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1. 发明授权

US4242101A Fuels for gasoline engines 失效
标题翻译：汽油发动机燃料
公开(公告)号：US4242101A
公开(公告)日：1980-12-30
申请号：US48478
申请日：1979-06-14
申请人： Hans-Henning Vogel , Knut Oppenlaender , Klaus Starke
发明人： Hans-Henning Vogel , Knut Oppenlaender , Klaus Starke
IPC分类号： C10L1/22 , C10L1/14 , C10L1/18 , C10L1/224 , C10L10/08 , F02B77/04
CPC分类号： C10L1/224 , C10L1/14 , C10L1/1822 , C10L1/1832 , F02B77/04
摘要： Fuels for gasoline engines, which contain small amounts of(a) imides or amide-imides, or mixtures of imides and amide-imides, obtained from nitrilotriacetic acid and/or from ethylenediaminetetraacetic acid and amines or amine mixtures of 7 to 18 carbon atoms, of the formula I ##STR1## where the radicals X are identical or different radicals --HN--R, or adjacent radicals X are a radical ##STR2## which completes a ring ##STR3## m is 0 or 1 and R is an unbranched or branched aliphatic radical of 7 to 18 carbon atoms, as valve and carburetor cleaners, and(b) mixtures of highly hydrogenated petroleum distillates, in the boiling range of the kerosine fraction and highly refined solvent raffinates with viscosities of from 50 to 500 mm.sup.2 /s at 40.degree. C., the weight ratio of these constituents being from 20:80 to 80:20, keep the carburetors and valves of gasoline engines clean, thereby achieving better combustion of the fuel in the engine.
摘要翻译：含有少量（a）酰亚胺或酰胺 - 酰亚胺或由次氮基三乙酸和/或乙二胺四乙酸和7至18个碳原子的胺或胺混合物获得的酰亚胺和酰胺 - 酰亚胺混合物的汽油发动机燃料，其中基团X是相同或不同的基团-HN-R或相邻基团X是完成环的基团，其中m是0或1，并且R是无支链或具有7至18个碳原子的支链脂肪族基团，作为阀和化油器清洁剂，和（b）高度氢化的石油馏分的混合物，在煤油馏分的沸点范围内，粘度为50-500mm2 / s的高度精制的溶剂残渣在40℃，这些成分的重量比为20:80至80:20，保持汽油发动机的化油器和阀门清洁，从而实现发动机燃料的更好的燃烧。

2. 发明授权

US4137263A Process for the evaporation of cyclohexanone oxime 失效
标题翻译：环己酮肟蒸发的方法
公开(公告)号：US4137263A
公开(公告)日：1979-01-30
申请号：US831790
申请日：1977-09-09
申请人： Otto Immel , Bernd-Ulrich Kaiser , Hans-Helmut Schwarz , Klaus Starke
发明人： Otto Immel , Bernd-Ulrich Kaiser , Hans-Helmut Schwarz , Klaus Starke
IPC分类号： C07C251/46 , C07C20060101 , C07C67/00 , C07C239/00 , C07D20060101 , C07D201/04 , C07D223/10 , C07C131/04
CPC分类号： F27B3/00
摘要： A process for the evaporation of cyclohexanone oxime, wherein the cyclohexanone oxime is evaporated in the presence of an inert gas at a superatmospheric pressure of at least 300 Torr at 110.degree. to 160.degree. C, the evaporation temperature being governed by the inert gas pressure or by the ratio of cyclohexanone oxime to inert gas.
摘要翻译：蒸发环己酮肟的方法，其中环己酮肟在惰性气体存在下，在110至160℃的超大气压至少300乇的条件下蒸发，蒸发温度由惰性气体压力或通过环己酮肟与惰性气体的比例。

3. 发明授权

US4141896A Process for the producing .epsilon.-caprolactam from the distillation of cyclohexanone oxime 失效
标题翻译：从环己酮肟蒸馏生产{68-己内酰胺的方法
公开(公告)号：US4141896A
公开(公告)日：1979-02-27
申请号：US832008
申请日：1977-09-09
申请人： Otto Immel , Andre DE Jager , Bernd-Ulrich Kaiser , Hans-Helmut Schwarz , Klaus Starke
发明人： Otto Immel , Andre DE Jager , Bernd-Ulrich Kaiser , Hans-Helmut Schwarz , Klaus Starke
IPC分类号： C07D201/02 , C07D201/04
CPC分类号： C07D201/04
摘要： A process for the production of .epsilon.-caprolactum from cyclohexanone oxime by rearrangement in the gaseous phase on a fluid-bed catalyst containing boron oxide, wherein residues from the distillation of cyclohexanone oxime are introduced into the reaction in liquid form, and wherein from 5 to 500 times their quantity of cyclohexanone oxime in vapor form and at least 50 times their quantity of inert gas are present during the reaction.
摘要翻译：一种通过在含有氧化硼的流化床催化剂上在气相中重新排列从环己酮肟生产ε-己内酰胺的方法，其中将来自环己酮肟蒸馏的残余物以液体形式引入反应中，其中从5至蒸气形式的环己酮肟的量为其500倍，并且在反应期间存在至少50倍量的惰性气体。

4. 发明授权

US4155876A Catalyst regeneration of boric acid on carbon catalysts 失效
标题翻译：硼酸在碳催化剂上的催化剂再生
公开(公告)号：US4155876A
公开(公告)日：1979-05-22
申请号：US831936
申请日：1977-09-09
申请人： Harry Danziger , Otto Immel , Bernd-Ulrich Kaiser , Hans-Helmut Schwarz , Klaus Starke
发明人： Harry Danziger , Otto Immel , Bernd-Ulrich Kaiser , Hans-Helmut Schwarz , Klaus Starke
IPC分类号： C07D223/10 , B01J21/20 , B01J38/30 , C07D201/04
CPC分类号： C07D201/04 , B01J21/20 , Y02P20/584
摘要： A process for the regeneration of a granular, supported catalyst of boric acid on carbon, wherein a part of the catalyst is removed from a fluidized bed reactor, in which cyclohexanone oxime is rearranged into caprolactam on this catalyst, when the "differential content in the catalyst of organic nitrogen" is between 0.3 and 2.0% by weight and is replaced by an equal amount of regenerated catalyst so that the differential organic nitrogen content remains in the above-mentioned range, the quantity of catalyst removed is regenerated with air in a fluidized bed at a temperature of from 400.degree. to 700.degree. C. and is returned to the fluidized bed reactor used for rearrangement when a further part of the catalyst is removed therefrom for regeneration.
摘要翻译：一种用于再生颗粒状载体上的硼酸催化剂的方法，其中将一部分催化剂从流化床反应器中除去，其中环己酮肟在该催化剂上重排为己内酰胺，当“ 有机氮的催化剂“为0.3-2.0重量％，并由等量的再生催化剂代替，使得差示有机氮含量保持在上述范围内，除去的催化剂的量在流化床中用空气再生在400〜700℃的温度下进行洗涤，并且当将另一部分催化剂从其中除去再生时，返回到用于重排的流化床反应器。

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