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1. 发明授权

US5394931A Aluminum-based alloy cast product and process for producing the same 失效
标题翻译：铝基合金铸造产品及其制造方法
公开(公告)号：US5394931A
公开(公告)日：1995-03-07
申请号：US119066
申请日：1993-11-08
申请人： Haruo Shiina , Nobuhiro Saito , Takeyoshi Nakamura
发明人： Haruo Shiina , Nobuhiro Saito , Takeyoshi Nakamura
IPC分类号： B22D17/00 , B22D23/00
CPC分类号： B22D17/007 , Y10S164/90
摘要： A process for producing an aluminum-based alloy cast product, includes the steps of: preparing a casting material having an aluminum-based hypo-eutectic alloy composition with solid and liquid phases coexisting therein; and subjecting the casting material to a casting under pressure. At this casting step, the casting material is passed through a gate in a casting mold under conditions of a viscosity .mu. in a range of 0.1 Pa.multidot.sec.ltoreq..mu..ltoreq.2,000 Pa.multidot.sec and a Reynolds number in a range of Re.ltoreq.1,500.
摘要翻译： PCT No.PCT / JP93 / 00030 Sec。 371日期：1993年11月8日 102（e）日期1993年11月8日PCT提交1993年1月12日PCT公布。公开号WO / 9313895 日期：1993年7月22日。一种铝基合金铸造产品的制造方法，包括以下步骤：制备具有固相和液相共存的铝基低共熔合金组合物的铸造材料; 并在压力下对铸造材料进行铸造。在该铸造步骤中，铸造材料通过铸模中的浇口，其粘度μ在0.1Pa·s·秒-2000 Paxsec的范围内，并且在Re的范围内的雷诺数， 1,500。

2. 发明授权

US5925199A Process for producing a thixocast semi-molten material 失效
标题翻译：生产触变半熔融材料的方法
公开(公告)号：US5925199A
公开(公告)日：1999-07-20
申请号：US755296
申请日：1996-11-22
申请人： Haruo Shiina , Nobuhiro Saito , Takeyoshi Nakamura
发明人： Haruo Shiina , Nobuhiro Saito , Takeyoshi Nakamura
IPC分类号： B22D18/02 , B22D17/00 , B22D17/30 , B22D27/09 , C22B9/16 , C22C1/00 , C22C1/02 , C22C21/02 , B22D27/02 , B22D27/04 , C22F1/00
CPC分类号： C22C1/005 , B22D17/007 , B22D17/30 , Y10S164/90
摘要： Solid and liquid phases coexist in a semi-molten casting material. A plurality of composite-solid phases having liquid and solid phase regions and a plurality of single-solid phases exist as the solid phases in a mixed state in an outer layer portion of the semi-molten casting material. If the sectional area of the solid phase region is represented by A, and the sectional area of the solid phase region is represented by B in one of the composite-solid phases, the liquid phase enclosure rate P of the composite-solid phase is defined as being represented by P={B/(A+B)}.times.100 (%). The liquid phase enclosure rate P of the single-solid phase is equal to 0 (%). When two groups are selected from a class of the solid phases, for example, by first and second straight lines so as to include a plurality of the solid phases, average values M.sub.1 and M.sub.2 of liquid phase enclosure rates of, for example, six solid phases in each of the first and second groups are represented by M.sub.1 =(P.sub.1 +P.sub.2 - - - +P.sub.5 +P.sub.6)/6 and M.sub.2 =(P.sub.7 +P.sub.8 - - - +P.sub.11 +P.sub.12)/6, and an average value M.sub.M of the average values M.sub.1 and M.sub.2 is set in a range of M.sub.M .gtoreq.20%. This inhibits the flow-out of the liquid phases from the outer layer portion in the thixocast semi-molten casting material.
摘要翻译：固体和液相在半熔融铸造材料中共存。在半熔融铸造材料的外层部分中，以混合状态存在多个具有液相和固相区域以及多个单相固相的复相固相。如果固相区域的截面积由A表示，并且固相区域的截面积在复合固相之一中由B表示，则复合固相的液相封闭率P被定义由P = {B /（A + B）}×100（％）表示。单相固相的液相封闭率P等于0（％）。当从一类固相中选择两组时，例如通过第一和第二直线选择包括多个固相，液相封装速率的平均值M1和M2例如为六个固体第一组和第二组中的每一个的相位由M1 =（P1 + P2 - - + P5 + P6）/ 6和M2 =（P7 + P8 - - + P11 + P12）/ 6表示，平均值将平均值M1和M2的MM设置在MM> / = 20％的范围内。这就抑制了在thixocast半熔融铸造材料中从外层部分流出的液相。

3. 发明授权

US5849115A Alloy material for thixocasting, process for preparing semi-molten alloy material for thixocasting and thixocasting process 失效
标题翻译：用于触媒的合金材料，用于制备用于触变和触变过程的半熔融合金材料的方法
公开(公告)号：US5849115A
公开(公告)日：1998-12-15
申请号：US861265
申请日：1997-05-21
申请人： Haruo Shiina , Nobuhiro Saito , Takeyoshi Nakamura , Takeshi Sugawara
发明人： Haruo Shiina , Nobuhiro Saito , Takeyoshi Nakamura , Takeshi Sugawara
IPC分类号： C22C1/00 , G01N33/20 , B22D21/00
CPC分类号： C22C1/005 , G01N33/20 , Y10S164/90
摘要： A differential thermal analysis thermograph for a thixocasting aluminum alloy material is such that, a relationship, E.sub.1 >E.sub.2, is established between a peak value E.sub.1 of a first angled endothermic section generated by eutectic melting and a peak value E.sub.2 of a second angled endothermic section generated by melting of an element having a melting point higher than the eutectic point. Thus, a liquid phase produced by the eutectic melting has a large latent heat due to the fact that the peak value E.sub.1 of the first angled endothermic section is larger than the peak value E.sub.2 of the second angled endothermic section in a semi-molten eutectic aluminum alloy material derived from the thixocasting aluminum alloy material. As a result, in a solidification step of the thixocasting process, a liquid phase produced by the eutectic melting is sufficiently fed around a solid phase in response to the solidification and shrinkage of the solid phase, and then solidified. Thus, it is possible to produce a casting free from defects such as voids on the order of a micron.
摘要翻译：用于触媒铝合金材料的差示热分析热成像仪是这样的，即通过由共晶熔融产生的第一倾斜吸热部分的峰值E1与第二成角度吸热部分的峰值E2之间建立关系E1> E2 通过熔点高于共晶点的熔点而产生。因此，由于第一成角度吸热部的峰值E1大于半熔融共晶铝中的第二倾斜吸热部的峰值E2，所以由共晶熔融产生的液相具有大的潜热衍生自thixocasting铝合金材料的合金材料。结果，在固化步骤中，通过共晶熔融产生的液相，以固相的固相和收缩为固相充分地进料，然后固化。因此，可以生产没有诸如微米级的空隙的缺陷的铸件。

4. 发明授权

US5993572A Thixocasting process, and thixocasting aluminum alloy material 失效
标题翻译： Thixocasting工艺，和thixocasting铝合金材料
公开(公告)号：US5993572A
公开(公告)日：1999-11-30
申请号：US728435
申请日：1996-10-09
申请人： Nobuhiro Saito , Haruo Shiina , Takeyoshi Nakamura , Takeshi Sugawara , Kazuo Kikawa
发明人： Nobuhiro Saito , Haruo Shiina , Takeyoshi Nakamura , Takeshi Sugawara , Kazuo Kikawa
IPC分类号： C22C1/00 , C22C21/00
CPC分类号： C22C1/005
摘要： In a thixocasting process, the following steps are used: a step of subjecting, to a heating treatment, an Al-Si based alloy material having a hypo eutectic crystal composition and a characteristic that a first angled endothermic section appearing due to the melting of a eutectic crystal and a second angled endothermic section appearing due to the melting of a component having a melting point higher than a eutectic point exist in a differential calorimetric curve, thereby preparing a semi-molten Al-Si based alloy material having solid and liquid phases coexisting therein; a step of pouring the semi-molten Al-Si based alloy material into a cavity in a casting mold under pressure; and a step of solidifying the semi-molten Al-Si based alloy material under pressure. When the temperature of a rise-start point in the first angled endothermic section is represented by T.sub.1, and the temperature of a drop-end point the first angled endothermic sections is represented by T.sub.2, the casting temperature T for the semi-molten Al-Si based alloy material is set in a range of T.sub.1 .ltoreq.T.ltoreq.T.sub.2. Thus, the fine precipitation of a primary crystal Si phase can be realized to provide an increase in strength of an aluminum alloy cast product.
摘要翻译：在触媒处理中，使用以下步骤：对具有低共晶组成的Al-Si系合金材料进行加热处理的步骤，以及由于熔融而形成的第一成角度的吸热部由于熔点高于共晶点的熔点高于共晶点而出现的共晶晶体和第二倾斜的吸热部分存在于差示热量曲线中，从而制备具有固相和液相的半熔融Al-Si基合金材料共存其中将半熔融的Al-Si基合金材料在压力下浇注到铸模中的空腔中的步骤; 以及在压力下使半熔融Al-Si系合金材料凝固的工序。当第一倾斜吸热部分中的起始点的温度由T1表示，并且下降端点的温度将第一倾斜吸热部分表示为T2时，半熔融Al- Si基合金材料设定在T1

5. 发明授权

US4989556A Valve spring retainer for valve operating mechanism for internal combustion engine 失效
标题翻译：用于内燃机的阀门操作机构的阀弹簧保持器
公开(公告)号：US4989556A
公开(公告)日：1991-02-05
申请号：US414692
申请日：1989-09-28
申请人： Haruo Shiina , Masami Hoshi , Tadayoshi Hayashi
发明人： Haruo Shiina , Masami Hoshi , Tadayoshi Hayashi
IPC分类号： C22C32/00 , F01L3/10
CPC分类号： F01L3/10 , C22C32/00 , C22C32/0036
摘要： A valve spring retainer for a valve operating mechanism for an internal combustion engine comprises a matrix formed from a quenched and solidified aluminum alloy powder, and a hard grain dispersed in said matrix. The hard grain is at least one selected from the group consisting of grains of Al.sub.2 O.sub.3, SiC, Si.sub.3 N.sub.4, ZrO.sub.2, SiO.sub.2, TiO.sub.2, Al.sub.2 O.sub.3 -SiO.sub.2 and metal Si. The amount of hard grain added is in a range of 0.5% to 20% by weight, and the area rate of said hard grain is in a range of from 1% to 6%.

6. 发明授权

US4853179A Method of manufacturing heat resistant, high-strength structural members of sintered aluminum alloy 失效
标题翻译：制造耐热，高强度烧结铝合金结构件的方法
公开(公告)号：US4853179A
公开(公告)日：1989-08-01
申请号：US921999
申请日：1986-10-22
申请人： Haruo Shiina
发明人： Haruo Shiina
IPC分类号： B22F3/02 , B22F3/17 , C22C1/04 , C22C21/02 , C22F1/043
CPC分类号： B21J5/08 , B21K1/766 , C22C1/0416 , C22F1/043
摘要： This invention relates to a method of manufacturing a structural member made of a sintered Al alloy having heat resistance and high strength. A powder is used having a composition which makes it difficult to perform hot forging, i.e. 8.0 to 30.0 wt. % of Si, 0.8 to 7.5 wt. % of Cu, 0.3 to 3.5 wt. % of Mg, 2.0 to 10.0 wt. % of Fe, 0.5 to 5.0 wt. % of Mn, and a balance of Al. After being subjected to press-forming, this Al alloy powder is subjected to hot extrusion at a temperature of 300.degree. to 450.degree. C., the extruded product is heated with electric resistance heating by electric current which is passed therethrough and subjected to forging at a temperature of 300.degree. to 495.degree. C. According to this method, a structural member made of a sintered Al alloy having heat resistance and high strength and having the aforementioned powder composition can be easily obtained without cracking.
摘要翻译：本发明涉及一种制造具有耐热性和高强度的烧结Al合金的结构件的方法。使用具有难以进行热锻造的组合物即8.0〜30.0重量％的粉末。％的Si，0.8〜7.5wt。％的Cu，0.3〜3.5wt。％的Mg，2.0〜10.0wt。％的Fe，0.5〜5.0wt。％的Mn，余量的Al。在进行压制成形之后，将该Al合金粉末在300〜450℃的温度下进行热挤压，通过电流加热，将其挤出，并通过电流加热，并进行锻造温度在300〜495℃。根据该方法，可以容易地获得具有耐热性和高强度并具有上述粉末组成的烧结Al合金的结构件而不会开裂。

7. 发明授权

US6136101A Casting material for thixocasting, method for preparing partially solidified casting material for thixocasting, thixo-casting method, iron-base cast, and method for heat-treating iron-base cast 有权
标题翻译：用于触媒的铸造材料，用于制备部分固化的用于触媒的铸造材料的方法，触变铸造法，铁基铸造和铁基铸造的热处理方法
公开(公告)号：US6136101A
公开(公告)日：2000-10-24
申请号：US77169
申请日：1998-11-09
申请人： Takeshi Sugawara , Haruo Shiina , Masayuki Tsuchiya , Kazuo Kikawa , Isamu Takagi
发明人： Takeshi Sugawara , Haruo Shiina , Masayuki Tsuchiya , Kazuo Kikawa , Isamu Takagi
IPC分类号： B22D17/00 , C21D1/32 , C21D5/00 , C22C37/04 , C22C37/10 , C22C38/02 , C22B38/04 , C22B38/08
CPC分类号： C22C38/02 , B22D17/007 , C21D1/32 , C21D5/00 , C22C37/04 , C22C37/10 , C21D2211/006
摘要： A thixocast casting material is formed of an Fe--C--Si based alloy in which an angle endothermic section due to the melting of a eutectic crystal exists in a latent heat distribution curve and has a eutectic crystal amount Ec in a range of 10% by weight
摘要翻译： PCT No.PCT / JP97 / 03058 Sec。 371日期：1998年11月9日 102（e）日期1998年11月9日PCT 1997年9月2日PCT公布。第WO98 / 10111号公报日期：1998年3月12日一种触变铸造材料由Fe-C-Si基合金形成，其中由于共晶晶体的熔化而导致的角度吸热部分存在于潜热分布曲线中，并且具有共晶晶体量Ec 范围为10重量％

8. 发明授权

US5415710A Heat-resistant aluminum alloy having high fatigue strength 失效
标题翻译：耐疲劳强度高的耐热铝合金
公开(公告)号：US5415710A
公开(公告)日：1995-05-16
申请号：US196643
申请日：1994-02-15
申请人： Haruo Shiina , Fumito Usuzaka , Yoshimasa Ohkubo , Shinichi Tani
发明人： Haruo Shiina , Fumito Usuzaka , Yoshimasa Ohkubo , Shinichi Tani
IPC分类号： B22F3/20 , C22C1/04 , C22C21/02
CPC分类号： C22C21/02 , Y10T428/12028
摘要： The aluminum alloy of the invention has excellent fatigue strength, high rigidity, and low thermal expansion coefficient, and is suitable for rotating components such as conrods in an internal combustion engine. The aluminum alloy is an Al-Si alloy which contains 7.0-12.0% wt. Si, 3.0-6.0 % wt. Cu, 0.20-1.0% wt. Mg, 0.30-1.5% wt. Mn, 0.40-2.0% wt. Ti+V, 0.05-0.5% wt. Zr, and the remainder Al and being inevitable impurities and which contains a dispersed intermetallic compound of average particle size of 0.5 m or less and containing Ti, V, and Zr. The alloy is preferably manufactured by the rapidly solidifying powder metallurgy process, or by the spray-forming process. By selecting a work-hardening exponent of 0.20 or less, the thread rolling workability is improved.
摘要翻译：本发明的铝合金具有优异的疲劳强度，高刚性和低热膨胀系数，适用于内燃机等旋转部件的旋转。铝合金是含有7.0-12.0重量％的Al-Si合金。 Si，3.0-6.0％wt。 Cu，0.20〜1.0重量％ Mg，0.30〜1.5重量％ Mn，0.40-2.0重量％ Ti + V，0.05〜0.5％ Zr，其余为Al，为不可避免的杂质，含有平均粒径为0.5μm以下且含有Ti，V，Zr的分散的金属间化合物。该合金优选通过快速凝固的粉末冶金方法或通过喷射成形方法制造。通过选择0.20以下的加工硬化指数，可以提高线滚动加工性。

9. 发明授权

US4711823A High strength structural member made of Al-alloy 失效
标题翻译：由Al合金制成的高强度结构件
公开(公告)号：US4711823A
公开(公告)日：1987-12-08
申请号：US795586
申请日：1985-11-06
申请人： Haruo Shiina
发明人： Haruo Shiina
IPC分类号： B22F3/24 , C22C1/04 , C22C21/02 , F02F7/00 , C21D1/06 , B22F3/14 , C22C21/04
CPC分类号： F02F7/0085 , C22C1/0416 , Y10T428/12021
摘要： A high strength structural member made of Al-alloy is essentially formed of a sintered body of Al-alloy powder containing Si and Fe in the proportion of 10.ltoreq.Si.ltoreq.30 wt. % and 4.ltoreq.Fe.ltoreq.33 wt. %, and the surface layer of the sintered body is subjected to remelting-solidifying treatment with a high-density energy source such as a laser beam, a plasma arc, a TIG arc, etc. In the treated surface layer of the sintered body, grain sizes of Si crystal grains and precipitated intermetallic compound are reduced to 1 .mu.m or smaller, whereas in the base portion of the sintered body that is not subjected to the remelting-solidifying treatment, grain sizes of Si crystal grains and precipitated intermetallic compound are kept 10 .mu.m or smaller.
摘要翻译：由Al合金制成的高强度结构件基本上由含有Si和Fe的Al合金粉末的烧结体构成，其比例为10％= 30wt。％和4

10. 发明授权

US06527878B1 Thixocast casting material, process for preparing thixocasting semi-molten casting material, thixocast process, fe-based cast product, and process for thermally treating fe-based cast product 有权
标题翻译： Thixocast铸造材料，制备触媒半熔融铸造材料的方法，thixocast工艺，fe基铸造产品和用于热处理基于Fe的铸造产品的方法
公开(公告)号：US06527878B1
公开(公告)日：2003-03-04
申请号：US09669219
申请日：2000-09-25
申请人： Takeshi Sugawara , Haruo Shiina , Masayuki Tsuchiya , Kazuo Kikawa , Isamu Takagi
发明人： Takeshi Sugawara , Haruo Shiina , Masayuki Tsuchiya , Kazuo Kikawa , Isamu Takagi
IPC分类号： C21D500
CPC分类号： C22C38/02 , B22D17/007 , C21D1/32 , C21D5/00 , C21D2211/006 , C22C37/04 , C22C37/10
摘要： A thixocast casting material is formed of an Fe—C—Si based alloy in which an angle endothermic section due to the melting of a eutectic crystal exists in a latent heat distribution curve and has a eutectic crystal amount Ec in a range of 10% by weight
摘要翻译：触变材料铸造材料由Fe-C-Si基合金形成，其中由于共晶晶体的熔化导致的角度吸热部分存在于潜热分布曲线中，并且具有10％的共晶晶体量Ec在10％的范围内重量

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