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1. 发明授权

US4507494A Process for the production of a diester of oxalic acid 失效
标题翻译：用于生产草酸二酯的方法
公开(公告)号：US4507494A
公开(公告)日：1985-03-26
申请号：US460574
申请日：1983-01-24
申请人： Haruhiko Miyazaki , Yasushi Shiomi , Satoru Fujitus , Katsuro Masunaga , Hiroshi Yanagisawa
发明人： Haruhiko Miyazaki , Yasushi Shiomi , Satoru Fujitus , Katsuro Masunaga , Hiroshi Yanagisawa
IPC分类号： C07C69/36 , B01J21/00 , B01J23/00 , C07B61/00 , C07C67/36
CPC分类号： C07C69/36 , Y02P20/582
摘要： In a process for preparing a diester of oxalic acid by the vapor phase catalytic reaction of carbon monoxide with an ester of nitrous acid in the presence of a catalyst composed of a solid carrier and a catalyst component supported on the carrier, the improvement wherein said catalyst component is composed of(a) a platinum-group metal or a salt thereof, and(b) at least one member selected from the group consisting of Ti and an oxide thereof.
摘要翻译：在由固体载体和负载在载体上的催化剂组分的催化剂存在下，通过一氧化碳与亚硝酸酯的气相催化反应制备草酸的方法，其中所述催化剂组分由（a）铂族金属或其盐组成，和（b）选自Ti及其氧化物中的至少一种。

2. 发明授权

US4410722A Process for preparing oxalic acid diesters using platinum group metals supported on alumina 失效
标题翻译：使用负载在氧化铝上的铂族金属制备草酸二酯的方法
公开(公告)号：US4410722A
公开(公告)日：1983-10-18
申请号：US338242
申请日：1982-01-11
申请人： Haruhiko Miyazaki , Yasushi Shiomi , Satoru Fujitus , Katsuro Masunaga , Hiroshi Yanagisawa
发明人： Haruhiko Miyazaki , Yasushi Shiomi , Satoru Fujitus , Katsuro Masunaga , Hiroshi Yanagisawa
IPC分类号： C07C69/00 , C07C69/36 , C07C67/36
CPC分类号： C07C69/36 , B01J23/44 , B01J37/035 , B01J37/16 , Y02P20/582
摘要： In a process for preparing a diester of oxalic acid by the vapor phase catalytic reaction of carbon monoxide with an ester of nitrous acid in the presence of a catalyst composed of a solid carrier and a platinum-group metal or a salt thereof supported on the carrier, the improvement wherein said solid carrier is alumina having a specific surface area of not more than 90 m.sup.2 /g.
摘要翻译：在由固体载体和铂族金属或其负载在载体上的盐的催化剂存在下，通过一氧化碳与亚硝酸酯的气相催化反应来制备草酸的方法其中所述固体载体是比表面积不大于90m 2 / g的氧化铝。

3. 发明授权

US4384133A Process for the preparation of oxalic acid diesters 失效
标题翻译：草酸二酯的制备方法
公开(公告)号：US4384133A
公开(公告)日：1983-05-17
申请号：US340034
申请日：1982-01-18
申请人： Haruhiko Miyazaki , Yasushi Shiomi , Satoru Fujitus , Katsuro Masunaga , Hiroshi Yanagisawa
发明人： Haruhiko Miyazaki , Yasushi Shiomi , Satoru Fujitus , Katsuro Masunaga , Hiroshi Yanagisawa
IPC分类号： C07C69/00 , B01J23/00 , C07B61/00 , C07C69/36 , C07C67/36
CPC分类号： C07C69/36 , Y02P20/582
摘要： In a process for preparing a diester of oxalic acid by the vapor phase catalytic reaction of carbon monoxide with an ester of nitrous acid in the presence of a catalyst composed of a solid carrier and a catalyst component supported on the carrier, the improvement wherein said catalyst component is composed of(a) a platinum-group metal or a salt thereof, and(b) at least one metal selected from the group consisting of Mo and Ni, or a salt thereof.
摘要翻译：在由固体载体和负载在载体上的催化剂组分的催化剂存在下，通过一氧化碳与亚硝酸酯的气相催化反应制备草酸的方法，其中所述催化剂组分由（a）铂族金属或其盐组成，和（b）至少一种选自Mo和Ni的金属或其盐。

4. 发明授权

US4874888A Process for the preparation of a diester of oxalic acid 失效
标题翻译：草酸二酯的制备方法
公开(公告)号：US4874888A
公开(公告)日：1989-10-17
申请号：US546532
申请日：1983-10-28
申请人： Yasushi Shiomi , Tokuo Matsuzaki , Katsuro Masunaga
发明人： Yasushi Shiomi , Tokuo Matsuzaki , Katsuro Masunaga
IPC分类号： B65G67/60 , C07C67/36
CPC分类号： B65G67/606 , C07C67/36 , Y02P20/582
摘要： In a process for preparing a diester of oxalic acid by the vapor phase catlytic reaction of carbon monoxide with an ester of nitrous acid in the presence of a catalyst composed of a solid carrier and a catalyst component supported on the carrier, the improvement wherein said catalyst component is composed of(a) a platinum-group metal or a salt thereof, and(b) at least one member selected from the group consisting of iron and an iron (II or III) compound,the atomic ratio of the component (a) to the component (b) as metal being from 10,000:1 to 1:4.
摘要翻译：在由固体载体和负载在载体上的催化剂组分的催化剂存在下，通过一氧化碳与亚硝酸酯的气相催化反应制备草酸的方法，其中所述催化剂组分由（a）铂族金属或其盐组成，和（b）至少一种选自铁和铁（II或III）化合物的组分，组分（a ）作为金属为10,000:1至1:4的组分（b）。

5. 发明申请

US20060074745A1 Calculation device and method and point or coupon service system 审中-公开
标题翻译：计算装置及方法及点或票务服务系统
公开(公告)号：US20060074745A1
公开(公告)日：2006-04-06
申请号：US10546646
申请日：2003-02-28
申请人： Yasushi Shiomi
发明人： Yasushi Shiomi
IPC分类号： G06Q30/00
CPC分类号： G06Q30/02 , G06Q30/0226
摘要： A point or coupon service system for issuing a point or a coupon for discount in selling a commodity or providing a service and enabling a commodity sales or service provision without defraying any incentive cost. In a point service, when a consumer (3) purchases a particular content sold by a content seller (1), the consumer (3) can receive a discount if he/she has a prepaid royalty point generated when a commodity seller (5) sells a non-particular commodity and can receive a discount when purchasing a non-particular commodity sold by the commodity seller (5) if he/she has a pre-taken royalty point generated when the content seller (1) cells a particular commodity. The content seller (1) receives a sales price as a benefit even when the content is sold at a discount price and does not defray the incentive cost by issuing a point.
摘要翻译：一个点或息票服务系统，用于在销售商品或提供服务时发行折扣或优惠券，并且可以在不支付任何奖励成本的情况下实现商品销售或服务提供。在点服务中，当消费者（3）购买由内容卖方（1）出售的特定内容时，消费者（3）可以在商品卖家（5）具有生成预付版税点时收到折扣，销售非特定商品，并且当购买商品卖家（5）销售的非特定商品时，如果内容卖家（1）对特定商品进行细分，则产生预先购买的特许权使用费点，则可以获得折扣。内容卖方（1）即使以折扣价格出售内容，也不会通过发出点来支付激励成本，因此收到销售价格作为利益。

6. 发明授权

US5648117A Powder coating composition 失效
标题翻译：粉末涂料组合物
公开(公告)号：US5648117A
公开(公告)日：1997-07-15
申请号：US480324
申请日：1995-06-07
申请人： Yasushi Shiomi , Akimitsu Uenaka , Koichi Tsutsui
发明人： Yasushi Shiomi , Akimitsu Uenaka , Koichi Tsutsui
IPC分类号： C08F299/00 , C08F290/00 , C09D5/03 , C09D5/46 , C09D133/00 , C09D133/04 , C09D133/06 , C09D133/14 , C09D163/00 , C09D163/08 , B05D3/02
CPC分类号： C09D133/068 , C09D133/14
摘要： A powder coating composition contains acrylic resin (A) containing at least 40 percent by weight of a glycidyl-group-containing monomer and having a solubility parameter which is in the range of 11.0 to 11.6 and a glass transition temperature of at least 20.degree. C., a surface modifier (B) consisting of a polymer having a solubility parameter which is in the range of 10.4 to 11.0, and polyvalent carboxylic acid (B). The surface modifier (B) is in a content of 0.1 to 4 parts by weight with respect to a total content of 100 parts by weight of the acrylic resin (A) and the polyvalent carboxylic acid (C), while the components are so mixed with each other that the amount of carboxylic groups contained in the polyvalent carboxylic acid (C) is at an equivalence ratio of at least 0.5 to the amount of glycidyl groups contained in the acrylic resin (A).
摘要翻译：粉末涂料组合物包含含有至少40重量％的含缩水甘油基的单体并且溶解度参数在11.0至11.6范围内且玻璃化转变温度至少为20℃的丙烯酸树脂（A）由具有在10.4至11.0范围内的溶解度参数的聚合物和多价羧酸（B）组成的表面改性剂（B）。相对于100重量份丙烯酸树脂（A）和多元羧酸（C）的总含量，表面改性剂（B）的含量为0.1〜4重量份，而成分混合相对于丙烯酸树脂（A）中含有的缩水甘油基的量，多价羧酸（C）中所含的羧基的量相对于至少为0.5的当量比。

7. 发明授权

US5536888A Process for producing diol compounds 失效
标题翻译：二醇化合物的制备方法
公开(公告)号：US5536888A
公开(公告)日：1996-07-16
申请号：US364712
申请日：1994-12-27
申请人： Yasushi Shiomi , Hiroyuki Fukushima , Toshihiko Sumida , Shinichi Furusaki
发明人： Yasushi Shiomi , Hiroyuki Fukushima , Toshihiko Sumida , Shinichi Furusaki
IPC分类号： B01J23/80 , B01J37/03 , C07C29/149 , C07C31/20
CPC分类号： B01J37/03 , B01J23/80 , C07C29/149
摘要： A diol compound, for example, hexanediol, is produced with a high efficiency by esterifying a carboxylic acid mixture, collected from a reaction product mixture of a liquid phase oxidation of cyclohexane, with an esterifying agent and hydrogenate-decomposing the resultant esterification product mixture with hydrogen. The hydrogenate-decomposition is carried out by using a specific catalyst free from chromium and including a member selected from (A) copper and zinc-containing catalytic materials which are prepared by mixing an aqueous solution of water-soluble copper and zinc salts with an aqueous alkali metal or ammonium carbonate or alkali metal or ammonium hydrogen carbonate solution, reducing the resultant precipitate comprising a basic copper and zinc carbonate mixture with hydrogen and partially oxidizing the resultant reduction product with an oxygen-containing gas, and (B) copper and zinc-containing catalytic materials which are prepared by conducting the same mixing procedure as that for the catalytic material (A) except that the mixing is carried out at a temperature of 60.degree. to 95.degree. C. at a pH of 6.5 to 9.0, and by calcining the resultant precipitate at a temperature of 300.degree. C. to 450.degree. C.
摘要翻译：通过将从环己烷的液相氧化反应产物混合物收集的羧酸混合物与酯化剂酯化，并将所得酯化产物混合物氢化分解，从而高效率地生产二醇化合物，例如己二醇，氢。氢化物分解通过使用不含铬的特定催化剂进行，并且包括选自（A）铜和锌的催化材料的成员，其通过将水溶性铜和锌盐的水溶液与水溶液碱金属或碳酸铵或碱金属或碳酸氢铵溶液，将含有碱性铜和碳酸锌混合物的所得沉淀物用氢气还原，并用含氧气体部分氧化所得的还原产物，和（B）铜和锌 - 含有催化剂材料，其通过进行与催化材料（A）相同的混合程序制备，不同之处在于在6.5至9.0的pH下在60℃至95℃的温度下进行混合，并通过煅烧所得沉淀物在300℃至450℃的温度下

8. 发明授权

US5523349A Powder coating composition 失效
标题翻译：粉末涂料组合物
公开(公告)号：US5523349A
公开(公告)日：1996-06-04
申请号：US331956
申请日：1994-10-31
申请人： Yasushi Shiomi , Akimitsu Uenaka , Koichi Tsutsui
发明人： Yasushi Shiomi , Akimitsu Uenaka , Koichi Tsutsui
IPC分类号： C08F299/00 , C08F290/00 , C09D5/03 , C09D5/46 , C09D133/00 , C09D133/04 , C09D133/06 , C09D133/14 , C09D163/00 , C09D163/08 , C08L37/00 , C08L63/02
CPC分类号： C09D133/068 , C09D133/14
摘要： A powder coating composition contains acrylic resin (A) containing at least 40 percent by weight of a glycidyl-group-containing monomer and having a solubility parameter which is in the range of 11.0 to 11.6 and a glass transition temperature of at least 20.degree. C., a surface modifier (B) consisting of a polymer having a solubility parameter which is in the range of 10.4 to 11.0, and polyvalent carboxylic acid (B). The surface modifier (B) is in a content of 0.1 to 4 parts by weight with respect to a total content of 100 parts by weight of the acrylic resin (A) and the polyvalent carboxylic acid (C), while the components are so mixed with each other that the amount of carboxylic groups contained in the polyvalent carboxylic acid (C) is at an equivalence ratio of at least 0.5 to the amount of glycidyl groups contained in the acrylic resin (A).
摘要翻译：粉末涂料组合物包含含有至少40重量％的含缩水甘油基的单体并且溶解度参数在11.0至11.6范围内且玻璃化转变温度至少为20℃的丙烯酸树脂（A）由具有在10.4至11.0范围内的溶解度参数的聚合物和多价羧酸（B）组成的表面改性剂（B）。相对于100重量份丙烯酸树脂（A）和多元羧酸（C）的总含量，表面改性剂（B）的含量为0.1〜4重量份，而成分混合相对于丙烯酸树脂（A）中含有的缩水甘油基的量，多价羧酸（C）中所含的羧基的量相对于至少为0.5的当量比。

9. 发明授权

US5710349A Process for producing diol compounds 失效
标题翻译：二醇化合物的制备方法
公开(公告)号：US5710349A
公开(公告)日：1998-01-20
申请号：US448488
申请日：1995-06-05
申请人： Shinichi Furusaki , Masaoki Matsuda , Yasunori Miyamoto , Yasushi Shiomi
发明人： Shinichi Furusaki , Masaoki Matsuda , Yasunori Miyamoto , Yasushi Shiomi
IPC分类号： B01J23/745 , B01J23/80 , B01J35/00 , C07C29/149
CPC分类号： C07C29/149 , B01J23/745 , B01J23/80 , B01J35/0006
摘要： In the process of the present invention for producing diol compounds by esterifying a carboxylic acid mixture collected from a reaction product mixture of a liquid phase oxidation of cyclohexane with air and hydrogenate-decomposing the resultant esterification product mixture with hydrogen, the hydrogenate-decomposition is carried out by using a combined catalyst which includes a catalyst (A) including, as principal components, copper oxide and zinc oxide and a catalyst (B) including copper oxide and iron oxide carried on aluminum oxide, does not include chromium, has a high catalytic activity and can be easily separated by filtering, and the combined catalyst is collected from the hydrogenate-decomposition reaction product mixture by filtering it.
摘要翻译： PCT No.PCT / JP94 / 01664 Sec。 371日期：1995年6月5日 102（e）日期1995年6月5日PCT 1994年10月5日PCT PCT。第WO95 / 10497号公报日本1995年4月20日在本发明的制备二醇化合物的方法中，通过将从环己烷的液相氧化反应产物混合物中收集的羧酸混合物与空气酯化，并将所得酯化产物混合物用氢氢化分解，氢化物分解通过使用包括以氧化铜和氧化锌为主要成分的催化剂（A）和在氧化铝上载有氧化铜和氧化铁的催化剂（B）的组合催化剂进行，不包括铬，具有高催化活性，可以通过过滤容易地分离，并且通过过滤从氢化物分解反应产物混合物中收集组合的催化剂。

10. 发明授权

US5248835A Method of producing a monoalkylether of a dihydric phenol compound 失效
标题翻译：制备二氢苯酚化合物的单硬脂醇的方法
公开(公告)号：US5248835A
公开(公告)日：1993-09-28
申请号：US868962
申请日：1992-04-16
申请人： Yasushi Shiomi , Yasuo Nakamura , Takumi Manabe , Shinichi Furusaki , Masaoki Matsuda , Muneki Saito
发明人： Yasushi Shiomi , Yasuo Nakamura , Takumi Manabe , Shinichi Furusaki , Masaoki Matsuda , Muneki Saito
IPC分类号： B01J27/18 , B01J27/182 , B01J27/185 , C07C41/09
CPC分类号： B01J27/1806 , B01J27/182 , B01J27/1853 , C07C41/09
摘要： A monoalkylether of a dihydric phenol compound is produced at a high conversion and selectivity by catalytically dehydration reacting a dihydric phenol compound with a lower monohydric alcohol in the presence of a catalyst comprising at least one inorganic substance of the empirical formula (I):Al.sub.a P.sub.b Ti.sub.c Si.sub.d X.sub.e O.sub.f (I):wherein X is an alkali metal (Group Ia) atom, alkaline earth metal (Group IIa) atom or a metal atom of Group VIII of the Periodic Table, a, b, c, d, e and f are the numbers of Al, P, Ti, Si, X and O atoms respectively, and provided that a =1, b =1.0 to 1.9, c =0 05 to 0.5, d=0.05 to 0.2, e=0 to 0.9 and f=4.2 to 8.1, and collecting the resultant reaction product from the reaction system.

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