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1. 发明授权

US4106927A Non-explosive glyoxime compositions 失效
标题翻译：非爆炸性乙二醛组合物
公开(公告)号：US4106927A
公开(公告)日：1978-08-15
申请号：US709134
申请日：1976-07-27
申请人： Harris E. Petree , James B. Nabors, Jr. , Henry C. Grace
发明人： Harris E. Petree , James B. Nabors, Jr. , Henry C. Grace
IPC分类号： A01N35/10 , A01N9/20 , A01N9/02
CPC分类号： A01N35/10
摘要： A thermally stable water soluble glyoxime composition comprising a blend of glyoxime and an ethylene glycol-type material and a process for the preparation thereof comprising reacting glyoxal and a hydroxylamine acid salt in the presence of said ethylene glycol-type material.
摘要翻译：一种热稳定的水溶性乙二醛组合物，其包含乙二醛和乙二醇型材料的共混物及其制备方法，包括在所述乙二醇型材料的存在下使乙二醛和羟胺酸盐反应。

2. 发明授权

US4252742A Chemical process for the preparation of 2,6-dialkylcyclohexylamines from 2,6-dialkylphenols 失效
标题翻译：从2,6-二烷基苯酚制备2,6-二烷基环己胺的化学方法
公开(公告)号：US4252742A
公开(公告)日：1981-02-24
申请号：US56164
申请日：1979-07-13
申请人： Joseph T. Blackwell, III , Henry C. Grace , James B. Nabors , Harris E. Petree
发明人： Joseph T. Blackwell, III , Henry C. Grace , James B. Nabors , Harris E. Petree
IPC分类号： C07B61/00 , A01N20060101 , A01N33/04 , B01J23/00 , B01J23/40 , C07C20060101 , C07C67/00 , C07C209/00 , C07C209/16 , C07C211/35 , C07C85/08 , C07C87/36 , C07C87/45
CPC分类号： C07C209/16 , C07C2101/14
摘要： A process for preparing 2,6-dialkylcyclohexylamine, e.g., 2,6-dimethylcyclohexylamine, from a corresponding dialkylphenol, e.g., 2,6-dimethylphenol, by passing the phenol over a bed of a hydrogen-transfer catalyst in the presence of ammonia at elevated temperatures and pressures.
摘要翻译：通过在氨的存在下使苯酚在氢转移催化剂的床上通过，将相应的二烷基苯酚例如2,6-二甲基苯酚制备2,6-二烷基环己胺例如2,6-二甲基环己胺的方法升高的温度和压力。

3. 发明授权

US3981712A Treatment of iron deficiencies in plants with iron complexes of ethylene-bis-(.alpha.-imino-2-hydroxyaryl acetic acids) 失效
标题翻译：用乙烯 - 双 - （{6-亚氨基-2-羟基芳基乙酸）铁络合物处理植物铁缺陷
公开(公告)号：US3981712A
公开(公告)日：1976-09-21
申请号：US593099
申请日：1975-07-03
申请人： Harris E. Petree , Joseph W. Stutts
发明人： Harris E. Petree , Joseph W. Stutts
IPC分类号： C05D9/02 , C07F15/02
CPC分类号： C07F15/025 , C05D9/02 , Y10S71/02
摘要： Compositions and methods useful for the treatment of iron deficiencies in plant utilizing new iron complexes of ethylene-bis(.alpha.-imino-2-hydroxyaryl-acetic acids) containing sulfonic acid groups are disclosed in which the molar ratio of iron to ligand is from about 1.1:1 to 3:1. These complexes are stable at pH values of from about 6.0 to 9.0.
摘要翻译：公开了使用含有磺酸基团的新型的具有亚乙基 - 双（α-亚氨基-2-羟基芳基 - 乙酸）的铁络合物来处理植物铁缺乏的组合物和方法，其中铁与配体的摩尔比为约 1.1：1到3：1。这些配合物在约6.0至9.0的pH值下是稳定的。

4. 发明授权

US4267347A Method for direct preparation for 1,2,4-triazole from hydrazine and formamide 失效
标题翻译：从肼和甲酰胺直接制备1,2,4-三唑的方法
公开(公告)号：US4267347A
公开(公告)日：1981-05-12
申请号：US92257
申请日：1979-11-07
申请人： Harris E. Petree , Joseph R. Pociask , John T. Gupton
发明人： Harris E. Petree , Joseph R. Pociask , John T. Gupton
IPC分类号： C07D249/08
CPC分类号： C07D249/08
摘要： Process for the preparation of 1,2,4-triazole comprises contacting hydrazine or its aqueous solutions with at least about 2.5 moles of formamide at a temperature of 140.degree. to 210.degree. C. and then recovering the resultant 1,2,4-triazole in yields of 92-98% with 94-98% purity. The formamide is maintained in an excess over about the 2.5 molar amount consumed in the reaction with the hydrazine. Recovery steps for isolating the 1,2,4-triazole are disclosed.
摘要翻译：制备1,2,4-三唑的方法包括在140〜210℃的温度下使肼或其水溶液与至少约2.5摩尔的甲酰胺接触，然后回收得到的1,2,4-三唑产率为92-98％，纯度为94-98％。在与肼的反应中消耗的甲酰胺保持超过约2.5摩尔量的过量。公开了用于分离1,2,4-三唑的回收步骤。

5. 发明授权

US4130582A Preparation of phenolic ethylenediaminepolycarboxylic acids 失效
标题翻译：酚醛二胺多羧酸的制备
公开(公告)号：US4130582A
公开(公告)日：1978-12-19
申请号：US788712
申请日：1977-04-19
申请人： Harris E. Petree , Hal L. Myatt , Alex M. Jelenevsky
发明人： Harris E. Petree , Hal L. Myatt , Alex M. Jelenevsky
IPC分类号： C07C51/00
CPC分类号： C07C233/12
摘要： A process for the preparation of phenolic ethylenediamine polycarboxylic acids in predominantly the ortho isomeric form which comprises reacting a phenol compound, ethylenediamine, glyoxylic acid and a base, said phenol compound functioning both as a reactant and as the sole solvent for the reaction system. The product can then be isolated or directly reacted with an iron salt to form the corresponding iron chelate.
摘要翻译：用于制备主要为邻位异构形式的酚类乙二胺多元羧酸的方法，其包括使酚化合物，乙二胺，乙醛酸和碱反应，所述酚化合物既用作反应物又用作反应体系的唯一溶剂。然后可以将产物与铁盐分离或直接反应形成相应的铁螯合物。

6. 发明授权

US4275238A Process for the preparation of cyclopropylmethyl-n-propylamine 失效
标题翻译：制备环丙基甲基正丙胺的方法
公开(公告)号：US4275238A
公开(公告)日：1981-06-23
申请号：US111055
申请日：1980-01-10
申请人： Harris E. Petree , James B. Nabors
发明人： Harris E. Petree , James B. Nabors
IPC分类号： C07C45/59 , C07D307/28 , C07C85/08
CPC分类号： C07D307/28 , C07C45/59
摘要： Cyclopropylmethyl-N-n-propylamine is prepared by (a) cyclizing 1,4-butanediol by a cobalt-containing catalyst to 2,3-dihydrofuran at a temperature in the range of about 210.degree.-235.degree. C.; (b) thermally isomerizing the 2,3-dihydrofuran to cyclopropanecarboxaldehyde in an open-reactor columm; and (c) reductively alkylating the cyclopropanecarboxaldehyde with n-propylamine and hydrogen in the presence of a platinum catalyst.
摘要翻译：环丙基甲基-N-正丙胺通过以下方法制备：（a）在约210-235℃的温度下，通过含钴催化剂将1,4-丁二醇环化为2,3-二氢呋喃。（b）在开放反应釜中将2,3-二氢呋喃热异构化为环丙烷甲醛; 和（c）在铂催化剂存在下，用正丙胺和氢还原烷基化环丙烷甲醛。

7. 发明授权

US4288594A Caustic-free process for the production of monochloro-diamino-s-triazines 失效
标题翻译：无氯工艺生产一氯二氨基三嗪
公开(公告)号：US4288594A
公开(公告)日：1981-09-08
申请号：US118375
申请日：1980-02-04
申请人： Philip G. McCracken , Hal Myatt , Harris E. Petree
发明人： Philip G. McCracken , Hal Myatt , Harris E. Petree
IPC分类号： C07D251/44 , C07D251/50
CPC分类号： C07D251/50 , C07D251/44
摘要： A new and improved process is provided for preparing monochloro-diamino-s-triazines which are useful as herbicides.The process comprises reacting in a first stage cyanuric chloride and a selected monoalkylamine hydrochloride at elevated temperature to give a dichloro-monoalkylamino-s-triazine and reacting in a second stage this dichloro-monoalkylamino-s-triazine with an excess of a different monoalkylamine which may be introduced as a pure liquid, as gas or as a solution in water. The third stage of the process consists of an exchange whereby the monoalkylamine hydrochloride of the first stage and the free monoalkylamine of the second stage are generated. The process gives consistent yields in excess of 97% of monochloro-diamino-s-triazines. Because the process is caustic-free and due to the feasibility of recycling the excess of monoalkylamines employed, no serious effluent problems arise.
摘要翻译：提供了一种新的改进方法，用于制备可用作除草剂的一氯二氨基-s-三嗪。该方法包括在升高的温度下使第一级氰尿酰氯和选择的单烷基胺盐酸盐反应，得到二氯单烷基氨基-s-三嗪并在第二阶段使该二氯单烷基氨基-s-三嗪与过量的不同的单烷基胺反应，可以作为纯液体，作为气体或作为在水中的溶液引入。该方法的第三阶段是由第一阶段的单烷基胺盐酸盐和第二阶段的游离单烷基胺生成的交换体。该方法得到超过97％的一氯二氨基-s-三嗪的一致收率。因为该方法是无腐蚀性的，并且由于使用过量的单烷基胺的循环的可行性，所以不会出现严重的流出物问题。

8. 发明授权

US4018771A Process for the production of 2-alkyl or 2-cycloalkyl-4-methyl-6-hydroxypyrimidines 失效
标题翻译： 2-烷基或2-环烷基-4-甲基-6-羟基嘧啶的制备方法
公开(公告)号：US4018771A
公开(公告)日：1977-04-19
申请号：US711035
申请日：1976-08-23
申请人： John T. Gupton, III , Alex M. Jelenevsky , Teruko U. Miyazaki , Harris E. Petree
发明人： John T. Gupton, III , Alex M. Jelenevsky , Teruko U. Miyazaki , Harris E. Petree
IPC分类号： C07D239/36 , C07D239/34
CPC分类号： C07D239/36
摘要： Production of 2-alkyl or 2-cycloalkyl-4-methyl-6-hydroxy pyrimidines by first reacting diketene and lower alkanoic or cycloalkanoic acid amides in the presence of catalytic amounts of Lewis bases or Lewis or Bronsted acids, followed by treating the N-acetoacetyl (lower) alkanoic or cycloalkanoic acid amide intermediates with ammonia in the presence of acid catalysts.
摘要翻译：通过在催化量的路易斯碱或路易斯酸或布朗斯台德酸存在下首先使双烯酮和低级链烷酸或环烷酸酰胺反应生产2-烷基或2-环烷基-4-甲基-6-羟基嘧啶，乙酰乙酰（低级）链烷酸或环烷酸酰胺与酸在酸催化剂存在下中间体。

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