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1. 发明授权

US6034142A Method for recycling aromatic polycarbonates 失效
标题翻译：芳烃聚碳酸酯的回收方法
公开(公告)号：US6034142A
公开(公告)日：2000-03-07
申请号：US989458
申请日：1997-12-12
申请人： Godavarthi Satyanarayana Varadarajan , Joseph Anthony King, Jr. , Bhaskar Bhairavnath Idage , Swaminathan Sivaram , Vishnu Ramchandra Ranade
发明人： Godavarthi Satyanarayana Varadarajan , Joseph Anthony King, Jr. , Bhaskar Bhairavnath Idage , Swaminathan Sivaram , Vishnu Ramchandra Ranade
IPC分类号： C08J11/08 , C08J11/04 , C08J11/20
CPC分类号： C08J11/08 , C08J2369/00 , Y02W30/701
摘要： Polycarbonates are recycled without the need for chemical modification by dissolution in a solvent followed by removal of any insoluble materials and precipitation by addition of a non-solvent. The precipitation step may be followed by solid state polymerization of the recycled polycarbonate. Particularly when solid state polymerization is to be performed, the use of a combination of solvent and non-solvent which produces a crystalline intermediate is performed, and use of a modifying reagent increasing the hydroxy end group concentration of the polycarbonate may be advantageous.
摘要翻译：聚碳酸酯被再循环，而不需要通过溶解在溶剂中进行化学改性，然后除去任何不溶物并通过加入非溶剂沉淀。沉淀步骤之后可以再循环聚碳酸酯的固态聚合。特别是当进行固态聚合时，进行使用产生结晶中间体的溶剂和非溶剂的组合，并且使用增加聚碳酸酯的羟基端基浓度的改性剂可能是有利的。

2. 发明授权

US5717056A Method for preparing polycarbonate by solid state polymerization 失效
标题翻译：通过固态聚合制备聚碳酸酯的方法
公开(公告)号：US5717056A
公开(公告)日：1998-02-10
申请号：US767740
申请日：1996-12-17
申请人： Godavarthi Satyanarayana Varadarajan , Swaminathan Sivaram , Bhaskar Bhairavnath Idage , Joseph Anthony King, Jr.
发明人： Godavarthi Satyanarayana Varadarajan , Swaminathan Sivaram , Bhaskar Bhairavnath Idage , Joseph Anthony King, Jr.
IPC分类号： C08G64/14 , C08G64/20 , C08G64/30 , C08G64/42 , C08G64/00
CPC分类号： C08G64/42 , C08G64/14 , C08G64/20 , C08G64/307
摘要： Solid state polycarbonate formation comprises an initial step of converting a precursor polycarbonate to an enhanced crystallinity precursor polycarbonate and a second step of polymerizing said enhanced crystallinity precursor polycarbonate in the solid state. Several options are employed. These include modifying the precursor polycarbonate by contact with a dihydroxy compound or diaryl carbonate, conversion of the precursor polycarbonate to the enhanced crystallinity polymer by contact with at least one compound selected from the group consisting of alkali metal hydroxides, tetraalkylammonium hydroxides, tetraalkylammonium carboxylates, tetraalkylphosphonium hydroxides and tetraalkylphosphonium carboxylates, and conducting the solid state polymerization in the presence of a catalytic amount of at least one tetralkylammonium or tetraalkylphosphonium carboxylate. The preferred tetralkylammonium compounds are tetramethylammonium maleate and tetramethylammonium hydroxide. Polymerization may be conducted in the presence of a solvent resistance-imparting monomer such as hydroquinone or resorcinol or a branching agent such as 1,1,1-tris(4-hydroxyphenyl)ethane.
摘要翻译：固体聚碳酸酯形成包括将前体聚碳酸酯转化为增强的结晶度前体聚碳酸酯的初始步骤和将固体状态的所述增强的结晶度前体聚碳酸酯聚合的第二步骤。采用了几个选项。这些包括通过与二羟基化合物或碳酸二芳基酯接触来改性前体聚碳酸酯，通过与至少一种选自碱金属氢氧化物，四烷基铵氢氧化物，四烷基铵羧酸盐，四烷基鏻盐的化合物接触，将前体聚碳酸酯转化为增强的结晶度聚合物氢氧化物和四烷基鏻羧酸盐，并在催化量的至少一种四烷基铵或四烷基鏻羧酸盐的存在下进行固态聚合。优选的四烷基铵化合物是马来酸四甲基铵和氢氧化四甲基铵。聚合可以在耐溶剂性单体如氢醌或间苯二酚或支化剂如1,1,1-三（4-羟基苯基）乙烷的存在下进行。

3. 发明授权

US6143859A Copolycarbonate preparation by solid state polymerization 有权
标题翻译：通过固态聚合制备共聚碳酸酯
公开(公告)号：US6143859A
公开(公告)日：2000-11-07
申请号：US370433
申请日：1999-08-09
申请人： Gautam Chatterjee , Godavarthi Satyanarayana Varadarajan , James Day , Patrick Joseph McCloskey , Bhaskar Bhairavnath Idage , Joseph Anthony King, Jr. , Arun Savalaram Jadhav
发明人： Gautam Chatterjee , Godavarthi Satyanarayana Varadarajan , James Day , Patrick Joseph McCloskey , Bhaskar Bhairavnath Idage , Joseph Anthony King, Jr. , Arun Savalaram Jadhav
IPC分类号： C08G64/06 , C08G64/18 , C08G64/20 , C08G64/00
CPC分类号： C08G64/20 , C08G64/06 , C08G64/183
摘要： Copolycarbonates containing such structural units as birefringence-reducing or "soft block" units are prepared by conducting a reaction, such as melt polymerization or equilibration, between a precursor polycarbonate and a monomer, polycarbonate oligomer or high molecular weight polycarbonate which is a source of other structural units. The crystallinity of the resulting precursor copolycarbonate or one of the reagents employed in its preparation is enhanced and the precursor copolycarbonate is subjected to solid state polymerization.
摘要翻译：通过在前体聚碳酸酯和单体，聚碳酸酯低聚物或高分子量聚碳酸酯之间进行诸如熔融聚合或平衡的反应来制备含有诸如双折射降低或“软嵌段”单元的结构单元的共聚碳酸酯结构单位。得到的前体共聚碳酸酯或其制备中使用的试剂之一的结晶度提高，前体共聚碳酸酯进行固态聚合。

4. 发明授权

US06333394B1 Copolycarbonate preparation by solid state polymerization 有权
标题翻译：通过固态聚合制备共聚碳酸酯
公开(公告)号：US06333394B1
公开(公告)日：2001-12-25
申请号：US09379234
申请日：1999-08-23
申请人： Christian Maria Emile Bailly , Bhaskar Bhairavnath Idage , Swaminathan Sivaram , Nayaku Nivarati Chavan , Rein Mollerus Faber , Shamal Karunakaran Menon , Gautam Chatterjee , Godavarthi Satyana Varadarajan , James Day , Patrick Joseph McCloskey , Joseph Anthony King, Jr. , Arun Savalaram Jadhav
发明人： Christian Maria Emile Bailly , Bhaskar Bhairavnath Idage , Swaminathan Sivaram , Nayaku Nivarati Chavan , Rein Mollerus Faber , Shamal Karunakaran Menon , Gautam Chatterjee , Godavarthi Satyana Varadarajan , James Day , Patrick Joseph McCloskey , Joseph Anthony King, Jr. , Arun Savalaram Jadhav
IPC分类号： C08G6400
CPC分类号： C08G64/20 , C08G64/06 , C08G64/14 , C08G64/183 , C08G64/307
摘要： Copolycarbonates containing such structural units as birefringence-reducing or “soft block” units are prepared by conducting a reaction, such as melt polymerization or equilibration, between a precursor polycarbonate and a monomer, polycarbonate oligomer or high molecular weight polycarbonate which is a source of other structural units. The crystallinity of the resulting precursor copolycarbonate or one of the reagents employed in its preparation is enhanced and the precursor copolycarbonate is subjected to solid state polymerization.
摘要翻译：通过在前体聚碳酸酯和单体，聚碳酸酯低聚物或高分子量聚碳酸酯之间进行诸如熔融聚合或平衡的反应来制备含有诸如双折射降低或“软嵌段”单元的结构单元的共聚碳酸酯结构单位。得到的前体共聚碳酸酯或其制备中使用的试剂之一的结晶度提高，前体共聚碳酸酯进行固态聚合。

5. 发明授权

US5905135A Method of preparing polycarbonates by solid state polymerization 失效
标题翻译：通过固态聚合制备聚碳酸酯的方法
公开(公告)号：US5905135A
公开(公告)日：1999-05-18
申请号：US986448
申请日：1997-12-08
申请人： Bhaskar Bhairavnath Idage , Swaminathan Sivaram , Godavarthi Satyanaryana Varadarajan , Joseph Anthony King, Jr.
发明人： Bhaskar Bhairavnath Idage , Swaminathan Sivaram , Godavarthi Satyanaryana Varadarajan , Joseph Anthony King, Jr.
IPC分类号： C08G64/30 , C08G64/40 , C08G64/00
CPC分类号： C08G64/40 , C08G64/30
摘要： Crystallization of precursor polycarbonates prior to solid state polymerization is achieved by contact with a non-solvent comprising, at least in part, a dialkyl carbonate such as dimethyl carbonate. The non-solvent can be a mixture, typically of dimethyl carbonate with water or an alkanol such as methanol.
摘要翻译：在固态聚合之前，前体聚碳酸酯的结晶通过与至少部分由碳酸二烷基酯如碳酸二甲酯组成的非溶剂的接触来实现。非溶剂可以是通常为碳酸二甲酯与水或链烷醇如甲醇的混合物。

6. 发明授权

US6042920A Optical quality copolycarbonates containing polyoxyalkylene carbonate units 有权
标题翻译：含有聚碳酸亚烷基酯单元的光学质量共聚碳酸酯
公开(公告)号：US6042920A
公开(公告)日：2000-03-28
申请号：US131218
申请日：1998-08-07
申请人： Gautam Chatterjee , Joseph Anthony King, Jr. , Donald George LeGrand , Godavarthi Satyanarayana Varadarajan
发明人： Gautam Chatterjee , Joseph Anthony King, Jr. , Donald George LeGrand , Godavarthi Satyanarayana Varadarajan
IPC分类号： C08G64/16 , C08G64/18 , C08G64/30 , G11B7/253 , B32B3/00
CPC分类号： C08G64/183 , C08G64/30 , Y10S428/913 , Y10S430/146 , Y10T428/21
摘要： Copolycarbonates comprise structural units derived from a bisphenol such as bisphenol A, a spiro(bis)indane bisphenol such as 6,6'-dihdyroxy-3,3,3',3'-tetramethyl-1,1'-spiro(bis)indane and a polyoxyalkylene glycol such as polyethylene glycol. These copolycarbonates have high processability and are expected to have low birefringence. They are useful for the fabrication of optical disks.
摘要翻译：共聚碳酸酯包括衍生自双酚的结构单元如双酚A，螺（双）茚满双酚如6,6'-二羟基-3,3,3'，3'-四甲基-1,1'-螺（双）茚满和聚氧亚烷基二醇如聚乙二醇。这些共聚碳酸酯具有高加工性，并且预期具有低双折射。它们对于制造光盘是有用的。

7. 发明授权

US5705696A Extractive method for the preparation of quaternary salts 失效
标题翻译：萃取法制备季盐
公开(公告)号：US5705696A
公开(公告)日：1998-01-06
申请号：US691168
申请日：1996-08-01
申请人： Joseph Anthony King, Jr.
发明人： Joseph Anthony King, Jr.
IPC分类号： C07C209/00 , C07D233/58 , C07F9/54 , C07C209/68 , C07F9/02
CPC分类号： C07C209/00 , C07F9/5407
摘要： Quaternary (e.g., tetraalkylammonium and tetraalkylphosphonium) salts containing non-halide anions are prepared by performing an anion exchange reaction by liquid-liquid extraction with a chlorinated solvent of a mixture of an aqueous solution an alkali metal salt of the anion and a corresponding quaternary halide.
摘要翻译：通过使用阴离子的碱金属盐的水溶液和相应的季卤化物的混合物的氯化溶剂进行液 - 液萃取，进行阴离子交换反应来制备含有非卤素阴离子的第四纪（例如四烷基铵和四烷基鏻）盐。

8. 发明授权

US5663406A Formation of carbonate esters and orthocarbonates 失效
标题翻译：碳酸酯和原碳酸酯的形成
公开(公告)号：US5663406A
公开(公告)日：1997-09-02
申请号：US758108
申请日：1996-11-25
申请人： Joseph Anthony King, Jr. , Robert Edgar Colborn , Deborah Ann Haitko , Jimmy Lynn Webb
发明人： Joseph Anthony King, Jr. , Robert Edgar Colborn , Deborah Ann Haitko , Jimmy Lynn Webb
IPC分类号： C07C68/00 , C07C68/06
CPC分类号： C07C68/00
摘要： A carbonate ester is produced by the metal-induced reaction of a hydroxy compound with a sulfur compound in a melt process. An orthocarbonate can also be produced. The orthocarbonate can be converted into carbonate ester in a subsequent operation.
摘要翻译：通过在熔融过程中羟基化合物与硫化合物的金属诱导反应来生产碳酸酯。也可以生产原碳酸酯。在随后的操作中，原碳酸酯可以转化为碳酸酯。

9. 发明授权

US08497010B2 Breathable low-emissivity metalized sheets 失效
标题翻译：透气低发射金属板
公开(公告)号：US08497010B2
公开(公告)日：2013-07-30
申请号：US11978102
申请日：2007-10-25
申请人： Ioannis V Bletsos , Edmee Lydie Marie-Jeanne Devaquet , Joseph Anthony King, Jr. , Michael G Mikhael , Jose Manuel Rodriguez-Parada , Angelo Yializis
发明人： Ioannis V Bletsos , Edmee Lydie Marie-Jeanne Devaquet , Joseph Anthony King, Jr. , Michael G Mikhael , Jose Manuel Rodriguez-Parada , Angelo Yializis
IPC分类号： B32B3/24
CPC分类号： E04D13/1625 , B32B5/022 , B32B5/024 , B32B5/22 , B32B5/26 , B32B2250/20 , B32B2255/02 , B32B2255/205 , B32B2255/26 , B32B2255/28 , B32B2260/021 , B32B2260/046 , B32B2307/304 , B32B2307/724 , B32B2307/7242 , B32B2307/7265 , B32B2419/00 , B32B2607/00 , C23C14/562 , D06N5/00 , D06N7/0094 , D06N2209/123 , E04B1/625 , E04B2001/7691 , E04D12/002 , E04D2015/047 , Y10T428/12361 , Y10T428/24322 , Y10T428/249953 , Y10T428/249955 , Y10T428/24998 , Y10T428/249987 , Y10T442/2139 , Y10T442/2148 , Y10T442/3398 , Y10T442/3439 , Y10T442/657
摘要： A moisture vapor permeable metalized composite sheet is formed by coating a moisture vapor permeable sheet with at least one metal layer and at least one outer organic coating layer. The moisture vapor permeability of the composite sheet is at least about 80% of the moisture vapor permeability of the starting sheet. The composite sheet provides a barrier to air and liquid water infiltration while having high moisture vapor permeability and good thermal barrier properties. The composite sheet material is suitable for use as a building construction wrap such as roof lining and house wrap.
摘要翻译：通过用至少一个金属层和至少一个外部有机涂层涂覆水分蒸汽透过性片材来形成透湿蒸气的金属化复合片材。复合片材的透湿度至少为起始片材的透湿度的约80％。复合片材对空气和液体水渗透提供屏障，同时具有高的透湿度和良好的隔热性能。复合片材适用于屋顶衬砌和房屋包装等建筑施工包装。

10. 发明授权

US5969086A Quaternary bisphenolates, methods for their preparation, and uses thereof 失效
标题翻译：第四纪双酚盐，其制备方法及其用途
公开(公告)号：US5969086A
公开(公告)日：1999-10-19
申请号：US990390
申请日：1997-12-15
申请人： Jimmy Lynn Webb , Thomas Link Guggenheim , Robert Joseph Nick , Patrick Joseph McCloskey , Joseph Anthony King, Jr.
发明人： Jimmy Lynn Webb , Thomas Link Guggenheim , Robert Joseph Nick , Patrick Joseph McCloskey , Joseph Anthony King, Jr.
IPC分类号： B01J31/02 , C07C277/08 , C07C279/02 , C07C319/20 , C07C323/20 , C07F9/54 , C08G64/20 , C08G64/30 , C08G65/34 , C08G64/00
CPC分类号： C08G64/307 , B01J31/0239 , B01J31/0247 , B01J31/0251 , B01J31/0268 , C08G64/20 , B01J2231/14 , B01J2531/98
摘要： Quaternary salts having a double helix structure are prepared by the reaction of dihydroxyaromatic compound, preferably a bisphenol, with an alkali metal hydroxide and a quaternary salt, such as a tetraalkylammonium or hexaalkylguanidinium chloride. The quaternary salts and their alkaline hydrolysis products are useful as catalysts in various reactions, including imide formation from bisphenol salts and halo- or nitro-substituted phthalimides and redistribution and equilibration of polycarbonates.
摘要翻译：通过二羟基芳族化合物，优选双酚与碱金属氢氧化物和季盐如四烷基铵或六烷基氯化胍的反应制备具有双螺旋结构的季铵盐。季盐及其碱性水解产物可用作各种反应中的催化剂，包括由双酚盐和卤代或硝基取代的邻苯二甲酰亚胺形成的酰亚胺以及聚碳酸酯的再分配和平衡。

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