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1. 发明授权

US09636657B2 Hydraulically set cement body for preservation of organic liquids 有权
公开(公告)号：US09636657B2
公开(公告)日：2017-05-02
申请号：US13661789
申请日：2012-10-26
申请人： Graham John Bratton , Kenneth George Mannering , Roger Leslie Brown , Neil McNeill Alford
发明人： Graham John Bratton , Kenneth George Mannering , Roger Leslie Brown , Neil McNeill Alford
IPC分类号： B01J20/02 , C04B28/04 , B01J20/28 , A23D9/00 , C04B111/00 , C04B111/80
CPC分类号： B01J20/02 , A23D9/00 , B01J20/28042 , B01J20/2805 , C04B28/04 , C04B2111/00284 , C04B2111/802 , C04B7/527 , C04B14/04 , C04B14/047 , C04B14/06 , C04B14/08 , C04B14/102 , C04B14/305 , C04B38/00
摘要： An hydraulically set oil-permeable cement body is provided in the form of a stand-alone block or briquette for preserving cooking oil during deep fat frying, said body. It has substantially no free water or having a low free water content for resisting damage on immersion in cooking oil and initial heating and is enclosed in packaging that resists ingress of water or water vapor The block or briquette consists of >50 wt % of a mixture of milled white OPC clinker and white OPC, optionally silica 1-2 wt % and/or titania (TiO2) 1-2 wt % and optionally further ingredients selected from calcium silicate, magnesium silicate, aluminum silicate, natural feldspars, natural sodium zeolites, natural calcium zeolites, synthetic sodium zeolites, synthetic calcium zeolites, wollastonite, calcium hydroxide, clays, pillared clays, activated clays/earths, talcs/kaolinite, amphiboles, granite porphyry, rhyolite, agalmatolite, porphyry, attapulgite and diatomaceous earth. It has the properties that calcium and magnesium substantially do not leach into the oil and that it is porous so that oil can diffuse into it and contaminants can be deposited on and within it.

2. 发明申请

US20130112607A1 HYDRAULICALLY SET CEMENT BODY FOR PRESERVATION OF ORGANIC LIQUIDS 有权
标题翻译：液压机构用于保存有机液体
公开(公告)号：US20130112607A1
公开(公告)日：2013-05-09
申请号：US13661789
申请日：2012-10-26
申请人： Graham John Bratton , Kenneth George Mannering , Roger Leslie Brown , Neil McNeill Alford
发明人： Graham John Bratton , Kenneth George Mannering , Roger Leslie Brown , Neil McNeill Alford
IPC分类号： B01J20/02
CPC分类号： B01J20/02 , A23D9/00 , B01J20/28042 , B01J20/2805 , C04B28/04 , C04B2111/00284 , C04B2111/802 , C04B7/527 , C04B14/04 , C04B14/047 , C04B14/06 , C04B14/08 , C04B14/102 , C04B14/305 , C04B38/00
摘要： An hydraulically set oil-permeable cement body is provided in the form of a stand-alone block or briquette for preserving cooking oil during deep fat frying, said body. It has substantially no free water or having a low free water content for resisting damage on immersion in cooking oil and initial heating and is enclosed in packaging that resists ingress of water or water vapour The block or briquette consists of >50 wt % of a mixture of milled white OPC clinker and white OPC, optionally silica 1-2 wt % and/or titania (TiO2) 1-2 wt % and optionally further ingredients selected from calcium silicate, magnesium silicate, aluminium silicate, natural feldspars, natural sodium zeolites, natural calcium zeolites, synthetic sodium zeolites, synthetic calcium zeolites, wollastonite, calcium hydroxide, clays, pillared clays, activated clays/earths, talcs/kaolinite, amphiboles, granite porphyry, rhyolite, agalmatolite, porphyry, attapulgite and diatomaceous earth. It has the properties that calcium and magnesium substantially do not leach into the oil and that it is porous so that oil can diffuse into it and contaminants can be deposited on and within it.
摘要翻译：一种液压设置的透水性水泥体以独立块体或块状的形式提供，用于在所述身体的油炸油炸期间保存食用油。它基本上没有游离水或具有低的游离水含量，用于抵抗在食用油浸渍和初始加热时的损害，并且被封装在防止水或水蒸汽进入的包装中。块或团块由> 50重量％的混合物组成的白色OPC熟料和白色OPC，任选的二氧化硅1-2wt％和/或二氧化钛（TiO 2）1-2wt％和任选的其它成分选自硅酸钙，硅酸镁，硅酸铝，天然长石，天然钠沸石，天然钙沸石，合成钠沸石，合成钙沸石，硅灰石，氢氧化钙，粘土，柱状粘土，活性粘土/土，滑石/高岭石，双极体，花岗岩斑岩，流纹岩，琼脂岩，斑岩，绿坡缕石和硅藻土。它具有钙和镁基本上不浸入油中的特性，并且它是多孔的，使得油可以扩散到其中，并且污染物可以沉积在其中并且内部。

3. 发明授权

US08389037B2 Preservation of organic liquids 有权
标题翻译：保存有机液体
公开(公告)号：US08389037B2
公开(公告)日：2013-03-05
申请号：US12452984
申请日：2008-08-04
申请人： Graham John Bratton , Neil McNeill Alford , Kenneth George Mannering , Roger Leslie Brown
发明人： Graham John Bratton , Neil McNeill Alford , Kenneth George Mannering , Roger Leslie Brown
IPC分类号： C11B3/10 , A47J37/12
CPC分类号： C11B3/10 , C04B28/04 , C04B2111/00793 , C04B2111/802 , C04B7/006 , C04B38/00 , C04B38/10 , C04B7/52
摘要： A method is provided for preserving cooking oil which may be cold or heated or during frying operations, which comprises in situtreatment of the oil withat least one oil-permeable cement body which has been hydraulically hardened from a paste comprising cement clinker and cement e.g. white OPC clinker and white OPC. The invention further comprises cooking oil having therein at least one oil-permeable cement body which has been hydraulically hardened from a paste comprising cement clinker and cement and an oil-permeable cement body for use in the above method.
摘要翻译：提供了一种用于保存烹饪油的方法，其可以是冷的或加热的或在油炸操作期间，其包括用至少一个油渗透的水泥体进行油的处理，该水泥体由包含水泥熟料和水泥的浆料水硬化。白色OPC熟料和白色OPC。本发明还包括在其中具有至少一个透水性水泥体的烹饪油，所述油渗透性水泥体已经由包含水泥熟料和水泥的浆料以及用于上述方法的透油性水泥体水硬化。

4. 发明申请

US20110250330A1 PRESERVATION OF ORGANIC LIQUIDS 有权
标题翻译：有机液体的保存
公开(公告)号：US20110250330A1
公开(公告)日：2011-10-13
申请号：US12452984
申请日：2008-08-04
申请人： Graham John Bratton , Neil McNeill Alford , Kenneth George Mannering , Roger Leslie Brown
发明人： Graham John Bratton , Neil McNeill Alford , Kenneth George Mannering , Roger Leslie Brown
IPC分类号： A23D9/06 , B65B63/08 , C11B3/10
CPC分类号： C11B3/10 , C04B28/04 , C04B2111/00793 , C04B2111/802 , C04B7/006 , C04B38/00 , C04B38/10 , C04B7/52
摘要： A method is provided for preserving cooking oil which may be cold or heated or during frying operations, which comprises in situ treatment of the oil withal least one oil-permeable cement body which has been hydraulically hardened from a paste comprising cement clinker and cement e.g. white OPC clinker and white OPC. The invention further comprises cooking oil having therein at least one oil-permeable cement body which has been hydraulically hardened from a paste comprising cement clinker and cement and an oil-permeable cement body for use in the above method.
摘要翻译：提供了一种用于保存烹饪油的方法，其可以是冷的或加热的或在油炸操作期间，其包括用至少一个油渗透的水泥体进行原位处理，该水泥体由包含水泥熟料和水泥的糊状物水硬化。白色OPC熟料和白色OPC。本发明还包括在其中具有至少一个透水性水泥体的烹饪油，所述油渗透性水泥体已经由包含水泥熟料和水泥的浆料以及用于上述方法的透油性水泥体水硬化。

5. 发明申请

US20090196968A1 PRESERVATION OF ORGANIC LIQUIDS 有权
标题翻译：有机液体的保存
公开(公告)号：US20090196968A1
公开(公告)日：2009-08-06
申请号：US12309900
申请日：2007-08-03
申请人： Graham John Bratton , Neil McNeill Alford , Kenneth George Mannering , Roger Leslie Brown
发明人： Graham John Bratton , Neil McNeill Alford , Kenneth George Mannering , Roger Leslie Brown
IPC分类号： A23C15/20 , A47J37/12
CPC分类号： C11B3/10
摘要： A method is provided for treating cooking oil during frying operations, which comprises in situ treatment of the oil with a source of calcium or magnesium combined with silicate such that the calcium or magnesium substantially does not leach into the oil. The filter treatment materials may be cement clinker, OPC, calcium silicate and combinations or mixtures thereof e.g. a combination of white OPC clinker and white OPC. The filter treatment materials may be in the form of a free briquette or block immersed in the oil. In other embodiments a decontaminating or filter cartridge is provided for fitting to a deep oil or fat cooker or a frying basket and comprises a foraminous housing containing filtering or decontaminant material. The cartridge may be used in association with a deep oil or fat fryer having a base formed with a depression defining a cool spot, the cartridge fitting in or on said cool spot.
摘要翻译：提供了一种用于在油炸操作期间处理烹饪油的方法，其包括用钙或镁与硅酸盐结合的原料处理油，使得钙或镁基本上不浸入油中。过滤处理材料可以是水泥熟料，OPC，硅酸钙及其组合或混合物。白色OPC熟料和白色OPC的组合。过滤处理材料可以是浸入油中的游离团块或块的形式。在其他实施例中，提供净化或过滤筒用于装配到深油或脂肪炊具或煎锅篮，并且包括含有过滤或去污剂材料的多孔壳体。墨盒可以与深油或油炸锅结合使用，该深油或油炸锅具有形成有限定冷点的凹陷的底部，该墨盒装配在所述冷点中或所述冷点上。

6. 发明授权

US06635594B1 Membrane pre-treatment process 失效
标题翻译：膜预处理过程
公开(公告)号：US06635594B1
公开(公告)日：2003-10-21
申请号：US09806817
申请日：2001-04-03
申请人： Graham John Bratton , Karon Doreen Buck , Timothy de Villiers Naylor , Martin Grayling Major
发明人： Graham John Bratton , Karon Doreen Buck , Timothy de Villiers Naylor , Martin Grayling Major
IPC分类号： B01J2906
CPC分类号： B01D63/066 , B01D71/028 , B01J29/06 , B01J37/0246
摘要： An improved porous substrate for zeolite membranes is formed by coating the substrate with a layer of zeolite particles of a narrow particle distribution size of between 20 and 0.01 microns.
摘要翻译：用于沸石膜的改进的多孔基材是通过用窄的颗粒分布尺寸为20至0.01微米的沸石颗粒层涂覆基材而形成的。

7. 发明授权

US06383563B1 Membrane 失效
标题翻译：膜
公开(公告)号：US06383563B1
公开(公告)日：2002-05-07
申请号：US09155316
申请日：1998-09-25
申请人： Graham John Bratton , Karon Doreen Buck , Timothy De Villiers Naylor
发明人： Graham John Bratton , Karon Doreen Buck , Timothy De Villiers Naylor
IPC分类号： B05D500
CPC分类号： B01J31/124 , B01D67/0051 , B01D67/0093 , B01D69/10 , B01D69/105 , B01D71/028 , B01D2325/10 , B01J31/0274 , B01J37/0246
摘要： A process for treating zeolite membranes to improve their performance and to improve their coherence consists of forming a film of zeolite material on a porous support to form a zeolite membrane, contacting the membrane with tetraethylorthosilicate (TEOS), and reacting said TEOS with said zeolite membrane to form a supported membrane with open pores without defective pin holes. The process may further comprise pre-treatment of the porous support with a zeolite initiating agent, or post-treatment of the treated membrane with a silicic or polysilicic acid.
摘要翻译：用于处理沸石膜以提高其性能并改善其相干性的方法包括在多孔载体上形成沸石材料膜以形成沸石膜，使膜与原硅酸四乙酯（TEOS）接触，并使所述TEOS与所述沸石膜以形成具有开孔的支撑膜，而没有有缺陷的针孔。该方法可以进一步包括用沸石引发剂预处理多孔载体，或用硅酸或聚硅酸对经处理的膜进行后处理。

8. 发明申请

US20100170851A1 MEMBRANE STRUCTURES AND THEIR PRODUCTION AND USE 审中-公开
公开(公告)号：US20100170851A1
公开(公告)日：2010-07-08
申请号：US12601910
申请日：2008-05-23
申请人： Graham John Bratton , Colin Danny Murton
发明人： Graham John Bratton , Colin Danny Murton
IPC分类号： C02F1/00 , B01D63/06
CPC分类号： B01D71/028 , B01D63/066 , B01D67/0051 , B01D67/0093 , B01D69/105 , B01D2313/04 , B01D2319/04 , B01D2323/30 , B01D2323/42 , C02F1/444 , Y02A20/131
摘要： A method is provided for forming zeolite membranes in internal surfaces of a plurality of conduits in a cylindrical porous ceramic monolith, the conduits extending from one end of the monolith to the other and being disposed in a single annulus, said method including a step of: flowing a pre-treatment liquid (50) including a zeolite initiating agent into the conduits; causing at least part of a carrier liquid component of the treatment liquid to flow from the FIG. 4 conduits into and through the body of the monolith to the exterior; and causing zeolite crystals to be deposited in the porous internal surfaces of the conduits as the carrier liquid component flows into the monolith. The substrates may be pre-conditioned for membrane formation by a method which comprises: (a) forming an aqueous suspension of zeolite particles; and (b) passing the suspension alternately (i) through the tubular conduits and (ii) out through the walls of the tubular conduits so as to deposit zeolite particles on the porous inner surfaces of the tubular conduits; wherein the porous substrates are treated in chambers (62) arranged e.g annularly and the suspension is supplied to the chambers from a first common manifold (58) via respective delivery tubes and is recovered via recovery tubes leading to a second common manifold (66), the first and second manifolds and the supply and recovery tubes being configured so that the branch path to and from each chamber is substantially the same. After pre-conditioning, formation of membranes may be by depositing or crystallising a zeolite membrane on the zeolite particles by gel crystallization. A membrane structure is also provided which comprises a tubular porous ceramic monolith having tubular conduits each having an internal diameter of 5 to 9 mm formed within the monolith with a zeolite membrane formed on the internal surface of each of the conduits, wherein either there are five or more conduits disposed in a singe annulus. The invention also provides methods for removal of water from organic liquids salts or other contaminants and methods for the purification of water using the above membrane structures e.g. to remove residual water from ethanol or butanol or to produce high purity water.

9. 发明申请

US20100090165A1 PROCESS AND APPARATUS FOR TREATMENT OF ORGANIC SOLVENTS 审中-公开
公开(公告)号：US20100090165A1
公开(公告)日：2010-04-15
申请号：US12530738
申请日：2008-03-13
申请人： Graham John Bratton , Colin Danny Murton
发明人： Graham John Bratton , Colin Danny Murton
IPC分类号： B01F1/00 , B01D35/18
CPC分类号： B01D61/362 , B01D1/00 , B01D3/002 , B01D3/145 , B01D5/0057 , B01D63/066 , B01D65/08 , B01D71/028 , B01D2321/2033
摘要： A method is provided for separating water from an organic solvent which comprises: passing the solvent through at least one conduit within a porous ceramic with a zeolite membrane formed on the internal surface of the conduit; recovering solvent of reduced water content from the conduit; and recovering water which has passed via the membrane through the ceramic to the exterior thereof. The velocity at which the solvent is passed through the conduit induces turbulent flow for scouring solids from the surface of the membrane and reducing or preventing concentration of the organic solvent on the membrane surface e.g. at 1-6 m/s The invention also provides a method of separating water from an organic solvent which comprises: supplying the solvent to first, second and third tanks; circulating solvent between the first tank and zeolite membranes to separate water therefrom; recovering separated water from the membranes; supplying fresh solvent to the second tank; recovering solvent separated of water from the third tank in heat-exchange relationship with solvent supplied to the second tank; and on completion of water separation initiating at least a first new processing cycle in which recovery is from the first tank, circulation is from the second tank and supply is to the third tank. On completion of said first new processing cycle at least a second cycle may be initiated in which supply is to the first tank, recovery is from the second tank and circulation is from the third tank. Apparatus is also provided for separating first and second fluids, comprising: a multiplicity of tubular porous ceramic monoliths having tubular conduits formed within the monolith with a zeolite membrane formed on the internal surface of each of the conduits; first and second support plates each formed with a multiplicity of holes for receiving the ends of the monoliths for supporting said monoliths in spaced parallel relationship, the holes where they open to outer faces of the support plates being formed with counterbores; O-rings in the counterbores for supporting the monoliths in the apertures each at a small clearance from its respective hole; first and second cover plates attached to the first and second support plates and formed with holes corresponding to the holes in the support plate leading to enlarged inwardly facing regions in which ends of the monoliths are received, attachment of the cover plate compressing the O-rings to seal against the monolith; and a housing having a flow passage in which the first and second support Phoenix,002-PCT26 plates are welded; wherein the support plates have outer surfaces machined flat after the support plates have been welded in position.

10. 发明申请

US20100006503A1 MEMBRANE STRUCTURES AND THEIR PRODUCTION AND USE 审中-公开
公开(公告)号：US20100006503A1
公开(公告)日：2010-01-14
申请号：US12530749
申请日：2008-03-13
申请人： Graham John Bratton , Colin Danny Murton
发明人： Graham John Bratton , Colin Danny Murton
IPC分类号： B01D61/00 , B01D69/04 , C07C29/76
CPC分类号： B01D61/362 , B01D63/066 , B01D67/0051 , B01D67/0069 , B01D67/0093 , B01D71/028 , B01D2323/30
摘要： A method is provided for forming zeolite membranes in internal surfaces of a plurality of conduits in a cylindrical porous ceramic monolith, the conduits extending from one end of the monolith to the other, said method including a step of: flowing a pre-treatment liquid including a zeolite initiating agent into the conduits; causing at least part of a carrier liquid component of the treatment liquid to flow from the conduits into and through the body of the monolith to the exterior; and causing zeolite crystals to be deposited in the porous internal surfaces of the conduits as the carrier liquid component flows into the monolith. The substrates may be pre-conditioned for membrane formation by a method which comprises: (a) forming an aqueous suspension of zeolite particles; and (b) passing the suspension alternately (i) through the tubular conduits and (ii) out through the walls of the tubular conduits so as to deposit a layer of zeolite particles on the inner surfaces of the tubular conduits; wherein the porous substrates are treated in chambers arranged e.g in annularly and the suspension is supplied to the chambers from a first common manifold via respective delivery tubes and is recovered via recovery tubes leading to a second common manifold, the first and second manifolds and the supply and recovery tubes being configured so that the branch path to and from each chamber is substantially the same. After pre-conditioning, formation of membranes may be by depositing or crystallizing a zeolite membrane on the zeolite particles by gel crystallization. A membrane structure is also provided which comprises a tubular porous ceramic monolith having tubular conduits each having an internal diameter of (5) to (9) mm formed within the monolith with a zeolite membrane formed on the internal surface of each of the conduits, wherein either there are four conduits and the monolith is longer than 600 mm or there are five or more conduits. The invention also provides methods for removal of water from organic liquids and methods for the purification of water using the above membrane structures e.g. to remove residual water from ethanol or butanol or to produce high purity water.

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