游离氧离子可被电子。

2. 发明授权

US07507289B2 Electroconductive 12CaO—7Al2O3 and compound of same type, and method for preparation thereof 有权
标题翻译：导电性12CaO-7Al2O3和相同类型的化合物及其制备方法
公开(公告)号：US07507289B2
公开(公告)日：2009-03-24
申请号：US10561968
申请日：2004-02-12
申请人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi , Masashi Miyakawa , Isao Tanaka
发明人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi , Masashi Miyakawa , Isao Tanaka
IPC分类号： C30B1/10
CPC分类号： H01B1/08 , C01F7/164 , C01F7/166 , C01P2006/40 , C04B35/44 , C04B35/653 , C04B2235/3208 , C04B2235/3213 , C04B2235/604 , C04B2235/6587 , C04B2235/664 , C04B2235/787 , C04B2235/94
摘要： In a solid solution system of Al2O3 and CAO or SrO, it has been difficult to obtain a material having a high electrical conductivity (>10−4 S·cm−) at room temperature.A compound is provided in which electrons at a high concentration are introduced into a 12CaO.7Al2O3 compound, a 12SrO.7Al2O3 compound, or a mixed crystal compound containing 12CaO.7Al2O3 and 12SrO.7Al2O3. The compound formed by substituting all the free oxygen ions with electrons is regarded as an electride compound in which [Ca24Al28O64]4+(4e−) or [Sr24Al28O64]4+(4e−) serves as a cation and electrons serve as anions. When a single crystal or a hydrostatic pressure press molded material of a fine powder thereof is held at approximately 700° C. in an alkaline metal vapor or an alkaline earth metal vapor, melt of a hydrostatic pressure press molded material of a powder is held at approximately 1,600° C. in a carbon crucible, followed by slow cooling for solidification, or a thin film of the compound held at approximately 600° C. is implanted with rare gas ions, a great number of the free oxygen ions can be substituted with electrons.
摘要翻译：在Al 2 O 3和CAO或SrO的固溶体系中，难以在室温下获得具有高电导率（> 10 -4 S.cm-）的材料。提供了一种化合物，其中将高浓度的电子引入12CaO.7Al2O3化合物，12SrO.7Al2O3化合物或含有12CaO.7Al2O3和12SrO.7Al2O3的混合晶体化合物。通过用电子代替全部游离氧离子形成的化合物被认为是其中[Ca24Al28O64] 4+（4e-）或[Sr24Al28O64] 4+（4e-）用作阳离子的电子化合物，电子用作阴离子。当在碱金属蒸气或碱土金属蒸气中将其细粉末的单晶或静水压成型材料保持在约700℃时，将粉末的流体静压加压成型材料的熔体保持在在碳坩埚中约1600℃，然后缓慢冷却固化，或者在约600℃保持的化合物薄膜注入稀有气体离子，大量的游离氧离子可被电子。

3. 发明申请

US20050279279A1 Hydrogen-containing electrically conductive organic compound 有权
标题翻译：含氢导电有机化合物
公开(公告)号：US20050279279A1
公开(公告)日：2005-12-22
申请号：US10511715
申请日：2003-04-18
申请人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi
发明人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi
IPC分类号： C01B3/00 , C01F7/16 , H01B1/08 , C30B21/02 , C30B7/00 , C30B9/00 , C30B11/00 , C30B28/06
CPC分类号： H01B1/08 , C01B3/00 , C01F7/164 , C01F7/166 , C01P2006/40 , C04B35/44 , C04B2235/3208 , C04B2235/3213 , C04B2235/44 , C04B2235/6565 , C04B2235/658 , C04B2235/6582 , C04B2235/96 , C30B7/00 , C30B7/005 , Y02E60/324
摘要： Disclosed is a 12CaO.7Al2O3 compound, a 12SrO.7Al2O3 compound, or a mixed crystal compound of 12CaO.7Al2O3 and 12SrO.7Al2O3, which contains a negative hydrogen ion (H−, H2−, H2− at a concentration of 1×1018 cm−3 or more. A negative hydrogen ion comprising a primary component of a hydride ion is incorporated into C12A7 (12CaO.7Al2O3), so that a function of being converted from an insulative material to an electrically conductive material in a sustained manner by means of irradiation with light can be exhibited even in the normal atmosphere at a room temperature. The present invention also provides a solid electrolyte capable of conducting a negative hydrogen ion, and means for releasing a hydride ion from the inside of a solid into a gaseous phase using an electric field.
摘要翻译：公开了一种12CaO·0.7Al 2 O 3 N 3化合物，12SrO·7H 2 O 3 O 3化合物，或 12CaO.7Al 2 O 3 3和12SrO 7 Al 2 O 3 3 N 3的混合晶体化合物，其含有负的浓度为1×10 18的氢离子（H 2 - ，H 2 - ，H 2 - ）包含氢离子的主要成分的负极性氢离子被并入到C12A7（12Ca0.7Al2O3）中， <！ - SIPO - >，即使在室温的正常气氛中也可以显示通过照射光从持续的方式将绝缘材料转换成导电材料的功能，本发明还提供能够导入负氢离子的固体电解质，以及使用电场将氢离子从固体内部释放到气相中的装置。

4. 发明授权

US07670585B2 Method for preparing electroconductive mayenite type compound 有权
标题翻译：导电钙铝石型化合物的制备方法
公开(公告)号：US07670585B2
公开(公告)日：2010-03-02
申请号：US11948147
申请日：2007-11-30
申请人： Hideo Hosono , Katsuro Hayashi , Sung Wng Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
发明人： Hideo Hosono , Katsuro Hayashi , Sung Wng Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
IPC分类号： C01F7/16
CPC分类号： C01F7/164 , C01F7/166 , C01P2002/50 , C01P2002/84 , C01P2006/40 , C01P2006/60 , H01B1/08
摘要： Provided is a method for preparing an electroconductive mayenite type compound with good properties readily and stably at low cost without need for expensive facilities, a reaction at high temperature and for a long period of time, or complicated control of reaction.A method for preparing an electroconductive mayenite type compound comprises a step of subjecting a precursor to heat treatment, wherein the precursor contains Ca and/or Sr, and Al, a molar ratio of (a total of CaO and SrO:Al2O3) is from (12.6:6.4) to (11.7:7.3) as calculated as oxides, a total content of CaO, SrO and Al2O3 in the precursor is at least 50 mol %, and the precursor is a vitreous or crystalline material; and the method comprises a step of mixing the precursor with a reducing agent and performing the heat treatment of holding the mixture at 600-1,415° C. in an inert gas or vacuum atmosphere with an oxygen partial pressure of at most 10 Pa.
摘要翻译：本发明提供一种低成本地容易且稳定地制备具有良好性能的导电性钙铝石型化合物的方法，而不需要昂贵的设备，高温反应和长时间的反应或复杂的反应控制。制备导电性钙铝石型化合物的方法包括使前体进行热处理的步骤，其中前体含有Ca和/或Sr，和Al，（CaO和SrO：Al 2 O 3的总和）的摩尔比为（ 12.6：6.4）至（11.7：7.3），前体中CaO，SrO和Al2O3的总含量为至少50摩尔％，前体为玻璃态或结晶性材料; 该方法包括将前体与还原剂混合并在氧分压至多10Pa的惰性气体或真空气氛中进行600-1,415℃保持混合物的热处理的步骤。

5. 发明授权

US07465433B2 Method for preparing electroconductive mayenite type compound 有权
标题翻译：导电钙铝石型化合物的制备方法
公开(公告)号：US07465433B2
公开(公告)日：2008-12-16
申请号：US11503244
申请日：2006-08-14
申请人： Hideo Hosono , Katsuro Hayashi , Masashi Miyakawa , Masahiro Hirano , Sungwng Kim , Setsuro Ito , Satoru Narushima
发明人： Hideo Hosono , Katsuro Hayashi , Masashi Miyakawa , Masahiro Hirano , Sungwng Kim , Setsuro Ito , Satoru Narushima
IPC分类号： C01F7/00 , C01F11/02
CPC分类号： C04B35/653 , C01F7/164 , C01P2006/40 , C04B35/44 , C04B2235/3205 , C04B2235/3208 , C04B2235/3213 , C04B2235/96
摘要： To provide a method for preparing a mayenite type compound having electroconductivity imparted.A method for preparing an electroconductive mayenite type compound, which comprises melting a raw material containing Al and at least one element selected from the group consisting of Ca and Sr, holding the melt in a low oxygen partial pressure atmosphere having an oxygen partial pressure of not higher than 10 Pa, followed by cooling or annealing in a low oxygen partial pressure atmosphere or in atmospheric air for solidification, thereby to replace oxygen present in cages by electrons in a high concentration.
摘要翻译：提供制备具有导电性的钙铝石型化合物的方法。一种制备导电性钙铝石型化合物的方法，其包括熔融含有Al的原料和选自Ca和Sr中的至少一种元素，将熔体保持在氧分压不为低的氧分压气氛中高于10Pa，然后在低氧分压气氛或大气中进行冷却或退火以固化，从而以高浓度的电子代替笼中存在的电子。

6. 发明申请

US20080095688A1 METHOD FOR PREPARING ELECTROCONDUCTIVE MAYENITE TYPE COMPOUND 有权
标题翻译：制备电极型MAYENITE型化合物的方法
公开(公告)号：US20080095688A1
公开(公告)日：2008-04-24
申请号：US11948147
申请日：2007-11-30
申请人： Hideo Hosono , Katsuro Hayashi , Sung Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
发明人： Hideo Hosono , Katsuro Hayashi , Sung Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
IPC分类号： C01F17/00 , C01F11/02 , C01F7/00
CPC分类号： C01F7/164 , C01F7/166 , C01P2002/50 , C01P2002/84 , C01P2006/40 , C01P2006/60 , H01B1/08
摘要： Provided is a method for preparing an electroconductive mayenite type compound with good properties readily and stably at low cost without need for expensive facilities, a reaction at high temperature and for a long period of time, or complicated control of reaction. A method for preparing an electroconductive mayenite type compound comprises a step of subjecting a precursor to heat treatment, wherein the precursor contains Ca and/or Sr, and Al, a molar ratio of (a total of CaO and SrO:Al2O3) is from (12.6:6.4) to (11.7:7.3) as calculated as oxides, a total content of CaO, SrO and Al2O3 in the precursor is at least 50 mol %, and the precursor is a vitreous or crystalline material; and the method comprises a step of mixing the precursor with a reducing agent and performing the heat treatment of holding the mixture at 600-1,415° C. in an inert gas or vacuum atmosphere with an oxygen partial pressure of at most 10 Pa.
摘要翻译：本发明提供一种低成本地容易且稳定地制备具有良好性能的导电性钙铝石型化合物的方法，而不需要昂贵的设备，高温反应和长时间的反应或复杂的反应控制。制备导电性钙铝石型化合物的方法包括以下步骤：将前体进行热处理，其中前体含有Ca和/或Sr，和Al，（CaO和SrO：Al 2的总和的摩尔比（12.6:4.4）至（11.7:7.3）按氧化物计算，CaO，SrO和Al 2 O 2的总含量前体中的3 <3>至少为50摩尔％，前体是玻璃状或结晶的材料; 该方法包括将前体与还原剂混合并在氧分压至多10Pa的惰性气体或真空气氛中进行600-1,415℃保持混合物的热处理的步骤。

7. 发明申请

US20080089826A1 METHOD FOR PREPARING ELECTROCONDUCTIVE MAYENITE TYPE COMPOUND 有权
标题翻译：制备电极型MAYENITE型化合物的方法
公开(公告)号：US20080089826A1
公开(公告)日：2008-04-17
申请号：US11948053
申请日：2007-11-30
申请人： Hideo Hosono , Katsuro Hayashi , Sung Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
发明人： Hideo Hosono , Katsuro Hayashi , Sung Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
IPC分类号： C01F7/02 , C01F17/00
CPC分类号： C01F7/164 , C01F7/002 , C01F7/166 , C01P2002/50 , C01P2002/84 , C01P2006/40 , C01P2006/60 , C03C4/14 , C03C10/0036 , C04B35/44 , C04B35/6262 , C04B35/62675 , C04B35/6268 , C04B2235/3201 , C04B2235/3203 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3224 , C04B2235/3229 , C04B2235/3232 , C04B2235/3239 , C04B2235/3241 , C04B2235/3262 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/3281 , C04B2235/3287 , C04B2235/3409 , C04B2235/3418 , C04B2235/44 , C04B2235/444 , C04B2235/445 , C04B2235/446 , C04B2235/652 , C30B29/22 , C30B33/00 , H01B1/08
摘要： Provided is a method for preparing an electroconductive mayenite type compound with good properties readily and stably at low cost. A production method of an electroconductive mayenite type compound comprising a step of subjecting a precursor to heat treatment, is a method for preparing an electroconductive mayenite type compound, comprising a step of subjecting a precursor to heat treatment; wherein the precursor is a vitreous or crystalline material, which contains Ca and Al, in which a molar ratio of (CaO:Al2O3) is from (12.6:6.4) to (11.7:7.3) as calculated as oxides, and in which a total amount of CaO and Al2O3 is at least 50 mol %, and wherein the heat treatment is heat treatment comprising holding the precursor at a heat treatment temperature T of from 600 to 1415° C. and in an inert gas or vacuum atmosphere with an oxygen partial pressure PO2 in a range of PO2≦105×exp[{−7.9×l04/(T+273)}+14.4] in the unit of Pa.
摘要翻译：提供了一种以低成本容易且稳定地制备具有良好性能的导电性钙铝石型化合物的方法。包括对前体进行热处理的步骤的导电性钙铝石型化合物的制造方法是制备导电性钙铝石型化合物的方法，包括使前体进行热处理的工序; 其中所述前体是含有Ca和Al的玻璃质或结晶材料，其中（CaO：Al 2 O 3 3）的摩尔比为（12.6:6.4））至（11.7:7.3），其中CaO和Al 2 O 3 3的总量为至少50摩尔％，其中热量处理是热处理，包括将前体保持在600-1415℃的热处理温度T下，在氧分压P

8. 发明授权

US07235225B2 12CaO·7A12O3 compound and method for preparation thereof 有权
标题翻译： 12CaO.7A12O3化合物及其制备方法
公开(公告)号：US07235225B2
公开(公告)日：2007-06-26
申请号：US10492938
申请日：2002-10-17
申请人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi
发明人： Hideo Hosono , Masahiro Hirano , Katsuro Hayashi
IPC分类号： C01F7/00 , A01N59/06 , B01J23/02 , H01M8/10
CPC分类号： H01M4/8605 , A01N59/06 , B01J23/002 , B01J23/02 , B01J37/08 , B01J2523/00 , C01F7/164 , C01P2002/76 , C01P2002/77 , C01P2002/82 , C01P2002/86 , C01P2002/90 , H01M4/9016 , H01M4/9025 , B01J2523/23 , B01J2523/31
摘要： There is provided a C12A7 compound capable of selectively and reversibly clathrating X− ions, such as active oxygen radicals, with improved controllability. The C12A7 compound clathrating OH− ions and On− at a concentration of 2×1019 cm−3 or less can be prepared by subjecting a mixed material containing Ca and Al to a solid phase reaction at a firing temperature not lower than 1200° C. and lower than 1449° C. in a dry oxygen atmosphere having an oxygen partial pressure of 0.1 atm or more and a water vapor partial pressure of 10−3 atm or less, keeping the resultant product at a temperature of 1200° C. or higher, and cooling rapidly. The C12A7 compound is heat-treated to clathrate OH− ions at a concentration of 2×1019 cm−3 or less, and On− at a high concentration of more than 2×1019 cm−3. The compound can reversibly clathrate or release On− ion radicals through the elevation or lowering of the temperature thereof in a temperature range of 300 to 850° C. The compound is useful for an oxidation catalyst, an anti-bacterial agent, an ion conducting material, an electrode for a solid-electrolyte fuel cell, and the like.
摘要翻译：提供了一种C12A7化合物，其能够选择性地和可逆地包合诸如活性氧自由基之类的X - O - 离子，具有改进的可控性。浓度为2×10 19 -3 -3或更低的C12A7化合物包合OH - O 2和O 2 - 通过在氧分压为0.1atm以上的干氧气氛中，在不低于1200℃且低于1449℃的烧成温度下对含有Ca和Al的混合材料进行固相反应来制备，以及水蒸汽分压为10 -3 atm或更低，保持所得产物在1200℃或更高的温度，并快速冷却。将C12A7化合物热处理以2×10 19 -3 -3或更低的浓度包合OH - O 2离子， - 超过2×10 9 cm -3 -3的高浓度。化合物可以通过在300至850℃的温度范围内升高或降低其温度来可逆地包合或释放离子自由基。该化合物可用于氧化催化剂，抗 - 细菌剂，离子导电材料，固体电解质燃料电池用电极等。

9. 发明申请

US20060276326A1 Method for preparing electroconductive mayenite type compound 有权
标题翻译：导电钙铝石型化合物的制备方法
公开(公告)号：US20060276326A1
公开(公告)日：2006-12-07
申请号：US11503244
申请日：2006-08-14
申请人： Hideo Hosono , Katsuro Hayashi , Masashi Miyakawa , Masahiro Hirano , Sungwng Kim , Setsuro Ito , Satoru Narushima
发明人： Hideo Hosono , Katsuro Hayashi , Masashi Miyakawa , Masahiro Hirano , Sungwng Kim , Setsuro Ito , Satoru Narushima
IPC分类号： C04B35/00
CPC分类号： C04B35/653 , C01F7/164 , C01P2006/40 , C04B35/44 , C04B2235/3205 , C04B2235/3208 , C04B2235/3213 , C04B2235/96
摘要： To provide a method for preparing a mayenite type compound having electroconductivity imparted. A method for preparing an electroconductive mayenite type compound, which comprises melting a raw material containing Al and at least one element selected from the group consisting of Ca and Sr, holding the melt in a low oxygen partial pressure atmosphere having an oxygen partial pressure of not higher than 10 Pa, followed by cooling or annealing in a low oxygen partial pressure atmosphere or in atmospheric air for solidification, thereby to replace oxygen present in cages by electrons in a high concentration.
摘要翻译：提供制备具有导电性的钙铝石型化合物的方法。一种制备导电性钙铝石型化合物的方法，其包括熔融含有Al的原料和选自Ca和Sr中的至少一种元素，将熔体保持在氧分压不为低的氧分压气氛中高于10Pa，然后在低氧分压气氛或大气中进行冷却或退火以固化，从而以高浓度的电子代替笼中存在的电子。

10. 发明授权

US07722846B2 Method for preparing electroconductive mayenite type compound 有权
标题翻译：导电钙铝石型化合物的制备方法
公开(公告)号：US07722846B2
公开(公告)日：2010-05-25
申请号：US11948053
申请日：2007-11-30
申请人： Hideo Hosono , Katsuro Hayashi , Sung Wng Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
发明人： Hideo Hosono , Katsuro Hayashi , Sung Wng Kim , Masahiro Hirano , Satoru Narushima , Setsuro Ito
IPC分类号： C01F7/16
CPC分类号： C01F7/164 , C01F7/002 , C01F7/166 , C01P2002/50 , C01P2002/84 , C01P2006/40 , C01P2006/60 , C03C4/14 , C03C10/0036 , C04B35/44 , C04B35/6262 , C04B35/62675 , C04B35/6268 , C04B2235/3201 , C04B2235/3203 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3224 , C04B2235/3229 , C04B2235/3232 , C04B2235/3239 , C04B2235/3241 , C04B2235/3262 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/3281 , C04B2235/3287 , C04B2235/3409 , C04B2235/3418 , C04B2235/44 , C04B2235/444 , C04B2235/445 , C04B2235/446 , C04B2235/652 , C30B29/22 , C30B33/00 , H01B1/08
摘要： Provided is a method for preparing an electroconductive mayenite type compound with good properties readily and stably at low cost.A production method of an electroconductive mayenite type compound comprising a step of subjecting a precursor to heat treatment, is a method for preparing an electroconductive mayenite type compound, comprising a step of subjecting a precursor to heat treatment; wherein the precursor is a vitreous or crystalline material, which contains Ca and Al, in which a molar ratio of (CaO:Al2O3) is from (12.6:6.4) to (11.7:7.3) as calculated as oxides, and in which a total amount of CaO and Al2O3 is at least 50 mol %, and wherein the heat treatment is heat treatment comprising holding the precursor at a heat treatment temperature T of from 600 to 1415° C. and in an inert gas or vacuum atmosphere with an oxygen partial pressure PO2 in a range ofPO2≦105×exp [{−7.9×l04/(T+273)}+14.4] in the unit of Pa.
摘要翻译：提供了一种以低成本容易且稳定地制备具有良好性能的导电性钙铝石型化合物的方法。包括对前体进行热处理的步骤的导电性钙铝石型化合物的制造方法是制备导电性钙铝石型化合物的方法，包括使前体进行热处理的工序; 其中所述前体是含有Ca和Al的玻璃质或结晶材料，其中（CaO：Al 2 O 3）的摩尔比为（12.6:4.4）至（11.7:7.3），其计算为氧化物，其中总计 CaO和Al 2 O 3的量为至少50摩尔％，其中热处理为热处理，包括将前体保持在600-1415℃的热处理温度T下，在惰性气体或具有氧部分的惰性气体或真空气氛中在PO2＆NlE的范围内的压力PO2为105×exp [{-7.9×104 /（T + 273）} + 14.4]。

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