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1. 发明授权

US5053421A Di-styrl-phenyl-triglycol ether as crystallization inhibitor 失效
标题翻译： DI-STYRL-PHENYL-TRIGLYCOL醚作为结晶抑制剂
公开(公告)号：US5053421A
公开(公告)日：1991-10-01
申请号：US501692
申请日：1990-03-29
申请人： Heinz-Otto Horstmann , Ulrich Engelhardt , Karl Reizlein , Rolf-Jurgen Singer , Klaus Wangermann , Wolfgang Wirth , Frank Bartkowiak , Gunther Boehmke , Hans Schulze
发明人： Heinz-Otto Horstmann , Ulrich Engelhardt , Karl Reizlein , Rolf-Jurgen Singer , Klaus Wangermann , Wolfgang Wirth , Frank Bartkowiak , Gunther Boehmke , Hans Schulze
IPC分类号： C07D249/08 , A01N25/02 , A01N25/22 , A01N25/30 , A01N31/14 , A01N43/653 , C07C43/23 , C09K3/30
CPC分类号： A01N25/02 , A01N25/22 , Y10S514/971
摘要： In the spraying of an aqueous liquor comprising at least one of 1-(4-chlorophenyl)-4,4-dimethyl-3-(1,2,4-triazol-1-yl-methyl)-pentan-3-ol and 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1,2,4-triazol-1-yl)-butan-2-ol, the improvement which comprises including in the liquor di-styryl-phenyl-tri-glycol ether, whereby crystallization of II and III is reduced.
摘要翻译：在喷雾包含1-（4-氯苯基）-4,4-二甲基-3-（1,2,4-三唑-1-基 - 甲基） - 戊-3-醇中的至少一种和 1-（4-氯苯氧基）-3,3-二甲基-1-（1,2,4-三唑-1-基） - 丁-2-醇的改进包括在二苯乙烯基苯基 - 三乙醇醚，由此降低了II和III的结晶。

2. 发明授权

US5369118A N-alkyl-lactams as crystallization inhibitors 失效
标题翻译： N-烷基 - 内酰胺作为结晶抑制剂
公开(公告)号：US5369118A
公开(公告)日：1994-11-29
申请号：US502369
申请日：1990-03-30
申请人： Karl Reizlein , Ulrich Engelhardt , Heinz-Otto Horstmann , Rolf-Jurgen Singer , Klaus Wangermann , Wolfgang Wirth
发明人： Karl Reizlein , Ulrich Engelhardt , Heinz-Otto Horstmann , Rolf-Jurgen Singer , Klaus Wangermann , Wolfgang Wirth
IPC分类号： A01N25/00 , A01N25/22 , A01N43/653 , C07D249/08 , C07D249/14 , A01N43/64 , C07D249/16
CPC分类号： A01N43/653
摘要： In the spraying of an aqueous liquor comprising at least one of 1-(4-chlorophenyl)-4,4-dimethyl-3-(1,2,4-triazol-1-yl-methyl)-pentan-3-ol and 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1,2,4-triazol-1-yl)-butan-2-ol, the improvement which comprises including in the liquor an N-alkyl-lactam of the formula ##STR1## in which R represents alkyl having 8 to 18 carbon atoms andn represents the numbers 3, 4 or 5,
摘要翻译：在喷雾包含1-（4-氯苯基）-4,4-二甲基-3-（1,2,4-三唑-1-基 - 甲基） - 戊-3-醇中的至少一种和 1-（4-氯苯氧基）-3,3-二甲基-1-（1,2,4-三唑-1-基） - 丁-2-醇的改进包括在该液体中包含N-烷基 - 内酰胺式8至18个碳原子，n表示数3,4或5，

3. 发明授权

US5326573A Coated granules containing liquid and solid active compounds 失效
标题翻译：包含液体和固体活性化合物的包衣颗粒
公开(公告)号：US5326573A
公开(公告)日：1994-07-05
申请号：US23418
申请日：1993-02-23
申请人： Elmar Antfang , Dimitrios Kerimis , Rolf-Jurgen Singer
发明人： Elmar Antfang , Dimitrios Kerimis , Rolf-Jurgen Singer
IPC分类号： A01N25/12 , A01N25/26 , A01N57/00 , A61K9/58 , C08L75/00 , C08L75/04
CPC分类号： A01N25/26 , Y10T428/2991 , Y10T428/2993 , Y10T428/2995 , Y10T428/2998
摘要： In the combating of agricultural and horticultural pests by applying to a locus from which it is desired to exclude such pests a normally liquid active compound and a normally solid active compound, the improvement which comprises applying such active compound in the form of granules comprisinga) carrier granules having a non-absorptive surface,b) at least one liquid active compound and at least one solid active compound,c) at least one adhesive based on polyurethane as a binder, optionally mixed with a further adhesive selected from the group consisting of polyvinyl acetate, polyvinylpyrrolidine, polyvinyl alcohol, vinyl acetate/di-n-butyl maleate copolymers, acrylic acid ester, vinyl acetate/ethylene, vinyl acetate/ethylene/vinyl chloride, vinyl acetate/acrylic acid ester, vinyl acetate/vinyl ester and styrene/acrylic acid ester, andd) optionally an additive.
摘要翻译：在通过应用于希望排除这种害虫的场所防止农业和园艺害虫通常是液体活性化合物和通常固体活性化合物的改进方案包括将这种活性化合物以颗粒形式施用，包括：a）具有非吸收性表面的载体颗粒，b）至少一种液体活性化合物和至少一种固体活性化合物，c）至少一种基于聚氨酯作为粘合剂的粘合剂，任选地与选自以下的另一种粘合剂混合：聚乙酸乙烯酯，聚乙烯吡咯烷酮，聚乙烯醇，乙酸乙烯酯/马来酸二正丁酯共聚物，丙烯酸酯，乙酸乙烯酯/乙烯，乙酸乙烯酯/乙烯/氯乙烯，乙酸乙烯酯/丙烯酸酯，乙酸乙烯酯/乙烯基酯和苯乙烯 /丙烯酸酯，和d）任选的添加剂。

4. 发明授权

US5047243A Carrier granules containing liquid active compounds 失效
标题翻译：含有液体活性化合物的载体颗粒
公开(公告)号：US5047243A
公开(公告)日：1991-09-10
申请号：US461208
申请日：1990-01-05
申请人： Elmar Antfang , Dimitrios Kerimis , Rolf-Jurgen Singer
发明人： Elmar Antfang , Dimitrios Kerimis , Rolf-Jurgen Singer
IPC分类号： A01N25/12 , A01N25/10 , A01N25/26 , A01N57/00 , C08L75/00 , C08L75/04
CPC分类号： A01N25/26 , A01N25/10 , Y10S514/919
摘要： In the combating of agricultural and horticultural pests by applying to a locus from which it is desired to exclude such pests a normally liquid active compound and a normally solid active compound, the improvement which comprises applying such active compound in the form of granules comprisinga) carrier granules having a non-absorptive surface,b) at least one liquid active compound,c) at least one adhesive based on polyurethane as a binder, optionally mixed with a further adhesive selected from the group consisting of polyvinyl acetate, polyvinylpyrrolidine, polyvinyl alcohol, copolymers of vinyl acetate/di-n-butyl maleate, acrylic acid ester, vinyl acetate/ethylene, vinyl acetate/ethylene/vinyl chloride, vinyl acetate/acrylic acid ester, vinyl acetate/vinyl ester and styrene/acrylic acid ester, andd) optionally an additive.
摘要翻译：在通过应用于希望排除这种害虫的场所防止农业和园艺害虫通常是液体活性化合物和通常固体活性化合物的改进方案包括将这种活性化合物以颗粒形式施用，包括：a）具有非吸收性表面的载体颗粒，b）至少一种液体活性化合物，c）至少一种基于聚氨酯作为粘合剂的粘合剂，任选地与选自聚乙酸乙烯酯，聚乙烯吡咯烷酮，聚乙烯醇，乙酸乙烯酯/马来酸二正丁酯，丙烯酸酯，乙酸乙烯酯/乙烯，乙酸乙烯酯/乙烯/氯乙烯，乙酸乙烯酯/丙烯酸酯，乙酸乙烯酯/乙烯基酯和苯乙烯/丙烯酸酯的共聚物，和 d）任选的添加剂。

5. 发明授权

US4309538A Preparation of 4-amino-6-tert.-butyl-3-alkylthio-1,2,4-triazin-5(4H)-ones 失效
标题翻译：制备4-氨基-6-叔丁基-3-烷硫基-1,2,4-三嗪-5（4H） - 酮
公开(公告)号：US4309538A
公开(公告)日：1982-01-05
申请号：US227442
申请日：1981-01-22
申请人： Thomas Schmidt , Andreas Wittig , Hans-Peter Sehnem , Hans Kratzer , Rolf-Jurgen Singer
发明人： Thomas Schmidt , Andreas Wittig , Hans-Peter Sehnem , Hans Kratzer , Rolf-Jurgen Singer
IPC分类号： C07D253/07 , C07D253/075 , C07D253/06
CPC分类号： C07D253/075 , C07D253/07
摘要： In the preparation of 4-amino-6-tert.-butyl-3-alkylthio-1,2,4-triazin-5(4H)-ones of the formula ##STR1## wherein (a) pivaloyl cyanide of the formula(CH.sub.3).sub.3 C--CO--CNis converted to a derivative of trimethylpyruvic acid, (b) the derivative is condensed with thiocarbohydrazide of the formulaH.sub.2 N--NH--CS--NH--NH.sub.2to form 4-amino-6-tert.-butyl-3-mercapto-1,2,4-triazin-5(4H)-one, and (c) that is alkylated to form the indicated end products, the improvement which comprises effecting (a) by reacting the pivaloyl cyanide with a strong anhydrous inorganic acid at about -50.degree. to +50.degree. C. thereby to form trimethylpyruvic acid amide. The derivative in (a) can be trimethylpyruvic acid amide or it may first be saponified to the free acid. The inorganic acid in (a) can be hydrochloric or hydrobromic acid in glacial acetic acid, or it can be concentrated sulphuric acid plus some chloride ion and followed by water. Trimethyl pyruvic acid amide is a new compound.
摘要翻译：在制备式（IMA）的4-氨基-6-叔丁基-3-烷硫基-1,2,4-三嗪-5（4H） - 酮的方法中，其中（a）式（CH3）的新戊酰氰）将3C-CO-CN转化为三甲基丙酮酸的衍生物，（b）将该衍生物与式H2N-NH-CS-NH-NH 2的硫代碳酰肼缩合形成4-氨基-6-叔丁基-3 - 巯基-1,2,4-三嗪-5（4H） - 酮，和（c）烷基化形成指定的最终产物，其改进包括通过使新戊酰氰与强无机无机无机酸在约-50℃至+ 50℃，从而形成三甲基丙酮酸酰胺。（a）中的衍生物可以是三甲基丙酮酸酰胺，或者它可以首先被皂化成游离酸。（a）中的无机酸可以是冰醋酸中的盐酸或氢溴酸，也可以是浓硫酸加一些氯离子，然后是水。三甲基丙酮酸酰胺是一种新的化合物。

6. 发明授权

US4006186A Process for the preparation of thiophenols 失效
标题翻译：制备苯硫酚的方法
公开(公告)号：US4006186A
公开(公告)日：1977-02-01
申请号：US466312
申请日：1974-05-02
申请人： Hans Dieter Engels , Rolf-Jurgen Singer
发明人： Hans Dieter Engels , Rolf-Jurgen Singer
IPC分类号： C07C149/00 , C07C149/12
CPC分类号： C07C323/00
摘要： Process for the production of thiophenols of the formula ##STR1## in which N IS AN INTEGER FROM 0 TO 5, INCLUSIVE, ANDR is hydroxy, nitro, halogen, alkyl of from 1 to 6 carbon atoms, alkoxy of from 1 to 6 carbon atoms, amino, monoalkylamino or dialkylamino.Which process comprises reacting, in a first step, the corresponding phenylsulfonic acid chloride with hydrazine, hydriodic acid and hydrochloric acid to give the corresponding sulfonehydrazide; and reacting the product so formed, in the second step, to give the corresponding disulfide; and then splitting the resulting material, in the third step, with hydrazine and alkali to form a thiophenolate from which the thiophenol can be liberated by treatment with a mineral acid.
摘要翻译：制备其中N为0至5，包含和R 1的整数的式（I）的苯硫酚的方法是羟基，硝基，卤素，1至6个碳原子的烷基，1的烷氧基至6个碳原子，氨基，单烷基氨基或二烷基氨基。

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