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1. 发明授权

US09353208B2 Method for preparing a sol-gel resin 有权
标题翻译：溶胶 - 凝胶树脂的制备方法
公开(公告)号：US09353208B2
公开(公告)日：2016-05-31
申请号：US14259884
申请日：2014-04-23
申请人： Hexion Inc.
发明人： Stephen W. Arbuckle , Gabriele Badini , John Huggins , Sanjay Gangal
IPC分类号： C08G8/24 , C08J3/12 , C08G8/22
CPC分类号： C08G8/24 , C08G8/22 , C08J3/12 , C08J2361/08 , C08J2361/12 , C08L61/12
摘要： Sol-gel resins can be prepared using one or two-step processes to produce small granules or pellets of resin that are easy to handle. The methods include agitating phenolic compounds and aldehydes in the presence of a catalyst and a solvent. The reactants are brought together over a period of time to avoid an undesirable buildup of heat within the reaction mass. Condensation of the material continues under agitation sufficient to knead the material as it gels. During this gelation, the material begins to form into smaller parts until particles, the shape of granules, are produced. The condensation continues to the degree that the material is no longer capable of sintering during packaging and storage. The material thus made can be easily discharged, packaged, portioned, and further processed.
摘要翻译：溶胶 - 凝胶树脂可以使用一步或两步法制备，以生产易于处理的小颗粒或树脂颗粒。所述方法包括在催化剂和溶剂的存在下搅拌酚类化合物和醛。将反应物在一段时间内聚合在一起，以避免反应物料内不希望的热积聚。材料的冷凝在搅拌下持续，足以在其凝胶时捏合材料。在这种凝胶化过程中，材料开始形成较小的部分，直到产生颗粒的形状。冷凝继续到在包装和储存期间材料不再能够烧结的程度。由此制成的材料可以容易地排出，包装，分割和进一步加工。

2. 发明授权

US09453098B2 Method for preparing a sol-gel resin 有权
标题翻译：溶胶 - 凝胶树脂的制备方法
公开(公告)号：US09453098B2
公开(公告)日：2016-09-27
申请号：US14260142
申请日：2014-04-23
申请人： Hexion Inc.
发明人： Stephen W. Arbuckle , Gabriele Badini , John Huggins , Sanjay Gangal
IPC分类号： C08G8/24 , C08G8/22 , C08L61/12
CPC分类号： C08G8/22 , C08G8/24 , C08L61/12
摘要： Disclosed are processes for preparing sol-gel resins from phenolic compounds and aldehydes. The process includes reacting an hydroxylated benzene and a catalyst with an aldehyde to form a liquid storage stable intermediate. The storage stable intermediate may then be stored for a period of time before being utilized in a process to prepare the sol-gel resin, in either monolith or particle form, by subsequently reacting the intermediate with an hydroxylated benzene and a catalyst.
摘要翻译：公开了从酚类化合物和醛制备溶胶 - 凝胶树脂的方法。该方法包括使羟基化苯和催化剂与醛反应以形成液体储存稳定的中间体。然后可以将储存稳定的中间体储存一段时间，然后在制备溶胶 - 凝胶树脂的方法中以整体或颗粒形式通过随后使中间体与羟基化苯和催化剂反应。

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