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1. 发明授权

US4859756A Polymers of oxyalkylated unsaturated quaternary ammonium salts, their preparation and their use 失效
标题翻译：烷氧基化不饱和季铵盐的聚合物及其制备及其应用
公开(公告)号：US4859756A
公开(公告)日：1989-08-22
申请号：US226198
申请日：1988-07-29
申请人： Hans-Helmut Goertz , Alfred Oftring , Friedrich Vogel
发明人： Hans-Helmut Goertz , Alfred Oftring , Friedrich Vogel
IPC分类号： B01D21/01 , A61K8/72 , A61K8/81 , A61Q5/12 , C02F1/54 , C07C51/58 , C07D233/60 , C08F20/36 , C08F20/52 , C08F20/60 , C08F26/00 , C08F26/02 , C08F120/36 , C08F120/60 , C08F126/02 , H01B1/12
CPC分类号： C02F1/54 , A61K8/8152 , A61K8/817 , A61Q5/12 , C07C51/58 , C08F20/36 , C08F20/60 , C08F26/02 , H01B1/122 , A61K2800/526 , A61K2800/5426
摘要： Polymers are obtained by polymerization of water-soluble monomers which contain one or more polymerizable olefinic double bonds and a quaternary nitrogen atom which is substituted by one or more hydroxyalkyl groups and are present in the form of halide-free salts, with or without further comonomers.
摘要翻译：聚合物通过含有一个或多个可聚合烯属双键的水溶性单体和被一个或多个羟烷基取代的季氮原子聚合而获得，并且以无卤盐形式存在，具有或不含有其它共聚单体。

2. 发明授权

US4908413A Preparation of copolymers of monoalkyl maleates and vinyl alkyl ethers 失效
标题翻译：制备马来酸单烷基酯和乙烯基烷基醚的共聚物
公开(公告)号：US4908413A
公开(公告)日：1990-03-13
申请号：US251754
申请日：1988-10-03
申请人： Hans-Helmut Goertz , Ferdinand Straub , Friedrich Vogel , Franz Frosch , Paul Naegele , Hans-Juergen Raubenheimer
发明人： Hans-Helmut Goertz , Ferdinand Straub , Friedrich Vogel , Franz Frosch , Paul Naegele , Hans-Juergen Raubenheimer
IPC分类号： C08F2/06 , C08F4/04 , C08F8/14 , C08F222/16
CPC分类号： C08F222/16 , C08F8/14
摘要： Copolymers of monoalkyl maleates and vinyl alkyl ethers are prepared by free radical copolymerization of maleic anhydride and a vinyl alkyl ether followed by reaction with an alkanol, by a process in which the vinyl alkyl ether component is present in excess in the reaction mixture in each phase of the polymerization, the free radical copolymerization is carried out in acetone and the acetone is removed by distillation during or after ester formation at up to 70.degree. C.
摘要翻译：单烷基马来酸酯和乙烯基烷基醚的共聚物是通过马来酸酐和乙烯基烷基醚的自由基共聚反应制备的，随后与链烷醇反应，其中乙烯基烷基醚组分在每相中的反应混合物中过量存在的聚合反应中，自由基共聚在丙酮中进行，在高达70℃的酯形成过程中或之后通过蒸馏除去丙酮。

3. 发明授权

US4841066A Preparation of 3-methyl-1-vinylimidazolium chlorides 失效
标题翻译： 3-甲基-1-乙烯基咪唑氯化物的制备
公开(公告)号：US4841066A
公开(公告)日：1989-06-20
申请号：US49314
申请日：1987-05-13
申请人： Hans-Helmut Goertz , Ferdinand Straub , Axel Sanner , Albrecht Kolb , Hans-Juergen Raubenheimer , Friedrich Vogel
发明人： Hans-Helmut Goertz , Ferdinand Straub , Axel Sanner , Albrecht Kolb , Hans-Juergen Raubenheimer , Friedrich Vogel
IPC分类号： C07D233/58 , C07D521/00 , C08F26/00 , C08F26/06
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08 , C08F26/06
摘要： 3-Methyl-1-vinylimidazolium chlorides are prepared by quaternizing N-vinylimidazoles in aqueous solution with methyl chloride and are used for the preparation of water-soluble homo- or copolymers.
摘要翻译： 3-甲基-1-乙烯基咪唑鎓氯化物通过用甲基氯季铵化N-乙烯基咪唑在水溶液中制备，并用于制备水溶性均聚物或共聚物。

4. 发明授权

US5455216A Preparation of a supported catalyst for the polymerization of .alpha.-olefins 失效
标题翻译：制备用于α-烯烃聚合的负载型催化剂
公开(公告)号：US5455216A
公开(公告)日：1995-10-03
申请号：US124047
申请日：1993-09-21
申请人： Hans-Joachim Mueller , Godofredo Follmer , Rainer Konrad , Roland Saive , Martin Lux , Hans-Helmut Goertz , Guido Funk
发明人： Hans-Joachim Mueller , Godofredo Follmer , Rainer Konrad , Roland Saive , Martin Lux , Hans-Helmut Goertz , Guido Funk
IPC分类号： C08F4/02 , C08F4/22 , C08F4/24 , C08F10/00 , B01J35/08 , B01J37/08
CPC分类号： C08F10/00
摘要： A process for the preparation of a supported catalyst for the polymerization of .alpha.-olefins, in which(1) a silicon dioxide-containing support gel is prepared by(1.1) introducing a sodium water glass or potassium water glass solution into a swirling stream of an aqueous mineral acid longitudinally and tangentially to the stream, spraying the resultant silica hydrosol in drop form into a gaseous medium and allowing it to solidify to form a hydrogel, and freeing the resultant hydrogel from salts by washing without prior ageing,(1.2) drying the hydrogel resulting from (1.1) to form the support gel,(2) the support gel (1) is charged with chromium trioxide or a chromium compound which can be converted into chromium trioxide under the conditions of process step (3), giving a chromium-containing support gel, and(3) the chromium-containing support gel (2) is heated at from 400.degree. to 1100.degree. C. for from 10 to 1000 minutes in an anhydrous gas stream containing oxygen in a concentration of greater than 10% by volume,comprises drying the hydrogel resulting from step (1.1) in step (1.2) within a time of not more than 60 seconds in a shaping, high-speed dryer at an inlet temperature of from 80.degree. to 400.degree. C.
摘要翻译：一种制备用于α-烯烃聚合的负载催化剂的方法，其中（1）含二氧化硅的载体凝胶通过（1.1）将钠水玻璃或钾水玻璃溶液引入旋流将水性无机酸纵向和切向于料流，将所得的二氧化硅水溶胶以液滴形式喷雾到气态介质中并使其固化形成水凝胶，并通过在没有预先熟化的情况下洗涤将所得水凝胶从盐中释放，（1.2）干燥由（1.1）产生的形成支持凝胶的水凝胶，（2）载体凝胶（1）中加入三氧化铬或铬化合物，其可以在工艺步骤（3）的条件下转化为三氧化铬，得到含铬载体凝胶，（3）含铬载体凝胶（2）在含有浓度浓度的氧的无水气流中在400〜1100℃下加热10〜1000分钟大于10体积％包括在入口温度为80°至400°的成形高速干燥器中在不超过60秒的时间内将步骤（1.2）中由步骤（1.1）得到的水凝胶干燥 DEG C.

5. 发明申请

US20050148755A1 Production of polyoxymethylene and suitable (II) catalysts 失效
标题翻译：聚甲醛和合适的（II）催化剂的生产
公开(公告)号：US20050148755A1
公开(公告)日：2005-07-07
申请号：US10510477
申请日：2003-04-10
申请人： Hans-Helmut Goertz , Gerrit Luinstra , Wolfram Wielandt , Michael Henes , Ekkehard Lindner
发明人： Hans-Helmut Goertz , Gerrit Luinstra , Wolfram Wielandt , Michael Henes , Ekkehard Lindner
IPC分类号： C07F17/00 , C08G2/06 , C08G2/08 , C08G2/00
CPC分类号： C08G2/06 , C07F17/00 , C08G2/08
摘要： A process is described for preparing polyoxymethylene by contacting a formaldehyde source with a catalyst of the formula I [CpvMLw]m+Zm/nn− (I) where M is Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, W, Mn, Re, Fe, Ru, Os, Co, Rh or Ir, Cp is a cyclopentadienyl ligand C5H(5−u)R1u, where u is from 0 to 5 and R1 is alkyl, alkenyl, aryl, heteroaryl, aralkyl, COOR2, COR2, CN or NO2, and R2 is H, alkyl, aryl or aralkyl, v is 1 or 2, each L is independently a nitrile, CO or a ligand displaceable by CO, w is an integer from 0 to 4, Z is an anion, and m and n are each independently an integer from 1 to 3.
摘要翻译：描述了通过使甲醛源与式I的催化剂接触来制备聚甲醛的方法，该方法式为：式中：=“引线”→[Cp （I） =“In-line Formulas”end =“tail”？>其中M是Ti，Zr，Hf，V，Nb，Ta，Cr，Mo，W，Mn，Re，Fe，Ru，Os，Co，Rh或Ir ，Cp是环戊二烯基配体C 5 H（5-u）R 1，其中u是 0至5，R 1是烷基，烯基，芳基，杂芳基，芳烷基，COOR 2，COR 2，CN或NO 2，R 2是H，烷基，芳基或芳烷基，v是1或2，每个L独立地是腈，CO或可被CO取代的配体，w是整数 0至4，Z是阴离子，m和n各自独立地为1至3的整数。

6. 发明授权

US5247025A Multistage graft copolymer and its use for the preparation of transparent PVC molding materials 失效
标题翻译：多层共聚物及其制备透明PVC模塑材料的用途
公开(公告)号：US5247025A
公开(公告)日：1993-09-21
申请号：US844316
申请日：1992-03-02
申请人： Hans-Helmut Goertz , Guenter Hatzmann , Werner Oschmann
发明人： Hans-Helmut Goertz , Guenter Hatzmann , Werner Oschmann
IPC分类号： C08F2/22 , C08F285/00 , C08L51/00
CPC分类号： C08L51/00 , C08F285/00 , Y10S525/902
摘要： Graft copolymers obtained byA) emulsion polymerization of from 5 to 35% by weight of a monomer mixture ofa.sub.1) 60-80% by weight of one or more vinylaromatic monomers,a.sub.2) 20-40% by weight of one or more ethylenically unsaturated nitriles,B) subsequent emulsion polymerization, in the presence of the emulsion polymer obtained in stage A), of 20-45% by weight of a monomer mixture ofb.sub.1) 50-75% by weight of one or more vinylaromatic monomers,b.sub.2) 25-50% by weight of one or more C.sub.1 -C.sub.18 -alkyl acrylates,C) subsequent emulsion polymerization, in the presence of the emulsion polymer obtained in stage B), of 5-35% by weight of a monomer mixture ofc.sub.1) 60-80% by weight of one or more vinylaromatic monomers,c.sub.2) 20-40% by weight of one or more ethylenically unsaturated nitriles,D) subsequent emulsion polymerization, in the presence of the emulsion polymer obtained in stage C), of 15-45% by weight of a monomer mixture ofd.sub.1) 80-99.9% by weight of one or more C.sub.1 -C.sub.18 -alkyl acrylates,d.sub.2) 0.1-0% by weight of one or more di- or polyethylenically unsaturated monomers.The graft copolymers can be used for the preparation of transparent PVC molding materials.
摘要翻译：通过A）乳液聚合获得的接枝共聚物，其通过5重量％至35重量％的a1）60-80重量％的一种或多种乙烯基芳族单体的混合物，a2）20-40重量％的一种或多种烯属不饱和单体腈）B）在步骤A）中得到的乳液聚合物存在下，随后的乳液聚合为20-45重量％的b1）50-75重量％的一种或多种乙烯基芳族单体的单体混合物，b2） 25-50重量％的一种或多种丙烯酸C 1 -C 18烷基酯，C）在步骤B）中获得的乳液聚合物存在下，随后的乳液聚合为5-35重量％的单体混合物c1） 60-80重量％的一种或多种乙烯基芳族单体，c2）20-40重量％的一种或多种烯键式不饱和腈，D）在步骤C）中获得的乳液聚合物存在下的随后乳液聚合为15 -45重量％的d1）80-99.9重量％的一种或多种C1-C18烷基丙烯酸酯的单体混合物，d2）0.1-0％一种或多种二烯或多烯属不饱和单体的重量。接枝共聚物可用于制备透明PVC成型材料。

7. 发明授权

US4880585A Continuous method of tableting 失效
标题翻译：连续压片方法
公开(公告)号：US4880585A
公开(公告)日：1989-11-14
申请号：US289407
申请日：1988-12-22
申请人： Roger G. Klimesch , Gerhard Bleckmann , Karl-Peter Farwerck , Hans-Helmut Goertz , Lothar Schlemmer
发明人： Roger G. Klimesch , Gerhard Bleckmann , Karl-Peter Farwerck , Hans-Helmut Goertz , Lothar Schlemmer
IPC分类号： A61H39/00 , A61J3/10 , A61K9/20 , A61K9/22 , A61K9/26 , B29B9/06 , B30B11/16 , B30B11/24
CPC分类号： A61J3/10 , A61K9/2095 , B29B9/06 , B30B11/16 , B30B15/308 , A61J2200/20 , B29K2503/00
摘要： Extrudable pharmaceutical mixtures are tableted by a continuous method in which the mixture is extruded and the still deformable extrudate is pressed between two rollers which are driven in opposite directions and possess depressions opposite one another in the roller shell, the form of these depressions determining the tablet shape.
摘要翻译：可挤出药物混合物通过连续方法压片，其中混合物被挤出，并且将可变形的挤出物压在两个辊之间，两个辊之间沿相反方向被驱动，并且在辊壳中具有彼此相对的凹陷，这些凹陷的形式决定了片剂形状。

8. 发明授权

US4801460A Preparation of solid pharmaceutical forms 失效
标题翻译：固体药物制剂的制备
公开(公告)号：US4801460A
公开(公告)日：1989-01-31
申请号：US34938
申请日：1987-04-06
申请人： Hans-Helmut Goertz , Roger G. Klimesch , Klaus Laemmerhirt , Siegfried Lang , Axel Sanner , Reinhard Spengler
发明人： Hans-Helmut Goertz , Roger G. Klimesch , Klaus Laemmerhirt , Siegfried Lang , Axel Sanner , Reinhard Spengler
IPC分类号： A61K47/32 , A61K9/20 , A61K9/22 , A61K9/26 , A61K47/00
CPC分类号： A61K9/2095 , A61K9/2027 , B29K2105/0035
摘要： Process for the preparation of solid pharmaceutical forms by mixing one or more pharmaceutical active compounds with one or more fusible, pharmacologically tolerated binders and, if required, other conventional pharmaceutical auxiliaries, at from 50.degree. to 180.degree. C., and subjecting the mixture to injection molding or extrusion and shaping, wherein the fusible binder used is a NVP polymer which contains not less than 20% by weight of NVP as copolymerized units, and, where they are present, all of whose comonomers contain nitrogen and/or oxygen.
摘要翻译：通过将一种或多种药物活性化合物与一种或多种可熔，药理学耐受的粘合剂和（如果需要的话）混合制备固体药物形式的方法，其中常规药物助剂在50至180℃下，注塑或挤出成型，其中所用的可熔粘合剂是NVP聚合物，其含有不少于20重量％的作为共聚单元的NVP，并且当它们存在时，所有共聚单体都含有氮和/或氧。

9. 发明授权

US5625013A Preparation of a supported catalyst for the polymerization of .alpha.-olefins 失效
标题翻译：制备用于α-烯烃聚合的负载型催化剂
公开(公告)号：US5625013A
公开(公告)日：1997-04-29
申请号：US422937
申请日：1995-05-24
申请人： Hans-Joachim Mueller , Godofredo Follmer , Rainer Konrad , Roland Saive , Martin Lux , Hans-Helmut Goertz , Guido Funk
发明人： Hans-Joachim Mueller , Godofredo Follmer , Rainer Konrad , Roland Saive , Martin Lux , Hans-Helmut Goertz , Guido Funk
IPC分类号： C08F4/02 , C08F4/22 , C08F4/24 , C08F10/00 , B01J35/08
CPC分类号： C08F10/00
摘要： A process for the preparation of a supported catalyst for the polymerization of .alpha.-olefins, in which(1) a silicon dioxide-containing support gel is prepared by(1.1) introducing a sodium water glass or potassium water glass solution into a swirling stream of an aqueous mineral acid longitudinally and tangentially to the stream, spraying the resultant silica hydrosol in drop form into a gaseous medium and allowing it to solidify to form a hydrogel, and freeing the resultant hydrogel from salts by washing without prior ageing,(1.2) drying the hydrogel resulting from (1.1) to form the support gel,(2) the support gel (1) is charged with chromium trioxide or a chromium compound which can be converted into chromium trioxide under the conditions of process step (3), giving a chromium-containing support gel, and(3) the chromium-containing support gel (2) is heated at from 400.degree. to 1100.degree. C. for from 10 to 1000 minutes in an anhydrous gas stream containing oxygen in a concentration of greater than 10% by volume,comprises drying the hydrogel resulting from step (1.1) in step (1.2) within a time of not more than 60 seconds in a shaping, high-speed dryer at an inlet temperature of from 80.degree. to 400.degree. C.
摘要翻译：一种制备用于α-烯烃聚合的负载催化剂的方法，其中（1）含二氧化硅的载体凝胶通过（1.1）将钠水玻璃或钾水玻璃溶液引入旋流将水性无机酸纵向和切向于料流，将所得的二氧化硅水溶胶以液滴形式喷雾到气态介质中并使其固化形成水凝胶，并通过在没有预先熟化的情况下洗涤将所得水凝胶从盐中释放，（1.2）干燥由（1.1）产生的形成支持凝胶的水凝胶，（2）载体凝胶（1）中加入三氧化铬或铬化合物，其可以在工艺步骤（3）的条件下转化为三氧化铬，得到含铬载体凝胶，（3）含铬载体凝胶（2）在含有浓度浓度的氧的无水气流中在400〜1100℃下加热10〜1000分钟大于10体积％包括在入口温度为80°至400°的成形高速干燥器中在不超过60秒的时间内将步骤（1.2）中由步骤（1.1）得到的水凝胶干燥 DEG C.

10. 发明授权

US5414064A Preparation of homopolymers of ethylene or copolymers of ethylene 失效
标题翻译：制备乙烯均聚物或乙烯共聚物
公开(公告)号：US5414064A
公开(公告)日：1995-05-09
申请号：US274692
申请日：1994-07-14
申请人： Martin Lux , Guido Funk , Roland Saive , Hans-Helmut Goertz , Rainer Konrad
发明人： Martin Lux , Guido Funk , Roland Saive , Hans-Helmut Goertz , Rainer Konrad
IPC分类号： C09K3/16 , C08F2/34 , C08F2/44 , C08F10/00 , C08F10/02 , C08F110/02 , C08K5/17 , C08K5/20 , C08L23/02
CPC分类号： C08F10/02 , C08F110/02 , Y10S526/901 , Y10S526/904
摘要： Homopolymers of ethylene or copolymers of ethylene with minor amounts of other C.sub.3 -C.sub.12 -alk-1-enes are prepared by catalytic polymerization in a suspension or in the gas phase in the presence of an antistatic agent at from 50 to 120.degree. C. and from 5 to 50 bar by a process in which the antistatic agent used is a mixture of the following substances:a) a metal salt of medialanic acid of the formula (I) ##STR1## b) a metal salt of an anthranilic acid of the general formula (II) ##STR2## where the organic radical R.sup.1 is either.alpha.)--CO--(CH.sub.2).sub.x --CH.sub.3 (II.alpha.)or.beta.)--CO--(CH.sub.2).sub.y --CH.dbd.CH--(CH.sub.2).sub.z --CH.sub.3(III.beta.)and x, y and z are each an integer and are from 6 to 18 for x, from 1 to 16 for y, from 1 to 16 for z and from 4 to 17 for y+z, andc) a polyamine obtainable by reacting epichlorohydrin and an aliphatic primary monoamine or an N-alkylalkylenediamine of the general formula (IV)R.sup.2 NH--R.sup.3 --NH.sub.2 (IV),whereR.sup.2 is C.sub.8 -C.sub.24 -alkyl andR.sup.3 is C.sub.2 -C.sub.6 -alkylene.
摘要翻译：乙烯均聚物或乙烯与少量其它C 3 -C 12烷-1-烯的共聚物通过在50至120℃的抗静电剂存在下在悬浮液或气相中催化聚合制备，以及使用的抗静电剂为以下物质的混合物的方法为5〜50巴：a）式（I）的中间体金属盐（a）b）邻氨基苯甲酸的金属盐通式（II）的酸其中有机基团R1是α）-CO-（CH2）x-CH3（IIa）或β）-CO-（CH2）y-CH = CH - （CH 2）z -CH 3（IIIβ），x，y和z各自为整数，x为6至18，y为1至16，z为1至16，y为4至17 + z，和c）通过使表氯醇和通式（IV）R 2 NH-R 3 -NH 2（IV）的脂族伯单胺或N-烷基亚烷基二胺反应得到的多胺，其中R 2是C 8 -C 24 - 烷基，R 3是C 2 -C 6-亚烷基。

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