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1. 发明申请

US20100209612A1 SILYL-FUNCTIONAL LINEAR PREPOLYMERS, PRODUCTION AND USE THEREOF 审中-公开
标题翻译：丝素官能线性预聚物，生产和使用
公开(公告)号：US20100209612A1
公开(公告)日：2010-08-19
申请号：US12708573
申请日：2010-02-19
申请人： Haitao Rong , Peter Grejwe , Jürgen Groll , Christine Mohr , Marina Glesius , Martin Möller
发明人： Haitao Rong , Peter Grejwe , Jürgen Groll , Christine Mohr , Marina Glesius , Martin Möller
IPC分类号： B05D3/00 , C08L83/00 , C07F7/02
CPC分类号： C09D183/12 , A61K8/86 , A61Q5/00 , C08G65/336 , C08G77/46 , C08G2650/50 , C09D171/02
摘要： The invention relates to coatings with a contact angle hysteresis in water as measured by the tilting plate method of at most 20° made from silyl-terminated linear prepolymers which may cross-link with the surface of the substrate for coating, wherein the silyl-terminated linear prepolymers may be obtained by reaction of compounds of general formula (I): X-A-X′ (I), where A=a polyoxyalkylene chain of ethylene oxide units or ethylene oxide and propylene oxide units with a maximum fraction of 50 wt. % of propylene oxide units based on the weight of A, X═OH, NH2, NHR, NR2 or OR, wherein R independently=a linear or branched 1-10 C alkyl, a 6-10 C alkaryl or aralkyl or a 5-10 C aryl and the compound of general formula (I) has a number average molecular weight of at least 100 g/mol, with compounds of general formula (II) Y—B—Si(OR1)r(R2)3−r, where Y=a group reactive with OH, NH2, NHR and/or NR2, B=a chemical bond or a divalent low-molecular weight organic group with preferably 1-50 carbon atoms, OR1=a hydrolysable group, R2=a linear or branched 1-6C alkyl and r=a number from 1 to 3 and optionally unreacted hydrogen atoms on the group X and/or the group X′ are optionally alkylated. The invention further relates to the production of such coatings and the use of the silyl-terminated linear pre-polymers from production of such coatings and application in mixtures with stellate silylated prepolymers.
摘要翻译：本发明涉及通过倾斜板法测量的水中接触角滞后的涂层，其由甲硅烷基封端的线性预聚物制成，其可以与用于涂覆的基材的表面交联，其中甲硅烷基封端线性预聚物可以通过使通式（I）的化合物：XAX'（I）反应得到，其中A =环氧乙烷单元的聚氧化烯链或环氧乙烷和环氧丙烷单元，最大分数为50wt。基于A，X = OH，NH 2，NHR，NR 2或OR的重量的环氧丙烷单元的％，其中R独立地为直链或支链的1-10C烷基，6-10C烷芳基或芳烷基或5- 10的芳基和通式（I）的化合物的数均分子量至少为100g / mol，与通式（Ⅱ）Y-B-Si（OR1）r（R2）3-r的化合物，其中Y =与OH，NH 2，NHR和/或NR 2反应的基团，B =具有优选1-50个碳原子的化学键或二价低分子量有机基团，OR 1 =可水解基团，R 2 =直链或支化的1-6C烷基和r = 1至3的数和任选的X基团和/或X'基团上未反应的氢原子任选被烷基化。本发明进一步涉及这种涂层的生产以及由这种涂层的生产使用甲硅烷基封端的线性预聚物以及与星状甲硅烷基化预聚物的混合物的应用。

2. 发明申请

US20100209613A1 MULTIFUNCTIONAL STELLATE PREPOLYMER MIXTURES, PRODUCTION AND USE AND COATINGS MADE THEREOF 有权
标题翻译：多功能硅酸盐预处理剂的混合物，生产和使用及其涂料
公开(公告)号：US20100209613A1
公开(公告)日：2010-08-19
申请号：US12709559
申请日：2010-02-22
申请人： Haitao Rong , Peter Grejwe , Jürgen Groll , Christine Mohr , Marina Glesius , Martin Möller
发明人： Haitao Rong , Peter Grejwe , Jürgen Groll , Christine Mohr , Marina Glesius , Martin Möller
IPC分类号： C08G77/00 , B05D3/02 , C11D3/37 , A61K8/89
CPC分类号： C08G83/00 , A61K8/86 , A61K2800/43 , A61K2800/57 , A61Q5/004 , A61Q5/065 , A61Q5/12 , A61Q19/10 , C08G18/10 , C08G18/4816 , C08G18/4837 , C08G18/718 , C08G83/002 , C08G2210/00 , C09D5/1662 , C09D175/08 , C09D201/02 , C11D3/373 , D06M15/643 , C08G18/755
摘要： The invention relates to coatings having a contact angle hysteresis with water measured by the sessile drop method of at most 20°. The coatings can be produced from a mixture of at least two different stellate prepolymers and/or stellate prepolymer/nanoparticle complexes which may cross-link to each other and to the surface of the substrate coated, wherein the stellate prepolymers and/or stellate prepolymer/nanoparticle complex have at least three hydrophilic polymer branches before cross-linking which are themselves soluble in water with on all or a part of the free ends thereof, silyl end groups R1 of general formula (I): R1=—CRa2—Si(ORb)r(Rc)3-r, where Ra=H or straight or branched chain 1-6C alkyl, ORb=a hydrolysable group, Rc=linear or branched chain 1-6C alkyl and r=a number from 1 to 3 and the optionally non silyl end group carrying ends have reactive end groups which a reactive with each other, with the substrate to be coated optional entities included in the coating and/or with the silyl end groups with the proviso the mixture (a) has at least one stellate prepolymer with 3-5 hydrophilic polymer branches and (b) at least one stellate prepolymer and/or a stellate prepolymer/nanoparticle complex with a least 6 hydrophilic polymer branches. The invention further relates to a method for production for said coatings and stellate prepolymers as used in the coatings. The invention furthermore relates to the use of the stellate prepolymers as additives in various materials for temporary or permanent anti-soiling treatment of surfaces.
摘要翻译：本发明涉及具有至多20°的无固定滴落法测量的与水接触角滞后的涂层。涂层可以由至少两种不同的星状预聚物和/或星状预聚物/纳米颗粒络合物的混合物制备，所述星状预聚物和/或星状预聚物/纳米颗粒复合物可以彼此交联并与涂覆的基材的表面交联，其中星状预聚物和/或星状预聚物/ 纳米颗粒络合物在交联之前具有至少三个亲水性聚合物分支，其自身可以在其全部或部分自由端上溶解在水中，通式（I）的甲硅烷基端基R1：R1 = -CRa2-Si（ORb ）r（Rc）3-r，其中R a = H或直链或支链1-6C烷基，ORb =可水解基团，Rc =直链或支链1-6C烷基，r = 1至3的数，任选的非甲硅烷基端基的端部具有彼此反应的反应性端基，待涂覆的底物包含在涂层中的任选实体和/或甲硅烷基端基，条件是混合物（a）具有至少一个星状预聚物与3-5亲水聚合物分支和（b）至少一种具有至少6个亲水性聚合物分支的星状预聚物和/或星状预聚物/纳米颗粒络合物。本发明还涉及用于涂料中的所述涂料和星状预聚物的生产方法。本发明还涉及星状预聚物作为各种材料中的添加剂用于表面的临时或永久性防污处理的用途。

3. 发明授权

US08816000B2 Multifunctional stellate prepolymer mixtures, production and use and coatings made thereof 有权
标题翻译：多功能星状预聚物混合物，其制备和使用以及涂层
公开(公告)号：US08816000B2
公开(公告)日：2014-08-26
申请号：US12709559
申请日：2010-02-22
申请人： Haitao Rong , Peter Greiwe , Jürgen Groll , Christine Mohr , Marina Glesius , Martin Möller
发明人： Haitao Rong , Peter Greiwe , Jürgen Groll , Christine Mohr , Marina Glesius , Martin Möller
IPC分类号： C08G83/00
CPC分类号： C08G83/00 , A61K8/86 , A61K2800/43 , A61K2800/57 , A61Q5/004 , A61Q5/065 , A61Q5/12 , A61Q19/10 , C08G18/10 , C08G18/4816 , C08G18/4837 , C08G18/718 , C08G83/002 , C08G2210/00 , C09D5/1662 , C09D175/08 , C09D201/02 , C11D3/373 , D06M15/643 , C08G18/755
摘要： The invention relates to coatings having a contact angle hysteresis with water measured by the sessile drop method of at most 20°. The coatings can be produced from a mixture of at least two different stellate prepolymers and/or stellate prepolymer/nanoparticle complexes which may cross-link to each other and to the surface of the substrate coated, wherein the stellate prepolymers and/or stellate prepolymer/nanoparticle complex have at least three hydrophilic polymer branches before cross-linking which are themselves soluble in water with on all or a part of the free ends thereof, silyl end groups R1 of general formula (I): R1=—CRa2—Si(ORb)r(Rc)3−r, where Ra=H or straight or branched chain 1-6C alkyl, ORb=a hydrolysable group, Rc=linear or branched chain 1-6C alkyl and r=a number from 1 to 3 and the optionally non silyl end group carrying ends have reactive end groups which a reactive with each other, with the substrate to be coated optional entities included in the coating and/or with the silyl end groups with the proviso the mixture (a) has at least one stellate prepolymer with 3-5 hydrophilic polymer branches and (b) at least one stellate prepolymer and/or a stellate prepolymer/nanoparticle complex with a least 6 hydrophilic polymer branches. The invention further relates to a method for production for said coatings and stellate prepolymers as used in the coatings. The invention furthermore relates to the use of the stellate prepolymers as additives in various materials for temporary or permanent anti-soiling treatment of surfaces.
摘要翻译：本发明涉及具有至多20°的无固定滴落法测量的与水接触角滞后的涂层。涂层可以由至少两种不同的星状预聚物和/或星状预聚物/纳米颗粒络合物的混合物制备，所述星状预聚物和/或星状预聚物/纳米颗粒复合物可以彼此交联并与涂覆的基材的表面交联，其中星状预聚物和/或星状预聚物/ 纳米颗粒络合物在交联之前具有至少三个亲水性聚合物分支，其自身可以在其全部或部分自由端上溶解在水中，通式（I）的甲硅烷基端基R1：R1 = -CRa2-Si（ORb ）r（Rc）3-r，其中R a = H或直链或支链1-6C烷基，ORb =可水解基团，Rc =直链或支链1-6C烷基，r = 1至3的数，任选的非甲硅烷基端基的端部具有彼此反应的反应性端基，待涂覆的底物包含在涂层中的任选实体和/或甲硅烷基端基，条件是混合物（a）具有至少一个星状预聚物与3-5亲水聚合物麸 c）和（b）至少一种具有至少6个亲水性聚合物分支的星状预聚物和/或星状预聚物/纳米颗粒络合物。本发明还涉及用于涂料中的所述涂料和星状预聚物的生产方法。本发明还涉及星状预聚物作为各种材料中的添加剂用于表面的临时或永久性防污处理的用途。

4. 发明申请

US20100081596A1 CLEANING COMPOSITIONS FOR HARD SURFACES 有权
标题翻译：清洁组合物硬表面
公开(公告)号：US20100081596A1
公开(公告)日：2010-04-01
申请号：US12517201
申请日：2007-12-04
申请人： Haitao Rong , Matthias Schweinsberg , Heinz-Dieter Soldanski , Marina Glesius
发明人： Haitao Rong , Matthias Schweinsberg , Heinz-Dieter Soldanski , Marina Glesius
IPC分类号： C11D3/34
CPC分类号： C11D3/3738 , C11D1/143 , C11D1/146 , C11D1/22 , C11D1/29 , C11D1/37 , C11D1/90 , C11D1/94 , C11D3/3742
摘要： Aqueous liquid compositions containing: (a) at least one alkyl ether sulphate (b) at least one multi-armed silyl polyalkoxylate of the formula (I) (H-A)n-Z-[A-B—Si(OR1)r(R2)3-r]m (I), where Z is an (m+n)-valent radical having at least three carbon atoms, A is a divalent polyoxyalkylene radical, wherein the m+n polyoxyalkylene radicals bound to Z can be different from one another, and wherein one radical A is in each case bound to Z via an oxygen atom belonging to Z, and one oxygen atom belonging to A is bound to B or hydrogen, B is a chemical bond or a divalent organic radical having 1 to 50 carbon atoms, OR1 is a hydrolysable group, R1 and R2 independently of one another are a linear or branched alkyl group having 1 to 6 carbon atoms and r is an integer from 1 to 3, and m is an integer ≧1 and n is 0 or an integer ≧1, and m+n has a value from 3 to 100, and (c) 0-50% of at least one alkylsulphonate and/or arylsulphonate; (d) 0-15% of at least one alkyl sulphate and/or (e) 0-20% of at least one amphoteric surfactant cause an improvement of the drying and draining behaviour in the cleaning of hard surfaces, in particular dishes.
摘要翻译：含有以下物质的水性液体组合物：（a）至少一种烷基醚硫酸盐（b）至少一种式（I）（HA）nZ- [AB-Si（OR1）r（R2）3-r的多臂甲硅烷基多烷氧基化物 ] m（I），其中Z是具有至少三个碳原子的（m + n）价基团，A是二价聚氧化烯基团，其中与Z结合的m + n聚氧化烯基团可以彼此不同，其中一个基团A在每种情况下都通过属于Z的氧原子与Z键合，并且属于A的一个氧原子与B或氢键合，B是化学键或具有1至50个碳原子的二价有机基团， OR1是可水解基团，R1和R2彼此独立地是具有1至6个碳原子的直链或支链烷基，r是1至3的整数，m是整数≥1且n是0或整数 ≥1，m + n的值为3〜100，（c）0-50％的至少一种烷基磺酸盐和/或芳基磺酸盐; （d）0-15％的至少一种烷基硫酸盐和/或（e）0-20％的至少一种两性表面活性剂导致清洁硬表面，特别是菜肴时的干燥和排水行为的改善。

5. 发明授权

US07998918B2 Cleaning compositions for hard surfaces comprising a silyl polyalkoxylate 有权
标题翻译：包含甲硅烷基聚烷氧基化物的硬表面的清洁组合物
公开(公告)号：US07998918B2
公开(公告)日：2011-08-16
申请号：US12517201
申请日：2007-12-04
申请人： Haitao Rong , Matthias Schweinsberg , Heinz-Dieter Soldanski , Marina Glesius
发明人： Haitao Rong , Matthias Schweinsberg , Heinz-Dieter Soldanski , Marina Glesius
IPC分类号： C11D9/36 , C11D1/29
CPC分类号： C11D3/3738 , C11D1/143 , C11D1/146 , C11D1/22 , C11D1/29 , C11D1/37 , C11D1/90 , C11D1/94 , C11D3/3742
摘要： Aqueous liquid compositions containing: (a) at least one alkyl ether sulphate (b) at least one multi-armed silyl polyalkoxylate of the formula (I) (H-A)n-Z-[A-B—Si(OR1)r(R2)3−r]m (I), where Z is an (m+n)-valent radical having at least three carbon atoms, A is a divalent polyoxyalkylene radical, wherein the m+n polyoxyalkylene radicals bound to Z can be different from one another, and wherein one radical A is in each case bound to Z via an oxygen atom belonging to Z, and one oxygen atom belonging to A is bound to B or hydrogen, B is a chemical bond or a divalent organic radical having 1 to 50 carbon atoms, OR1 is a hydrolysable group, R1 and R2 independently of one another are a linear or branched alkyl group having 1 to 6 carbon atoms and r is an integer from 1 to 3, and m is an integer ≧1 and n is 0 or an integer ≧1, and m+n has a value from 3 to 100, and (c) 0-50% of at least one alkylsulphonate and/or arylsulphonate; (d) 0-15% of at least one alkyl sulphate and/or (e) 0-20% of at least one amphoteric surfactant cause an improvement of the drying and draining behavior in the cleaning of hard surfaces, in particular dishes.
摘要翻译：含有以下物质的水性液体组合物：（a）至少一种烷基醚硫酸盐（b）至少一种式（I）（HA）nZ- [AB-Si（OR1）r（R2）3-r的多臂甲硅烷基多烷氧基化物 ] m（I），其中Z是具有至少三个碳原子的（m + n）价基团，A是二价聚氧化烯基团，其中与Z结合的m + n聚氧化烯基团可以彼此不同，其中一个基团A在每种情况下都通过属于Z的氧原子与Z键合，并且属于A的一个氧原子与B或氢键合，B是化学键或具有1至50个碳原子的二价有机基团， OR1是可水解基团，R1和R2彼此独立地是具有1至6个碳原子的直链或支链烷基，r是1至3的整数，m是整数≥1且n是0或整数 ≥1，m + n的值为3〜100，（c）0-50％的至少一种烷基磺酸盐和/或芳基磺酸盐; （d）0-15％的至少一种烷基硫酸盐和/或（e）0-20％的至少一种两性表面活性剂导致清洁硬表面，特别是菜肴时的干燥和排水行为的改善。

6. 发明申请

US20110251118A1 ADSORPTION AGENT FOR SEPARATING DYED COMPOUNDS FROM AQUEOUS FORMULATIONS 审中-公开
标题翻译：用于从水性配方中分离染料化合物的吸附剂
公开(公告)号：US20110251118A1
公开(公告)日：2011-10-13
申请号：US13164518
申请日：2011-06-20
申请人： Oliver Bedford , Daniela Kropp , Marina Glesius , Olaf Musolf
发明人： Oliver Bedford , Daniela Kropp , Marina Glesius , Olaf Musolf
IPC分类号： C11D3/37 , C08G65/336
CPC分类号： C08G65/336 , C08G18/2865 , C08G18/718 , C08G65/2606 , C08G65/2609
摘要： In order to separate dyes from aqueous solutions, an improved adsorption agent is proposed, which can be produced according to a method, wherein in a first reaction step, a multifunctional alcohol is reacted with an alkylene oxide into a star-shaped OH-terminated polyether. In a second reaction step, the polyether is reacted with a silane compound such that at an average more than one alkoxy silane group per molecule polyether is present, and in a third reaction step a cross-linking product is obtained by condensation in the presence of acids, wherein optionally further siloxane group-containing modifying agents can be incorporated, and wherein in a final treatment step, the cross-linked products obtained in said manner are separated and optionally dried or ground,
摘要翻译：为了从水溶液中分离染料，提出了一种改进的吸附剂，其可以根据一种方法制备，其中在第一反应步骤中，多官能醇与烯化氧反应成星形OH封端的聚醚。在第二反应步骤中，使聚醚与硅烷化合物反应，使得每分子聚醚存在平均多于一个烷氧基硅烷基团，并且在第三反应步骤中，在存在下，通过缩合得到交联产物酸，其中任选地可以加入另外含硅氧烷基的改性剂，并且其中在最终处理步骤中，以所述方式获得的交联产物被分离并任选地干燥或研磨，

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