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1. 发明授权

US5777183A Process for the production of Guerbet alcohols 失效
标题翻译：格瑞特醇生产工艺
公开(公告)号：US5777183A
公开(公告)日：1998-07-07
申请号：US676029
申请日：1996-07-05
申请人： Gerd Mueller , Bernhardt Gutsche , Lutz Jeromin , Udo Steinberner , Reinhold Sedelies , Ralf Bohlander , Richard Ridinger , Dirk Springer , Franz Buettgen , Frank Bartschik
发明人： Gerd Mueller , Bernhardt Gutsche , Lutz Jeromin , Udo Steinberner , Reinhold Sedelies , Ralf Bohlander , Richard Ridinger , Dirk Springer , Franz Buettgen , Frank Bartschik
IPC分类号： B01J23/02 , C07C29/34 , C07C27/00
CPC分类号： B01J23/02 , C07C29/34 , C07C2101/14
摘要： The invention relates to a process for the production of Guerbet alcohols by condensation of aliphatic alcohols in the presence of alkali metal or alkaline earth metal hydroxides as catalyst using the Guerbet reaction, in which the initial pressure in the reactor corresponds to the vapor pressure of the alcohol components used and, during the reaction, the pressure is continually reduced to the vapor pressure of the reaction mixture at the particular temperature.
摘要翻译：本发明涉及一种通过使用Guerbet反应在碱金属或碱土金属氢氧化物作为催化剂存在下脂族醇缩合生产格尔伯特醇的方法，其中反应器中的初始压力对应于使用的醇组分，并且在反应期间，压力在特定温度下持续降低至反应混合物的蒸气压。

2. 发明授权

US06331607B1 Method for producing glucoprotamines 有权
标题翻译：葡聚糖的制备方法
公开(公告)号：US06331607B1
公开(公告)日：2001-12-18
申请号：US09508929
申请日：2000-06-08
申请人： Ralf Bohlander , Sven Jaensch , Dirk Springer
发明人： Ralf Bohlander , Sven Jaensch , Dirk Springer
IPC分类号： C08G6908
CPC分类号： C07C231/02 , B01D19/0413 , C07C237/10
摘要： A process for producing glucoprotamines by condensation of N-substituted propylene diamines with 2-aminoglutaric compounds in which the reaction is carried out in the presence of aminosilicones is disclosed. Glucoprotamines produced in accordance with the disclosed process exhibit improved color quality and longer storage stability.
摘要翻译：公开了一种通过N-取代的丙烯二胺与在氨基硅氧烷存在下进行反应的2-氨基戊二酸的化合物的缩合生产葡糖基多肽的方法。根据所公开的方法生产的葡萄糖肽具有改善的颜色质量和较长的储存稳定性。

3. 发明申请

US20100006006A1 Water-Soluble Silicates and Use Thereof 审中-公开
标题翻译：水溶性硅酸盐及其用途
公开(公告)号：US20100006006A1
公开(公告)日：2010-01-14
申请号：US12500949
申请日：2009-07-10
申请人： Ralf Bohlander , Thomas Albers , Wolfgang Pesch , Michael Langen
发明人： Ralf Bohlander , Thomas Albers , Wolfgang Pesch , Michael Langen
IPC分类号： C09D5/00 , C07F7/08
CPC分类号： C01B33/325 , C23C2222/20
摘要： Modified silicates are described which are obtained by reacting a waterglass solution with alkylsilanes of the general formula R—(CH2)n—Si—(X)3, in which X, in each case independently, is CH3, OCH3, OC2H5, OC3H7, OCOCH3 or Cl, and R is a saturated or unsaturated, linear or branched or cyclic radical having at least one O and/or N atom and at least 2 carbon atoms, and n is a number between 1 and 3, at a temperature in the range of from about 20 to about 80° C. The modified silicates are suitable for the hydrophilic finishing of hard surfaces, and can be used in detergents and cleaners.
摘要翻译：描述了通过使水玻璃溶液与通式R-（CH 2）n -Si-（X）3的烷基硅烷反应获得的改性硅酸盐，其中X，在各种情况下独立地为CH 3，OCH 3，OC 2 H 5，OC 3 H 7， OCOCH 3或Cl，并且R是具有至少一个O和/或N原子和至少2个碳原子的饱和或不饱和的直链或支链或环状基团，n是1和3之间的数，在范围为约20至约80℃。改性硅酸盐适用于硬表面的亲水整理，并可用于洗涤剂和清洁剂。

4. 发明授权

US09090781B2 Solvent-free water-soluble silane-modified silicates 有权
标题翻译：无溶剂的水溶性硅烷改性硅酸盐
公开(公告)号：US09090781B2
公开(公告)日：2015-07-28
申请号：US13147425
申请日：2010-01-29
申请人： Ralf Bohlander
发明人： Ralf Bohlander
IPC分类号： C09D1/04 , C01C1/00 , C04B41/68 , C01B33/20 , C01B33/32 , C04B12/04 , C04B28/26 , C09C1/28 , C09C1/30 , C09D5/00 , C09D5/18 , C04B111/10
CPC分类号： C09D1/04 , C01B33/20 , C01B33/32 , C01B33/325 , C01C1/00 , C04B12/04 , C04B28/26 , C04B41/68 , C04B2111/1012 , C09C1/28 , C09C1/3081 , C09D5/00 , C09D5/18 , C04B22/16 , C04B24/42 , C04B22/0013 , C04B41/5024 , C04B41/4922
摘要： The invention relates to an aqueous solution of modified silicates, wherein the solution is free of organic solvents and is obtained by reacting (a) an initially charge aqueous solution of silicates of the general formula M2O·nSiO2, wherein M is a cation from the group Li+, Na+, K+, NY4+, where Y is a hydrogen atom and/or an alkyl or alkenyl radical having 1 to 22 C atoms, and (b) at least one silane of the general formula R—(CH2)n—Si—(X)3 where X is independently a CH3, OCH3, OC2H5, OC3H7, OCOCH3, H or Cl radical, and R is a saturated or unsaturated, linear or branched or ring-shaped radical having at least one O and/or N atom and at least 2 C atoms, and n is a number between 1 and 3; at temperatures from 5 to 100° C., and wherein the alcohols arising from the conversion are subsequently removed. The aqueous solution of modified silicates is used to hydrophilize surfaces, particularly for high-temperature coatings.
摘要翻译：本发明涉及一种改性硅酸盐水溶液，其中该溶液不含有机溶剂，并且通过使（a）通式M a·nSiO 2的硅酸盐的初始加入水溶液与式 Li +，Na +，K +，NY4 +，其中Y是氢原子和/或具有1至22个C原子的烷基或烯基，和（b）至少一种通式R-（CH 2）n-Si- （X）3，其中X独立地是CH 3，OCH 3，OC 2 H 5，OC 3 H 7，OCOCH 3，H或Cl基，R是具有至少一个O和/或N原子的饱和或不饱和的直链或支链或环状基团和至少2个C原子，n是1和3之间的数字; 在5至100℃的温度下，随后除去转化产生的醇。改性硅酸盐水溶液用于亲水化表面，特别是用于高温涂料。

5. 发明申请

US20110283916A1 Solvent-Free Water-Soluble Silane-Modified Silicates 有权
标题翻译：无溶剂水溶性硅烷改性硅酸盐
公开(公告)号：US20110283916A1
公开(公告)日：2011-11-24
申请号：US13147425
申请日：2010-01-29
申请人： Ralf Bohlander
发明人： Ralf Bohlander
IPC分类号： C09D7/00
CPC分类号： C09D1/04 , C01B33/20 , C01B33/32 , C01B33/325 , C01C1/00 , C04B12/04 , C04B28/26 , C04B41/68 , C04B2111/1012 , C09C1/28 , C09C1/3081 , C09D5/00 , C09D5/18 , C04B22/16 , C04B24/42 , C04B22/0013 , C04B41/5024 , C04B41/4922
摘要： The invention relates to an aqueous solution of modified silicates, wherein the solution is free of organic solvents and is obtained by reacting (a) an initially charge aqueous solution of silicates of the general formula M2O.nSiO2, wherein M is a cation from the group Li+, Na+, K+, NY4+, where Y is a hydrogen atom and/or an alkyl or alkenyl radical having 1 to 22 C atoms, and (b) at least one silane of the general formula R—(CH2)n—Si—(X)3 where X is independently a CH3, OCH3, OC2H5, OC3H7, OCOCH3, H or Cl radical, and R is a saturated or unsaturated, linear or branched or ring-shaped radical having at least one O and/or N atom and at least 2 C atoms, and n is a number between 1 and 3; at temperatures from 5 to 100° C., and wherein the alcohols arising from the conversion are subsequently removed. The aqueous solution of modified silicates is used to hydrophilize surfaces, particularly for high-temperature coatings.
摘要翻译：本发明涉及一种改性硅酸盐的水溶液，其中该溶液不含有机溶剂，并且通过使（a）通式M 2 O·nSiO 2的硅酸盐的初始加入水溶液（其中M为基团的阳离子） Li +，Na +，K +，NY4 +，其中Y是氢原子和/或具有1至22个C原子的烷基或烯基，和（b）至少一种通式R-（CH 2）n-Si- （X）3，其中X独立地是CH 3，OCH 3，OC 2 H 5，OC 3 H 7，OCOCH 3，H或Cl基，R是具有至少一个O和/或N原子的饱和或不饱和的直链或支链或环状基团和至少2个C原子，n是1和3之间的数字; 在5至100℃的温度下，随后除去转化产生的醇。改性硅酸盐水溶液用于亲水化表面，特别是用于高温涂料。

6. 发明授权

US09193598B2 Storage-stable silicate solutions 有权
标题翻译：储存稳定的硅酸盐溶液
公开(公告)号：US09193598B2
公开(公告)日：2015-11-24
申请号：US13022092
申请日：2011-02-07
申请人： Ralf Bohlander , Silke Muckenfuβ , Rüdiger Ziervogel
发明人： Ralf Bohlander , Silke Muckenfuβ , Rüdiger Ziervogel
IPC分类号： C09D1/00 , C01B33/32
CPC分类号： C01B33/325
摘要： Disclosed are aqueous solutions of silicates (waterglasses), comprising (a) 20 to 40% by weight of SiO2, (b) 10 to 30% by weight of M2O, where M is a cation selected from the group consisting of Li+, Na+, K+, and NY4+, where Y is a C1-C6 alkyl or alkenyl radical, and (c) water; which solutions are obtained by a process comprising (i) providing an aqueous solution of a silicate (waterglass) of the formula M2O×nSiO2, as above, where n=1-5, and (ii) fine filtering the solution over a filter element that is stable at pH values of 12 or more, at a temperature in the range of 20 to 140° C., provided that the filtrate solution has a turbidity of 4 FNU or less. The aqueous solutions are clear at temperatures below −10° C., and are storage-stable against turbidity for at least 1 month.
摘要翻译：公开了硅酸盐（水晶）的水溶液，其包含（a）20至40重量％的SiO 2，（b）10至30重量％的M 2 O，其中M是选自Li +，Na +， K +和NY4 +，其中Y是C1-C6烷基或烯基，和（c）水; 该方法通过以下方法获得，该方法包括（i）如上所述提供式M 2 O×nSiO 2的硅酸盐（水玻璃）的水溶液，其中n = 1-5，和（ii）在过滤元件上精细过滤溶液其pH值为12以上，在20〜140℃的温度下稳定，条件是滤液的浊度为4Fun以下。水溶液在低于-10℃的温度下是透明的，并且对于浑浊物质储存稳定至少1个月。

7. 发明授权

US08858923B2 Hair relaxer 有权
标题翻译：头发放松
公开(公告)号：US08858923B2
公开(公告)日：2014-10-14
申请号：US13379788
申请日：2010-06-17
申请人： Hans-Martin Haake , Ralf Bohlander , Jessica Cecchini , Mehmet Yücel Altunok , Albrecht Weiss , Angela Brands
发明人： Hans-Martin Haake , Ralf Bohlander , Jessica Cecchini , Mehmet Yücel Altunok , Albrecht Weiss , Angela Brands
IPC分类号： A61K8/30 , A61K8/00 , A61K8/19 , A61K8/25 , A61Q5/04
CPC分类号： A61K8/25 , A61K8/062 , A61K8/19 , A61K8/345 , A61K8/43 , A61K8/604 , A61Q5/04
摘要： The invention relates to a hair smoothing agent characterized by a content of sodium silicate.
摘要翻译：本发明涉及以硅酸钠的含量为特征的毛发光滑剂。

8. 发明申请

US20120196736A1 Aluminum-Containing Waterglass Solutions 有权
标题翻译：含铝水玻璃解决方案
公开(公告)号：US20120196736A1
公开(公告)日：2012-08-02
申请号：US13499856
申请日：2010-09-28
申请人： Ralf Bohlander
发明人： Ralf Bohlander
IPC分类号： C03C3/062
CPC分类号： C01B33/32 , C01B33/26 , C04B12/04 , C04B2111/00215
摘要： The invention relates to a process for preparing clear aqueous solutions of silicates, remaining stable at 20° C. on storage for at least 6 months, containing 20% to 40% by weight SiO2, 10% to 20% by weight M2O, where M is a cation from the group consisting of Li+, Na+, K+ and NY4+ and Y is an alkyl or alkenyl radical having 1 to 6 C atoms, 0.5% to 6% by weight Al2O3 and 100% by weight water, by introducing an aqueous solution of a silicate of the general formula M2O x nSiO2, in which M is a cation from the group consisting of Li+, Na+, K+ and NY4+, and where Y is an alkyl or alkenyl radical having 1 to 6 C atoms, and n is a number in the range from 1 to 5, and metering in an aluminium compound in such a way that the viscosity of the reaction mixture remains below 10 000 mPas, and the reaction being carried out in a temperature range from 20 to 140° C., with the proviso that, following the metered addition of the total amount of the aluminium compound, the reaction mixture is cooled to room temperature as soon as the reaction mixture is clear.
摘要翻译：本发明涉及一种制备透明硅酸盐水溶液的方法，在20℃下保存稳定至少6个月，其含有20重量％至40重量％的SiO 2，10重量％至20重量％的M 2 O，其中M 是由Li +，Na +，K +和NY4 +组成的组中的阳离子，Y是具有1至6个C原子的烷基或烯基，0.5至6重量％的Al 2 O 3和100重量％的水，的通式为M 2 O x nSiO 2的硅酸盐，其中M是由Li +，Na +，K +和NY4 +组成的组中的阳离子，其中Y是具有1至6个C原子的烷基或烯基，n是数量范围为1至5，并以铝化合物计量，使得反应混合物的粘度保持在10 000 mPa·s以下，反应在20〜140℃的温度范围内进行，条件是，在计量加入铝化合物的总量之后，将反应混合物冷却一旦反应混合物清澈，至室温。

9. 发明授权

US08460453B2 Aluminum-containing waterglass solutions 有权
标题翻译：含铝水玻璃溶液
公开(公告)号：US08460453B2
公开(公告)日：2013-06-11
申请号：US13499856
申请日：2010-09-28
申请人： Ralf Bohlander
发明人： Ralf Bohlander
IPC分类号： C01B33/32 , C01B33/26 , C04B12/04
CPC分类号： C01B33/32 , C01B33/26 , C04B12/04 , C04B2111/00215
摘要： The invention relates to a process for preparing clear aqueous solutions of silicates, remaining stable at 20° C. on storage for at least 6 months, containing 20% to 40% by weight SiO2, 10% to 20% by weight M2O, where M is a cation from the group consisting of Li+, Na+, K+ and NY4+ and Y is an alkyl or alkenyl radical having 1 to 6 C atoms, 0.5% to 6% by weight Al2O3 and 100% by weight water, by introducing an aqueous solution of a silicate of the general formula M2O x nSiO2, in which M is a cation from the group consisting of Li+, Na+, K+ and NY4+, and where Y is an alkyl or alkenyl radical having 1 to 6 C atoms, and n is a number in the range from 1 to 5, and metering in an aluminium compound in such a way that the viscosity of the reaction mixture remains below 10 000 mPas, and the reaction being carried out in a temperature range from 20 to 140° C., with the proviso that, following the metered addition of the total amount of the aluminium compound, the reaction mixture is cooled to room temperature as soon as the reaction mixture is clear.
摘要翻译：本发明涉及一种制备透明硅酸盐水溶液的方法，在20℃下保存稳定至少6个月，其含有20重量％至40重量％的SiO 2，10重量％至20重量％的M 2 O，其中M 是由Li +，Na +，K +和NY4 +组成的组中的阳离子，Y是具有1至6个C原子的烷基或烯基，0.5至6重量％的Al 2 O 3和100重量％的水，的通式为M 2 O x nSiO 2的硅酸盐，其中M是由Li +，Na +，K +和NY4 +组成的组中的阳离子，其中Y是具有1至6个C原子的烷基或烯基，n是数量范围为1至5，并以铝化合物计量，使得反应混合物的粘度保持在10 000 mPa·s以下，反应在20〜140℃的温度范围内进行，条件是，在计量加入铝化合物的总量之后，将反应混合物冷却一旦反应混合物清澈，至室温。

10. 发明申请

US20120201776A1 Hair Relaxer 有权
标题翻译：头发放松
公开(公告)号：US20120201776A1
公开(公告)日：2012-08-09
申请号：US13379788
申请日：2010-06-17
申请人： Hans-Martin Haake , Ralf Bohlander , Jessica Cecchini , Mehmet Yücel Altunok , Albrecht Weiss , Angela Brands
发明人： Hans-Martin Haake , Ralf Bohlander , Jessica Cecchini , Mehmet Yücel Altunok , Albrecht Weiss , Angela Brands
IPC分类号： A61K8/25 , A61Q5/04 , A61K8/73
CPC分类号： A61K8/25 , A61K8/062 , A61K8/19 , A61K8/345 , A61K8/43 , A61K8/604 , A61Q5/04
摘要： The invention relates to a hair smoothing agent characterized by a content of sodium silicate.
摘要翻译：本发明涉及以硅酸钠的含量为特征的毛发光滑剂。

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