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1. 发明授权

US5534638A Bis(ethylenedithio)tetrathiafulvalene.cyanometalate complex 失效
标题翻译：双（亚乙基二硫）四硫富瓦烯氰化金属络合物
公开(公告)号：US5534638A
公开(公告)日：1996-07-09
申请号：US429009
申请日：1995-04-26
申请人： Hatsumi Mori , Izumi Hirabayashi , Shoji Tanaka , Takehiko Mori , Yusei Maruyama , Hiroo Inokuchi
发明人： Hatsumi Mori , Izumi Hirabayashi , Shoji Tanaka , Takehiko Mori , Yusei Maruyama , Hiroo Inokuchi
IPC分类号： C07D519/00 , C07F15/00 , C07F15/04 , H01L39/12 , C07D409/04
CPC分类号： C07D519/00 , C07F15/006 , C07F15/0066 , C07F15/0086 , C07F15/0093 , C07F15/04 , C07F15/045 , H01L39/121 , Y10S505/811
摘要： This describes the following five novel organic substances: Bis (ethylenedithio) tetrathiafulvalene (henceforth to be called BEDT-TTF) compounded with cyanometalate anions in what is called Tetracyano Nickel acid Bis (Ethylenedithio) Tetrathiafulvalene salt.hydrate expressed by (BEDT-TTF).sub.4 [Ni(CN).sub.4 ].H.sub.2 O, Tetracyano Platinum acid Bis (Ethylenedithio) Tetrathiafulvalene salt.hydrate that is expressed by (BEDT-TTF).sub.4 [Pt(CN).sub.4 ].H.sub.2 O, Cyanide Palladium Bis (Ethylenedithio) Tetrathiafulvalene salt that is expressed by (BEDT-TTF)-[Pd(CN).sub.2 ], Tetracyano Palladium acid Bis (Ethylenedithio) Tetrathiafulvalene salt.hydrate that is expressed by (BEDT-TFF).sub.4 [Pd(CN).sub.4 ].H.sub.2 O and Tetracyano Palladium acid Bis (Ethylenedithio) Tetrathiafulvalene salt that is represented by (BEDT-TTF).sub.4 [Pd(CN).sub.4 ]. BEDT-TTF, acting as a common constituent in the crystals of all of the above substances, provides the properties of an insulator, a metal or a superconductor. Anions that construct the framework of BEDT-TTF determine the arrangement of BEDT-TTF and thus the electronic state of the compound. It can be predicted that superconducting phenomena could be discovered in compounds of BEDT-TTF type in which there are compounded cyanometalate anions that have the tendency to form large frameworks so that the effective volume is large as in the case of the novel substances of the present invention.
摘要翻译：这描述了以下五种新型有机物质：由（BEDT-TTF）4表示的所谓的四氰基镍酸双（乙二硫）四硫富瓦烯盐水合物与氰化金属阴离子复合的双（亚乙基二硫）四硫富瓦烯（以下称为BEDT-TTF）由[BEDT-TTF] 4 [Pt（CN）4]·H 2 O，氰化物钯双（亚乙基二硫）四硫富瓦烯盐表示的四硫代双（亚乙基二硫）四硫富瓦烯盐水合物，[Ni（CN）4]·H 2 O，由（BEDT-TFF）4 [Pd（CN）4]·H 2 O和四氰基钯表示的（BEDT-TTF） - [Pd（CN）2]，四氰基钯酸双（亚乙基二硫）四硫富瓦烯盐水合物由（BEDT-TTF）4 [Pd（CN）4]表示的酸性双（亚乙基二硫）四硫富瓦烯盐。作为所有上述物质的晶体中的共同成分的BEDT-TTF提供绝缘体，金属或超导体的性质。构建BEDT-TTF框架的阴离子决定了BEDT-TTF的排列以及化合物的电子状态。可以预测，在具有复合的氰化金属阴离子的BEDT-TTF型化合物中可以发现超导现象，其具有形成大框架的趋势，使得有效体积大，如在本发明的新物质的情况下发明。

2. 发明授权

US5276012A Laser-assisted CVD process forming oxide superconducting films 失效
标题翻译：激光辅助CVD工艺形成氧化物超导薄膜
公开(公告)号：US5276012A
公开(公告)日：1994-01-04
申请号：US833509
申请日：1992-02-11
申请人： Takahisa Ushida , Kazutoshi Higashiyama , Izumi Hirabayashi , Shoji Tanaka
发明人： Takahisa Ushida , Kazutoshi Higashiyama , Izumi Hirabayashi , Shoji Tanaka
IPC分类号： H01L39/24 , B05D3/06 , C23C16/00
CPC分类号： H01L39/2441 , Y10S505/73 , Y10S505/734
摘要： A method is disclosed of forming an oxide superconducting film comprising the steps of (1) mixing (a) the vapors of organic metal materials in such proportions as to provide a predetermined metal composition, or (b) said organic metal materials in such proportions as to provide a predetermined metal composition vaporizing and mixture, and (2) bringing the mixture into contact with a heated substrate so that an oxide superconducting film is formed on said substrate by a chemical vapor deposition process, wherein laser light is applied onto said substrate during formation of said oxide superconducting film on said substrate, whereby the crystallographic orientation of said oxide superconducting film being formed in the irradiated area of said substrate is such that the c-axis is parallel to the substrate.
摘要翻译：公开了一种形成氧化物超导膜的方法，包括以下步骤：（1）将（a）有机金属材料的蒸气以提供预定金属组合物的比例混合，或（b）所述有机金属材料的比例如以提供预定的金属组合物蒸发和混合，和（2）使混合物与加热的基底接触，使得通过化学气相沉积工艺在所述基底上形成氧化物超导膜，其中在所述基底上施加激光在所述衬底上形成所述氧化物超导膜，由此在所述衬底的照射区域中形成的所述氧化物超导膜的结晶取向使得c轴平行于衬底。

3. 发明授权

US5190913A Apparatus for producing superconducting oxide film 失效
标题翻译：用于生产超导氧化膜的装置
公开(公告)号：US5190913A
公开(公告)日：1993-03-02
申请号：US857272
申请日：1992-03-25
申请人： Kazutoshi Higashiyama , Takahisa Ushida , Izumi Hirabayashi , Shoji Tanaka
发明人： Kazutoshi Higashiyama , Takahisa Ushida , Izumi Hirabayashi , Shoji Tanaka
IPC分类号： C23C16/30 , C23C16/40 , C23C16/44 , C23C16/448 , C23C16/455 , C23C16/52 , C30B25/14
CPC分类号： C23C16/45561 , C23C16/408 , C23C16/448 , C23C16/52 , Y10S505/73 , Y10S505/734 , Y10S505/786
摘要： An apparatus for producing a superconducting oxide film with stable properties by metal organic chemical vapor deposition, suitable for mass production, is provided with a gas analyzer comprising a differential pressure meter 38 between a raw material gas collector tube 35 provided in a transfer line 8 for leading a raw material gas to a film forming chamber 10 and a bypass line 37, a dilution gas line 49 interlocked with the differential pressure meter 38 and for leading a dilution gas to the raw material gas collector tube 35, a gas separation column 42 branched from the bypass line, a gas detector 31 connected to the gas separation column 42, flow rate controllers 50 for carrier gases 43 and 45 and a thermostat 13 for heating all the lines. Amounts of raw materials gases can be readily measured and controlled and thus superconducting oxide films of stable properties in a constant metal composition ratio can be continuously produced, and thus the present apparatus is suitable for mass production of tape form, superconducting materials.

4. 发明授权

US5849670A Thallium group superconducting wire 失效
标题翻译：铊组超导线
公开(公告)号：US5849670A
公开(公告)日：1998-12-15
申请号：US572748
申请日：1995-12-14
申请人： Toshihide Nabatame , Junichi Kawashima , Izumi Hirabayashi , Yuh Shiobara , Shoji Tanaka
发明人： Toshihide Nabatame , Junichi Kawashima , Izumi Hirabayashi , Yuh Shiobara , Shoji Tanaka
IPC分类号： C04B35/45 , C01G1/00 , C01G15/00 , H01B12/04 , H01B12/10 , H01F6/06 , H01L39/14 , H01L39/24 , H01B12/00
CPC分类号： H01L39/143 , H01L39/2425 , H01L39/2458 , Y10S428/93 , Y10S505/704 , Y10S505/705 , Y10T428/2929
摘要： In order to provide a crystal oriented high quality thallium group superconducting wire having a high critical current density, thallium group superconducting film is formed on oxide single crystal fiber having plane facets and polygonal cross section in the thallium group superconducting wire, wherein c-axis of the thallium group superconducting film is oriented perpendicularly, and a- and b-axis are oriented in parallel to the longitudinal direction of the above fiber, respectively, and resulting to obtain a high quality thallium group superconducting wire with Jc of 10.sup.5 A/cm.sup.2 or more at 77K.
摘要翻译：为了提供具有高临界电流密度的晶体取向的高品质铊族超导线，在铊族超导线中具有平面和多边形横截面的氧化物单晶纤维上形成铊基超导膜，其中c轴铊组超导膜垂直取向，a轴和b轴分别与上述纤维的纵向平行取向，得到JC为105A / cm2的高品质铊基超导线，或更多在77K。

5. 发明授权

US5284822A Oxide superconductor and process for producing the same 失效
标题翻译：氧化物超导体及其制造方法
公开(公告)号：US5284822A
公开(公告)日：1994-02-08
申请号：US695813
申请日：1991-05-07
申请人： Takenobu Sakai , Kozi Nishio , Naoyuki Ogawa , Izumi Hirabayashi , Shoji Tanaka
发明人： Takenobu Sakai , Kozi Nishio , Naoyuki Ogawa , Izumi Hirabayashi , Shoji Tanaka
IPC分类号： C04B35/00 , C01G1/00 , C01G3/00 , C04B35/45 , C04B35/653 , H01B12/10 , H01B13/00 , H01L39/12 , H01L39/24 , H01L39/00
CPC分类号： C04B35/4512 , C04B35/4504 , C04B35/4508 , C04B35/653 , H01L39/126 , Y10S428/93 , Y10S505/729 , Y10S505/785
摘要： Disclosed are an oxide superconductor, and an optimum process for producing the same. The oxide superconductor comprises a base material phase including an oxide superconducting material, the oxide superconducting material including barium (Ba) at least and being free from grain boundaries, and precipitation phases contained in an amount of 1 to 50% by volume in the base material phase and dotted therein in a manner like islands, the precipitation phases being oxides of a metal selected from the group consisting of silicon (Si), aluminum (Al), zirconium (Zr), magnesium (Mg), titanium (Ti), strontium (Sr), tungsten (W), cobalt (Co) and vanadium (V), and being products of decomposition reaction of the base material phase. In the production process, the constituent materials are treated thermally at a partially melting temperature in order to give the above-described novel structure to the oxide superconductor. Thus, the precipitation phases are dotted in a manner like islands in a sea of the base material phase being free from the grain boundaries, and the precipitation phases work as the pinning centers. Therefore, the oxide superconductor exhibits a high "Jc" value.
摘要翻译：公开了一种氧化物超导体及其制造方法。氧化物超导体包括含有氧化物超导材料的基体材料相，氧化物超导材料至少包含钡（Ba）并且不含晶界，沉淀相在基材中的含量为1〜50体积％相，点状，析出相为选自硅（Si），铝（Al），锆（Zr），镁（Mg），钛（Ti），锶等的金属的氧化物（Sr），钨（W），钴（Co）和钒（V），并且是基材相分解反应的产物。在制造工序中，在部分熔融温度下对构成材料进行热处理，以使氧化物超导体具有上述新颖的结构。因此，沉淀相以基材相的海中的岛离开晶界的方式点着，沉淀相作为钉扎中心起作用。因此，氧化物超导体表现出高的“Jc”值。

6. 发明授权

US06610632B2 Tape-formed oxide superconductor 有权
标题翻译：带状氧化物超导体
公开(公告)号：US06610632B2
公开(公告)日：2003-08-26
申请号：US09974972
申请日：2001-10-12
申请人： Tetsuji Honjo , Hiroshi Fuji , Yuichi Nakamura , Teruo Izumi , Takeshi Araki , Yutaka Yamada , Izumi Hirabayashi , Yuh Shiohara , Yasuhiro Iijima , Kaoru Takeda
发明人： Tetsuji Honjo , Hiroshi Fuji , Yuichi Nakamura , Teruo Izumi , Takeshi Araki , Yutaka Yamada , Izumi Hirabayashi , Yuh Shiohara , Yasuhiro Iijima , Kaoru Takeda
IPC分类号： B32B100
CPC分类号： H01L39/2461 , H01L39/2425
摘要： The present invention provides a tape-form oxide superconductor having a high degree of c-axis alignment and in-plane alignment and an improved Jc value. On a tape-form metal substrate which is non-magnetic or weakly magnetic and has high strength, there are sequentially formed a first intermediate layer wherein YSZ or Zr2Rx2O7 particles are deposited from a target with ion irradiation from a direction inclined to the metal substrate, a second intermediate layer of CeO2 or Y2O3 is formed and an RE1+XBa2−XCu3OY superconducting layer is formed by coating metalorganic salts containing F, followed by thermal decomposition.
摘要翻译：本发明提供具有高度c轴对准和面内对准的带状氧化物超导体和改进的Jc值。在非磁性或弱磁性并且具有高强度的带状金属基材上，依次形成第一中间层，其中YSZ或Zr2Rx2O7颗粒从靶向与金属基底倾斜的方向进行离子辐射沉积，形成CeO 2或Y 2 O 3的第二中间层，并且通过涂覆含有F的金属有机盐然后热分解形成RE1 + XBa2-XCu3OY超导层。

7. 发明授权

US5962374A Preparation of oxide crystals 失效
标题翻译：氧化物晶体的制备
公开(公告)号：US5962374A
公开(公告)日：1999-10-05
申请号：US27065
申请日：1998-02-20
申请人： Yuusuke Niiori , Yasuji Yamada , Junichi Kawashima , Izumi Hirabayashi
发明人： Yuusuke Niiori , Yasuji Yamada , Junichi Kawashima , Izumi Hirabayashi
IPC分类号： C01G1/00 , C01G3/00 , C30B7/08 , C30B9/00 , H01L39/24 , C30B9/12 , C04B35/653 , C30B15/00
CPC分类号： C30B29/225 , C30B9/00 , Y10S505/729
摘要： A process for preparing an oxide crystal by means of solution growth in the presence of a solvent is provided. The solvent includes a mixture of an oxide containing at least one member of those elements which constitute the oxide crystal, a halide containing at least one member of those elements which constitute the oxide crystal, and metallic silver.
摘要翻译：提供了在溶剂存在下通过溶液生长制备氧化物晶体的方法。溶剂包括含有构成氧化物晶体的那些元素中的至少一种元素的氧化物，包含构成氧化物晶体的元素中的至少一种的卤化物和金属银的混合物。

8. 发明授权

US5496799A Method for making rare earth superconductive composite 失效
标题翻译：制备稀土超导复合材料的方法
公开(公告)号：US5496799A
公开(公告)日：1996-03-05
申请号：US366384
申请日：1994-12-29
申请人： Manabu Yoshida , Izumi Hirabayashi
发明人： Manabu Yoshida , Izumi Hirabayashi
IPC分类号： C01G1/00 , C01G3/00 , C04B35/00 , C04B35/45 , C04B35/653 , H01B12/00 , H01B13/00 , H01L39/24
CPC分类号： C04B35/4508 , C04B35/653 , H01L39/2483
摘要： A method for making a rare earth superconductive composite which includes a matrix of REBa.sub.2 Cu.sub.3 O.sub.7-x grains and fine particles of RE.sub.2 BaCuO.sub.5 dispersed therein. The method includes a step of forming a compacted mass of powder particles of REBa.sub.2 Cu.sub.3 O.sub.7-x and powder particles of RE.sub.2 BaCuO.sub.5, each of which has an average diameter not greater than 6 .mu.m, and a maximum diameter not greater than 20 .mu.m. The compacted mass is heated to temperature higher than an incongruent melting temperature of the REBa.sub.2 Cu.sub.3 O.sub.7-x and lower than an incongruent melting temperature of RE.sub.2 BaCuO.sub.5, and is gradually cooled such that fine particles of RE.sub.2 BaCuO.sub.5 are dispersed in REBa.sub.2 Cu.sub.3 O.sub.7-x grains. The mass is annealed in an atmosphere containing oxygen.
摘要翻译：一种制备稀土超导复合材料的方法，其包括REBa2Cu3O7-x晶粒的基体和分散在其中的RE2BaCuO5的细颗粒。该方法包括形成REBa2Cu3O7-x粉末颗粒和RE2BaCuO5粉末颗粒的压实块的平均直径不大于6μm，最大直径不大于20μm的步骤。将压实的物料加热到高于REBa2Cu3O7-x的不一致熔融温度并低于RE2BaCuO5的不一致熔融温度的温度，并逐渐冷却，使得RE2BaCuO5的细颗粒分散在REBa2Cu3O7-x颗粒中。质量在含氧的气氛中退火。

9. 发明授权

US07732376B2 Oxide superconducting film and method of preparing the same 有权
标题翻译：氧化物超导薄膜及其制备方法
公开(公告)号：US07732376B2
公开(公告)日：2010-06-08
申请号：US12550445
申请日：2009-08-31
申请人： Takeshi Araki , Koichi Nakao , Izumi Hirabayashi
发明人： Takeshi Araki , Koichi Nakao , Izumi Hirabayashi
IPC分类号： H01B1/12 , H01L39/24
CPC分类号： C23C18/1216 , C23C18/1254 , C23C18/1279 , C23C18/1283 , H01L39/2425 , Y10T428/265
摘要： The present invention relates to a method of preparing an oxide superconducting film, the method includes reacting a metal acetate containing metal M selected from the group consisting of lanthanum, neodymium and samarium with fluorocarboxylic acid having not less than three carbon atoms, reacting barium acetate with fluorocarboxylic acid having two carbon atoms, reacting copper acetate with fluorocarboxylic acid having not less than two carbon atoms, respectively, followed by refining reaction products, dissolving the reaction products in methanol such that a molar ratio of the metal M, barium and copper is 1:2:3 to prepare a coating solution, and coating a substrate with the coating solution to form a gel film, followed by calcining and firing the gel film to prepare an oxide superconducting film.
摘要翻译：本发明涉及一种制备氧化物超导膜的方法，该方法包括使选自镧，钕和钐的金属乙酸盐与含有不少于3个碳原子的氟代羧酸反应，使乙酸钡与具有两个碳原子的氟代羧酸，分别使乙酸铜与不少于2个碳原子的氟代羧酸反应，然后精制反应产物，将反应产物溶解在甲醇中，使金属M，钡和铜的摩尔比为1 ：2:3以制备涂布溶液，并用涂布溶液涂布基材以形成凝胶膜，然后煅烧和烧结凝胶膜以制备氧化物超导膜。

10. 发明授权

US07361627B2 Method of preparing oxide superconducting film 有权
标题翻译：制备氧化物超导薄膜的方法
公开(公告)号：US07361627B2
公开(公告)日：2008-04-22
申请号：US11354970
申请日：2006-02-16
申请人： Takeshi Araki , Koichi Nakao , Izumi Hirabayashi
发明人： Takeshi Araki , Koichi Nakao , Izumi Hirabayashi
IPC分类号： H01B12/00 , H01L39/12 , B05D5/12
CPC分类号： C23C18/1216 , C23C18/1254 , C23C18/1279 , C23C18/1283 , H01L39/2425 , Y10T428/265
摘要： The present invention relates to a method of preparing an oxide superconducting film, the method includes reacting a metal acetate containing metal M selected from the group consisting of lanthanum, neodymium and samarium with fluorocarboxylic acid having not less than three carbon atoms, reacting barium acetate with fluorocarboxylic acid having two carbon atoms, reacting copper acetate with fluorocarboxylic acid having not less than two carbon atoms, respectively, followed by refining reaction products, dissolving the reaction products in methanol such that a molar ratio of the metal M, barium and copper is 1:2:3 to prepare a coating solution, and coating a substrate with the coating solution to form a gel film, followed by calcining and firing the gel film to prepare an oxide superconducting film.
摘要翻译：本发明涉及一种制备氧化物超导膜的方法，该方法包括使选自镧，钕和钐的金属乙酸盐与含有不少于3个碳原子的氟代羧酸反应，使乙酸钡与具有两个碳原子的氟代羧酸，分别使乙酸铜与不少于2个碳原子的氟代羧酸反应，然后精制反应产物，将反应产物溶解在甲醇中，使金属M，钡和铜的摩尔比为1 ：2:3以制备涂布溶液，并用涂布溶液涂布基材以形成凝胶膜，然后煅烧和烧结凝胶膜以制备氧化物超导膜。

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