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1. 发明授权

US5445698A Method of fabricating an internal composite layer composed of an electrically insulating substrate with a copper layer formed thereon and a film of a coupling agent covering the copper layer for a multilayer circuit board 失效
标题翻译：制作由形成有铜层的电绝缘性基板构成的内部复合层的方法以及覆盖多层电路基板用铜层的偶联剂膜
公开(公告)号：US5445698A
公开(公告)日：1995-08-29
申请号：US22027
申请日：1993-02-24
申请人： Hidekazu Takano , Tokio Yoshimitsu , Akinori Hibino , Yoshihide Sawa , Motoyuki Toki , Yang Wu , Yuen C. Tak , Tadao Ohnaka
发明人： Hidekazu Takano , Tokio Yoshimitsu , Akinori Hibino , Yoshihide Sawa , Motoyuki Toki , Yang Wu , Yuen C. Tak , Tadao Ohnaka
IPC分类号： B32B15/08 , C08J5/12 , H05K3/38 , H05K3/46 , B32B31/12
CPC分类号： C08J5/12 , B32B15/08 , H05K3/385 , H05K3/389 , C08J2363/00 , H05K2203/0315 , H05K3/382 , H05K3/4611 , Y10T156/10
摘要： An internal composite layer for a multilayer circuit board, which is composed of an electrically insulating substrate with a copper layer formed thereon and a film of a coupling agent covering the copper layer is fabricated in accordance with the following method. That is, the copper layer is treated with a base or the base and an accelerating agent to supply hydroxyl groups to a surface thereof. Subsequently, thus treated copper layer is coated with the coupling agent, e.g., a silane coupling agent. The coupling agent is chemically bonded to the treated copper layer by the reaction of the hydroxyl groups with the coupling agent, so that an adhesion strength between the copper layer and the coupling agent is remarkably increased. In addition, since it is not necessary for forming a copper oxide layer in the surface of the copper layer, the internal composite layer shows excellent acid resistance without causing a pink-ring which usually occur around a through-hole plating.
摘要翻译：根据以下方法制造由其上形成有铜层的电绝缘基板和覆盖铜层的偶联剂膜构成的用于多层电路板的内部复合层。也就是说，铜层用碱或碱和加速剂处理以向其表面提供羟基。随后，用偶联剂例如硅烷偶联剂涂覆这样处理过的铜层。偶联剂通过羟基与偶联剂的反应与经处理的铜层化学键合，使得铜层和偶联剂之间的粘合强度显着增加。此外，由于不需要在铜层的表面形成氧化铜层，因此内部复合层显示优异的耐酸性，而不会在通孔电镀周围通常发生粉红色环。

2. 发明授权

US09303257B2 Method and system for cell and tissue cultivation 有权
标题翻译：细胞和组织培养的方法和系统
公开(公告)号：US09303257B2
公开(公告)日：2016-04-05
申请号：US13131152
申请日：2010-07-01
申请人： Toshimi Fukui , Motoyuki Toki
发明人： Toshimi Fukui , Motoyuki Toki
IPC分类号： C12M1/00 , C12M3/00 , C12N13/00 , C12M1/12 , C12M1/26 , C12N11/00
CPC分类号： C12N13/00 , C12M23/04 , C12M23/20 , C12M33/00 , C12N11/00
摘要： A cell cultivating platform includes a substrate having a surface, at least one actuator moveable relative to the substrate, and a deformable material layer positioned above at least a portion of the supporting surface and the at least one actuator. The deformable material layer positioned opposite the substrate surface includes a biocompatible supportive surface suitable for supporting cultivated cells. The supportive surface deforms or otherwise deflects in response to activation of the at least one actuator, effectively releasing at least a portion of the cultured cells from the supportive surface. Suitable actuators include piezoelectric actuators that can be selectively energized according to one or more patterns to facilitate separation of cells from the supportive surface. Such activation cycles can be repeated.
摘要翻译：细胞培养平台包括具有表面的基底，可相对于基底移动的至少一个致动器和位于支撑表面和至少一个致动器的至少一部分上方的可变形材料层。与基底表面相对定位的可变形材料层包括适于支撑培养细胞的生物相容支撑表面。支撑表面响应于至少一个致动器的激活而变形或以其它方式偏转，有效地将至少一部分培养细胞从支撑表面释放出来。合适的致动器包括压电致动器，其可以根据一个或多个图案选择性地通电以便于将细胞与支撑表面分离。可以重复这样的激活循环。

3. 发明授权

US07741376B2 Process for preparing dispersed ingredient having metal-oxygen bonds 有权
标题翻译：制备具有金属 - 氧键的分散成分的方法
公开(公告)号：US07741376B2
公开(公告)日：2010-06-22
申请号：US12332620
申请日：2008-12-11
申请人： Motoyuki Toki , Akiji Higuchi , Nobuo Kimura , Yoshitaka Fujita
发明人： Motoyuki Toki , Akiji Higuchi , Nobuo Kimura , Yoshitaka Fujita
IPC分类号： B01F3/08
CPC分类号： C08K5/0091 , C08F291/00 , C08G18/3876 , C08G18/775 , C08L51/003 , C08L51/10 , C09D1/00
摘要： A dispersed ingredient having metal-oxygen bonds which is obtained by hydrolyzing a metal alkoxide in an organic solvent in the absence of an acid, a base, and/or a dispersion stabilizer, either with 0.5 to less than 1 mol of water per mol of the metal alkoxide or at −20° C. or lower with 1.0 to less than 2.0 mol of water per mol of the metal alkoxide. In the organic solvent, the dispersed ingredient is stably dispersed without aggregating. Use of the dispersed ingredient enables a thin metal oxide film and a homogeneous organic/inorganic composite to be produced at a temperature as low as 200° C. or below.
摘要翻译：具有金属 - 氧键的分散成分，其通过在不存在酸，碱和/或分散稳定剂的情况下在有机溶剂中水解金属醇盐而获得，每摩尔0.5〜1摩尔水金属醇盐，或者在-20℃以下，相对于每摩尔金属醇盐为1.0〜小于2.0摩尔的水。在有机溶剂中，分散成分稳定地分散而不聚集。使用分散成分可以在低至200℃或更低的温度下生产薄金属氧化物膜和均匀的有机/无机复合材料。

4. 发明申请

US20090143498A1 PROCESS FOR PREPARING DISPERSED INGEDIENT HAVING METAL-OXYGEN BONDS 有权
标题翻译：用于制备具有金属氧原子的分解成分的方法
公开(公告)号：US20090143498A1
公开(公告)日：2009-06-04
申请号：US12332620
申请日：2008-12-11
申请人： Motoyuki Toki , Akiji Higuchi , Nobuo Kimura , Yoshitaka Fujita
发明人： Motoyuki Toki , Akiji Higuchi , Nobuo Kimura , Yoshitaka Fujita
IPC分类号： G02B1/04 , B05D5/06
CPC分类号： C08K5/0091 , C08F291/00 , C08G18/3876 , C08G18/775 , C08L51/003 , C08L51/10 , C09D1/00
摘要： A dispersed ingredient having metal-oxygen bonds which is obtained by hydrolyzing a metal alkoxide in an organic solvent in the absence of an acid, a base, and/or a dispersion stabilizer, either with 0.5 to less than 1 mol of water per mol of the metal alkoxide or at −20° C. or lower with 1.0 to less than 2.0 mol of water per mol of the metal alkoxide. In the organic solvent, the dispersed ingredient is stably dispersed without aggregating. Use of the dispersed ingredient enables a thin metal oxide film and a homogeneous organic/inorganic composite to be produced at a temperature as low as 200° C. or below.
摘要翻译：具有金属 - 氧键的分散成分，其通过在不存在酸，碱和/或分散稳定剂的情况下在有机溶剂中水解金属醇盐而获得，每摩尔0.5〜1摩尔水金属醇盐，或者在-20℃以下，相对于每摩尔金属醇盐为1.0〜小于2.0摩尔的水。在有机溶剂中，分散成分稳定地分散而不聚集。使用分散成分可以在低至200℃或更低的温度下生产薄金属氧化物膜和均匀的有机/无机复合材料。

5. 发明申请

US20060239902A1 Dispersoid having metal-oxygen bonds, metal oxide film, and monomolecular film 有权
标题翻译：具有金属氧键的分散体，金属氧化物膜和单分子膜
公开(公告)号：US20060239902A1
公开(公告)日：2006-10-26
申请号：US10533580
申请日：2003-11-12
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
IPC分类号： C01G23/047
CPC分类号： C01B13/32 , C01G23/053 , C23C18/1216 , C23C18/122 , Y10T428/24355
摘要： The invention provides dispersoids having metal-oxygen groups which are suitable for the production of metal oxide thin-films at a low temperature of 200° C. or below and for the production of homogeneous organic-inorganic hybrid materials. The invention also provides metal oxide thin-films and organic-inorganic hybrid materials endowed with various capabilities, particularly organic-inorganic hybrid materials having a high refractive index and high transparency. Use is made of a dispersoid having metal-oxygen bonds which is obtained by mixing a metal compound having at least three hydrolyzable groups with at least 0.5 mole but less than 2 moles of water per mole of the metal compound in an organic solvent, in the absence of an acid, a base and/or a dispersion stabilizer, and at a temperature at or below the temperature at which the metal compound begins to hydrolyze, then raising the temperature to at least the temperature at which hydrolysis begins.
摘要翻译：本发明提供了适用于在200℃或更低的低温下生产金属氧化物薄膜的金属 - 氧基分散体和用于生产均相有机 - 无机混合材料的分散体。本发明还提供具有各种能力的金属氧化物薄膜和有机 - 无机混合材料，特别是具有高折射率和高透明度的有机 - 无机混合材料。使用具有金属 - 氧键的分散体，其通过在有机溶剂中将具有至少三个可水解基团的金属化合物与每摩尔金属化合物混合至少0.5摩尔但小于2摩尔水而获得，不存在酸，碱和/或分散体稳定剂，并且在金属化合物开始水解或在低于金属化合物开始水解的温度的温度下，将温度升至至少水解开始的温度。

6. 发明授权

US06247799B1 Ferroelectric element, process for producing the same, and ink jet head 失效
标题翻译：铁电元件，其制造方法和喷墨头
公开(公告)号：US06247799B1
公开(公告)日：2001-06-19
申请号：US09499686
申请日：2000-02-08
申请人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
发明人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
IPC分类号： B41J2045
CPC分类号： B41J2/14233 , B41J2202/03 , C23C18/1216 , C23C18/1254 , H01L41/1876 , H01L41/318
摘要： A ferroelectric element, having a ferroelectric material containing at least two metals, the ferroelectric element having been produced by a process including the steps of: providing alkoxides of the respective metals as starting compounds; hydrolyzing the metal alkoxides in the presence of a catalytic amount of a protonic acid to increase the molecular weight; and adding a film-forming polymer material to the sol-like solution prepared in the step of increasing the molecular weight to prepare a sol-like ferroelectric precursor solution. The ferroelectric element can be formed in a thick film form without creating any cracks. It can be advantageously used as a piezoelectric element in a piezoelectric ink jet head.
摘要翻译：具有含有至少两种金属的铁电材料的铁电体元件，所述铁电体元件通过包括以下步骤的方法生产：提供各种金属的醇盐作为起始化合物; 在催化量的质子酸存在下水解金属醇盐以提高分子量; 并将成膜聚合物材料添加到在提高分子量的步骤中制备的溶胶状溶液中以制备溶胶状铁电体前体溶液。铁电元件可以形成为厚膜形式而不产生任何裂纹。它可以有利地用作压电喷墨头中的压电元件。

7. 发明申请

US20110135878A1 Dispersoid having metal-oxygen bonds, metal oxide film, and monomolecular film 审中-公开
标题翻译：具有金属氧键的分散体，金属氧化物膜和单分子膜
公开(公告)号：US20110135878A1
公开(公告)日：2011-06-09
申请号：US12929592
申请日：2011-02-02
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
IPC分类号： B32B3/30 , B32B27/06 , C09D1/00 , C01B13/00
CPC分类号： C01B13/32 , C01G23/053 , C23C18/1216 , C23C18/122 , Y10T428/24355
摘要： Dispersoids having metal-oxygen groups that are suitable for the production of metal oxide thin-films at a low temperature of 200° C. or below and for the production of homogeneous organic-inorganic hybrid materials. The dispersoid having metal-oxygen bonds may be obtained by mixing a metal compound having at least three hydrolyzable groups with at least 0.5 mole but less than 2 moles of water per mole of the metal compound in an organic solvent, in the absence of an acid, a base, and/or a dispersion stabilizer, and at a temperature at or below the temperature at which the metal compound begins to hydrolyze, then raising the temperature to at least the temperature at which hydrolysis begins.
摘要翻译：具有适合于在200℃或更低的低温下生产金属氧化物薄膜并用于生产均相有机 - 无机杂化材料的金属 - 氧基的分散体。具有金属 - 氧键的分散质可以通过在不存在酸的情况下，在有机溶剂中将具有至少三个可水解基团的金属化合物与每摩尔金属化合物相混合至少0.5摩尔但小于2摩尔的水，碱和/或分散稳定剂，并且在等于或低于金属化合物开始水解的温度的温度下，然后将温度升至至少水解开始的温度。

8. 发明授权

US06350486B2 Ferroelectric element and process for producing the same 失效
标题翻译：铁电元件及其制造方法
公开(公告)号：US06350486B2
公开(公告)日：2002-02-26
申请号：US09432231
申请日：1999-11-03
申请人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
发明人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
IPC分类号： B05D512
CPC分类号： H01L41/318 , C01G25/006 , C01P2002/34 , C01P2002/72 , C01P2002/77 , C01P2004/02 , H01L41/1876 , Y10T29/42 , Y10T29/49002
摘要： A ferroelectric element comprising a ferroelectric material containing at least two metals, the ferroelectric element having been produced by a process including a sol-gel process in the presence of a thickener and/or an association preventive from aqueous solutions of respective salts of the metals. The ferroelectric element is advantageous in that the handling of starting compounds and the production of the ferroelectric element are easy, the storage stability of the starting compound solution is good, the cost is low, the ferroelectric element can be formed as a thin layer, particles on the surface of the thin layer are fine and dense, and, hence, the surface smoothness is good. The ferroelectric element is excellent also in piezoelectric properties and therefore can be advantageously used as a piezoelectric element in a piezoelectric ink jet head.
摘要翻译：一种铁电体元件，其包含含有至少两种金属的铁电材料，所述铁电体元件是通过包括溶胶 - 凝胶法在增稠剂存在下和/或与金属的各种盐的水溶液缔合防止的方法制备的。铁电元件的优点在于，起始化合物的处理和铁电体元素的制备容易，起始化合物溶液的储存稳定性好，成本低，铁电元件可以形成为薄层，颗粒薄层表面细致密集，表面光洁度好。铁电体元件在压电性能方面也是优异的，因此可以有利地用作压电喷墨头中的压电元件。

9. 发明授权

US06336716B1 Ferroelectric element, process for producing the same, and ink jet head 失效
标题翻译：铁电元件，其制造方法和喷墨头
公开(公告)号：US06336716B1
公开(公告)日：2002-01-08
申请号：US09499688
申请日：2000-02-08
申请人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
发明人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
IPC分类号： B41J2045
CPC分类号： B41J2/14233 , B41J2202/03 , C23C18/1216 , C23C18/1254 , H01L41/1876 , H01L41/318
摘要： A ferroelectric element, including a ferroelectric material containing at least two metals, the ferroelectric element having been produced by a process including the steps of: providing alkoxides of the respective metals as starting compounds; hydrolyzing the metal alkoxides in the presence of a catalytic amount of a protonic acid to increase the molecular weight; and adding a film-forming polymer material to the sol-like solution prepared in the step of increasing the molecular weight to prepare a sol-like ferroelectric precursor solution. The ferroelectric element can be formed in a thick film form without creating any cracks. It can be advantageously used as a piezoelectric element in a piezoelectric ink jet head.
摘要翻译：铁电元件包括含有至少两种金属的铁电材料，所述铁电元件已经通过包括以下步骤的方法制备：提供各种金属的醇盐作为起始化合物; 在催化量的质子酸存在下水解金属醇盐以提高分子量; 并将成膜聚合物材料添加到在提高分子量的步骤中制备的溶胶状溶液中以制备溶胶状铁电体前体溶液。铁电元件可以形成为厚膜形式而不产生任何裂纹。它可以有利地用作压电喷墨头中的压电元件。

10. 发明授权

US06316866B1 Ferroelectric element and process for producing the same 失效
公开(公告)号：US06316866B1
公开(公告)日：2001-11-13
申请号：US09432230
申请日：1999-11-03
申请人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
发明人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
IPC分类号： H01L41187
CPC分类号： H01L41/318 , C01G25/006 , C01P2002/34 , C01P2002/72 , C01P2002/77 , C01P2004/02 , H01L41/1876 , Y10T29/42 , Y10T29/49002
摘要： A ferroelectric element comprising a ferroelectric material containing at least two metals, the ferroelectric element having been produced by a process including a sol-gel process in the presence of a thickener and/or an association preventive from aqueous solutions of respective salts of the metals. The ferroelectric element is advantageous in that the handling of starting compounds and the production of the ferroelectric element are easy, the storage stability of the starting compound solution is good, the cost is low, the ferroelectric element can be formed as a thin layer, particles on the surface of the thin layer are fine and dense, and, hence, the surface smoothness is good. The ferroelectric element is excellent also in piezoelectric properties and therefore can be advantageously used as a piezoelectric element in a piezoelectric ink jet head.

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