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1. 发明申请

US20050106114A1 Process for improving the sun protection factor of cellulosic fibre material 失效
标题翻译：改善纤维素纤维材料防晒系数的方法
公开(公告)号：US20050106114A1
公开(公告)日：2005-05-19
申请号：US10504945
申请日：2003-02-11
申请人： Georges Metzger , Jean-Jacques Donze , Hans Kramer , Serge Hauger , Volker Papendick , Michael Milde , Ted Deisenroth , Rainer Traber , Ullrich Menge , Hauke Rohwer
发明人： Georges Metzger , Jean-Jacques Donze , Hans Kramer , Serge Hauger , Volker Papendick , Michael Milde , Ted Deisenroth , Rainer Traber , Ullrich Menge , Hauke Rohwer
IPC分类号： C09B57/00 , C07D251/68 , C11D3/28 , D06L3/12 , D06M13/355 , D06M13/358 , D06M101/04 , D06P1/00 , D06M13/322 , A61K7/42
CPC分类号： D06M13/358 , C07D251/68 , D06M2200/25
摘要： A process for improving the sun protection factor (SPF) of cellulosic fibre materials and blends thereof, which comprises contacting said materials with at least one compound of the formula (1) according to claim 1.
摘要翻译：一种用于改善纤维素纤维材料及其共混物的防晒因子（SPF）的方法，其包括使所述材料与至少一种根据权利要求1的式（1）化合物接触。

2. 发明授权

US07425222B2 Process for improving the sun protection factor of cellulosic fibre material 失效
标题翻译：改善纤维素纤维材料防晒系数的方法
公开(公告)号：US07425222B2
公开(公告)日：2008-09-16
申请号：US10504945
申请日：2002-02-11
申请人： Georges Metzger , Jean-Jacques Donzé , Hans Kramer , Serge Hauger , Volker Papendick , Michael Milde , Ted Deisenroth , Rainer Hans Traber , Ullrich Menge , Hauke Rohwer
发明人： Georges Metzger , Jean-Jacques Donzé , Hans Kramer , Serge Hauger , Volker Papendick , Michael Milde , Ted Deisenroth , Rainer Hans Traber , Ullrich Menge , Hauke Rohwer
IPC分类号： D06L3/12
CPC分类号： D06M13/358 , C07D251/68 , D06M2200/25
摘要： A process for improving the sun protection factor (SPF) of cellulosic fibre materials and blends thereof, which comprises contacting said materials with at least one compound of the formula (1) in which M is hydrogen, an alkali metal atom, ammonium or a cation formed from an amine; R1 and R1′ independently of each other are hydrogen, hydroxy, optionally substituted alkyl, 4-morpholinyl, —NH—R3, —N(R3)2 or —O—R3, wherein R3is optionally substituted alkyl or optionally substituted aryl, R2 is a group of formula (2) wherein X is —O— or —NH— and R4 is C1-C4-alkyl which carries at least one hydrophilic substituent and R2′ has the meaning of R1 or R2.
摘要翻译：一种用于改善纤维素纤维材料及其共混物的防晒因子（SPF）的方法，其包括使所述材料与至少一种其中M为氢的式（1）化合物，碱金属原子，铵或阳离子由胺形成; R 1和R 2彼此独立地是氢，羟基，任选取代的烷基，4-吗啉基，-NH-R 3， -N（R 3 3）2或-OR 3，其中R 3是任选取代的烷基或任选取代的芳基，R 2是式（2）的基团，其中X是-O-或-NH-，R 4是C 1 - 携带至少一个亲水取代基的C 4 - 烷基和R 2'具有R 1或R 2的含义， SUB>。

3. 发明授权

US06723846B1 Triazinylaminostilbene derivative as fluorescent whitening agents 失效
标题翻译：三嗪基氨基芪衍生物作为荧光增白剂
公开(公告)号：US06723846B1
公开(公告)日：2004-04-20
申请号：US10070525
申请日：2002-03-06
申请人： Georges Metzger , Serge Hauger , Fabienne Cuesta , Christophe Bulliard , Peter Rohringer , Marc Roger Grienenberger
发明人： Georges Metzger , Serge Hauger , Fabienne Cuesta , Christophe Bulliard , Peter Rohringer , Marc Roger Grienenberger
IPC分类号： C07D25168
CPC分类号： C07D251/68 , Y10S8/919
摘要： The present invention relates to compounds having formula (1): wherein each R1 represents, independently, a linear C1-C4-alkylene residue which is unsubstituted or substituted by hydroxy, C1-C4-alkyl, C1-C4-alkoxy, C1-C4-hydroxy- or alkoxy-alkoxy, —OCOM, —OCOC1-C4-alkyl, or an amino acid residue from which a hydrogen atom on the amino group has been removed; each R2 represents, independently, a linear C1-C4-alkylene residue which is unsubstituted or substituted by hydroxy, C1-C4-alkyl, C1-C4-alkoxy, C1-C4-hydroxy- or alkoxy-alkoxy, —OCOM, —OCOC1-C4-alkyl, —CO2M, CO2C1-C4-alkyl SO3M or phenoxy which is unsubstituted or substituted by halogen, C1-C4-alkyl or C1-C4-alkoxy, —CO2M or CO2C1-C4-alkyl, NH3 or mono- or disubstituted amino; or phenyl which is unsubstituted or substituted by 1 to 3 SO3M, SO2NHC1-C4-alkyl, —SO2NH2, —CO2M, —CO2M, —CO2C1-C4-alkyl, —CONH2, —CONHC1-C4-alkyl, —NHCOC1-C4-alkyl or mono- or disubstituted amino groups; each R3 represents independently, hydrogen, C1-C4-alkyl, halogen, cyano, SO3M, —SO2NH2, SO2NHC1-C4-alkyl, —CO2M, —CO2C1-C4-alkyl, —CONH2, —CONHC1-C4-alkyl, or —NHCOC1-C4-alkyl; M is hydrogen, an alkali metal atom, ammonium or a cation formed from an amine and m is an integer of 1 to 3, a process for their preparation and use of the compounds as optical brightening agents for synthetic or natural organic materials or for removing stain in photographic materials.
摘要翻译：本发明涉及具有式（1）的化合物：其中每个R 1独立地表示未被取代或被羟基，C 1 -C 4烷基，C 1 -C 4烷氧基，C 1 -C 4烷基取代的直链C 1 -C 4亚烷基 - 羟基 - 或烷氧基 - 烷氧基，-OCOM，-OCOC1-C4-烷基或氨基上氨基的氢原子被除去的氨基酸残基; 每个R 2独立地表示未被取代或被羟基，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，C 1 -C 4 - 羟基 - 或烷氧基 - 烷氧基取代的直链C 1 -C 4 - 亚烷基残基，-OCOM，-OCOC 1 -C 1-4烷基，-CO 2 M，CO 2 C 1 -C 4 - 烷基SO 3 M或苯氧基，其未被取代或被卤素，C 1 -C 4 - 烷基或C 1 -C 4 - 烷氧基，-CO 2 M或CO 2 C 1 -C 4烷基，NH 3或单 - 或二取代氨基; 或未被取代或被1至3个SO 3 M，SO 2 NHC 1 -C 4烷基，-SO 2 NH 2，-CO 2 M，-CO 2 M，-CO 2 C 1 -C 4 - 烷基，-CONH 2，-CONHC 1 -C 4烷基，-NHCOC 1 -C 4 - 烷基或单或二取代的氨基; 每个R 3独立地表示氢，C 1 -C 4 - 烷基，卤素，氰基，SO 3 M，-SO 2 NH 2，SO 2 NHC 1 -C 4烷基，-CO 2 M，

4. 发明授权

US6040443A Process for the production of benzoxazinones 失效
标题翻译：生产苯并恶嗪酮的方法
公开(公告)号：US6040443A
公开(公告)日：2000-03-21
申请号：US119300
申请日：1998-07-20
申请人： Georges Metzger , Dieter Reinehr , Serge Hauger
发明人： Georges Metzger , Dieter Reinehr , Serge Hauger
IPC分类号： C07D265/22 , C07D265/02
CPC分类号： C07D265/22
摘要： There is described a process for the production of a 1,3-benzoxazin-4-one having the formula: ##STR1## in which R.sub.1 and R.sub.2, independently, are hydrogen, cyano, halogen, nitro, C.sub.1 -C.sub.20 alkyl, O--C.sub.1 -C.sub.20 alkyl, phenyl, NH--CO--C.sub.1 -C.sub.20 alkyl, N(R.sub.3).sub.2, SO.sub.2 N(R.sub.3).sub.2, COOR.sub.3 or CON(R.sub.3).sub.2 in which R.sub.3 is hydrogen, cyano, halogen, nitro, C.sub.1 -C.sub.20 alkyl, O--C.sub.1 -C.sub.20 alkyl, phenyl or NH--CO--C.sub.1 -C.sub.20 alkyl, comprising reacting, at elevated temperature, 1 molar equivalent of an o-hydroxybenzamide of formula: ##STR2## in which R.sub.1 has its previous significance, with 2 to 6 molar equivalents of a benzoyl chloride of formula: ##STR3## in which R.sub.2 has its previous significance. The 1,3-benzoxazin-4-ones having the formula (1) so obtained are important intermediates for the production of triazine compounds having excellent absorption spectrum characteristics and good resistance to exposure to UV light.
摘要翻译：描述了制备具有下式的1,3-苯并恶嗪-4-酮的方法：其中R 1和R 2独立地是氢，氰基，卤素，硝基，C 1 -C 20烷基，O-C 1 -C 20烷基，苯基，NH-CO-C 1 -C 20烷基，N（R 3）2，SO 2 N（R 3）2，COOR 3或CON（R 3）2，其中R 3是氢，氰基，卤素，硝基，C 1 -C 20烷基，O-C 1 -C 20烷基苯基或NH-CO-C 1 -C 20烷基，其包括在升高的温度下，将1摩尔当量的具有其先前意义的式的邻羟基苯甲酰胺与2至6摩尔当量的下式的苯甲酰氯反应：其中R2具有以前的意义。具有式（1）的1,3-苯并恶嗪-4-酮是制备具有优异的吸收光谱特性和良好的耐紫外线性的三嗪化合物的重要中间体。

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