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1. 发明授权

US07008914B2 Alkylbenzene detergents with high 2-isomer content 有权
公开(公告)号：US07008914B2
公开(公告)日：2006-03-07
申请号：US10263547
申请日：2002-10-03
申请人： George A. Smith , Prakasa R. Anantaneni , Samir S. Ashrawi , Raeda M. Smadi , John F. Knifton , Melvin Stockton
发明人： George A. Smith , Prakasa R. Anantaneni , Samir S. Ashrawi , Raeda M. Smadi , John F. Knifton , Melvin Stockton
IPC分类号： C11D17/00
CPC分类号： C11D17/0073 , C11D1/22
摘要： This invention is directed to a fluorine-containing mordenite catalyst and use thereof in the manufacture of alkylbenzene (LAB) by alkylation of benzene with an olefin. The olefin may have from about 10 to 14 carbons. The fluorine-containing mordenite is prepared typically by treatment with an aqueous hydrogen fluoride solution. The benzene alkylation may be conducted using reactive distillation. This invention is also directed to a process for production of LAB having a high 2-phenyl isomer content by use of the fluorine-containing mordenite in conjunction with a conventional solid LAB alkylation catalyst. The two catalysts may be used in a mixed catalyst bed or may be packed in series, with the relative proportions being adjusted to provide a desired 2-phenyl isomer content of in the final product.

2. 发明授权

US06562776B1 Solid alkylbenzene sulfonates and cleaning compositions having enhanced water hardness tolerance 有权
公开(公告)号：US06562776B1
公开(公告)日：2003-05-13
申请号：US09559841
申请日：2000-04-26
申请人： George A. Smith , Samir S. Ashrawi , Raeda M. Smadi , Prakasa R. Anantaneni
发明人： George A. Smith , Samir S. Ashrawi , Raeda M. Smadi , Prakasa R. Anantaneni
IPC分类号： C11D1700
CPC分类号： B01D3/322 , B01J29/18 , B01J37/26 , B01J2229/16 , C01B39/026 , C07C2/66 , C07C15/107 , C07C2521/12 , C07C2521/16 , C07C2527/126 , C07C2529/16 , C07C2529/18 , C07C2529/70 , C11D1/22 , C11D17/0073
摘要： This invention is directed to detergent compositions which employ sulfonated linear alkylbenzenes as surfactants, wherein the sulfonated linear alkylbenzenes have a higher content of the sulfonated 2-phenyl alkylbenzene isomers than was previously available in sulfonated phenyl alkylbenzene surfactants of the prior art. Cleaning compositions according to the invention are more effective as cleaning agents over their counterparts of prior art which contain sulfonated linear alkylbenzenes having lower contents of the 2-phenyl alkylbenzene isomers, owing to an unexpected increase in tolerance of water hardness minerals normally associated with precipitation of the active detergent agent. Solid sulfonate salts of alkylbenzenes are also provided, including dry formulations containing same.

3. 发明授权

US06995127B1 Alkyl toluene sulfonate detergent 失效
标题翻译：烷基甲苯磺酸盐洗涤剂
公开(公告)号：US06995127B1
公开(公告)日：2006-02-07
申请号：US09665642
申请日：2000-09-19
申请人： George A. Smith , Prakasa R. Anantaneni , Samir S. Ashrawi , Raeda M. Smadi
发明人： George A. Smith , Prakasa R. Anantaneni , Samir S. Ashrawi , Raeda M. Smadi
IPC分类号： C11D17/00
CPC分类号： C11D3/3418 , C11D1/22
摘要： This invention is directed to detergent compositions which employ sulfonated alkyltoluenes as surfactants, wherein the sulfonated alkyltoluenes have a higher content of the sulfonated 2-phenyl alkyltoluenes isomers than was previously available in sulfonated alkyltoluene surfactants of the prior art. Cleaning compositions according to the invention are more effective as cleaning agents over their counterparts of prior art which contain sulfonated alkyltoluenes having lower contents of the 2-phenyl alkyltoluene isomers, owing to an unexpected increase in tolerance of water hardness minerals normally associated with precipitation of the active detergent agent. Solid sulfonate salts of alkyltoluenes are also provided, including dry cleaning formulations containing same. The alkyltoluenes of this invention may be combined with alkylbenzene surfactants in order to provide detergent blends having increased water hardness tolerance, lower Krafft temperature, and increased cleaning performance over what was previously afforded by the prior art.
摘要翻译：本发明涉及使用磺化烷基甲苯作为表面活性剂的洗涤剂组合物，其中磺化烷基甲苯具有比以前在现有技术的磺化烷基甲苯表面活性剂中可获得的磺化2-苯基烷基甲苯异构体更高的含量。根据本发明的清洁组合物比现有技术的清洁剂更有效，其中含有较低含量的2-苯基烷基甲苯异构体的磺化烷基甲苯，因为通常与活性洗涤剂。还提供了烷基甲苯的固体磺酸盐，包括含有它们的干洗制剂。本发明的烷基甲苯可与烷基苯表面活性剂组合，以提供具有增加的水硬度耐受性，较低克拉夫特温度和相对于现有技术以前提供的清洁性能提高的清洁性能的洗涤剂混合物。

4. 发明授权

US06887839B2 Solid alkylbenzene sulfonates and cleaning compositions having enhanced water hardness tolerance 失效
标题翻译：固体烷基苯磺酸盐和具有增强的水硬度耐受性的清洁组合物
公开(公告)号：US06887839B2
公开(公告)日：2005-05-03
申请号：US10370144
申请日：2003-02-19
申请人： George A. Smith , Samir S. Ashrawi , Raeda M. Smadi , Prakasa R. Anantaneni
发明人： George A. Smith , Samir S. Ashrawi , Raeda M. Smadi , Prakasa R. Anantaneni
IPC分类号： B01D3/32 , B01J29/18 , B01J37/26 , C01B39/02 , C07C2/66 , C07C15/107 , C11D1/22 , C11D17/00
CPC分类号： C11D17/0073 , B01D3/322 , B01J29/18 , B01J37/26 , B01J2229/16 , C01B39/026 , C07C2/66 , C07C15/107 , C07C2521/12 , C07C2521/16 , C07C2527/126 , C07C2529/16 , C07C2529/18 , C07C2529/70 , C11D1/22
摘要： This invention is directed to detergent compositions which employ sulfonated linear alkylbenzenes as surfactants, wherein the sulfonated linear alkylbenzenes have a higher content of the sulfonated 2-phenyl alkylbenzene isomers than was previously available in sulfonated phenyl alkylbenzene surfactants of the prior art. Cleaning compositions according to the invention are more effective as cleaning agents over their counterparts of prior art which contain sulfonated linear alkylbenzenes having lower contents of the 2-phenyl alkylbenzene isomers, owing to an unexpected increase in tolerance of water hardness minerals normally associated with precipitation of the active detergent agent. Solid sulfonate salts of alkylbenzenes are also provided, including dry formulations containing same.
摘要翻译：本发明涉及使用磺化直链烷基苯作为表面活性剂的洗涤剂组合物，其中磺化的直链烷基苯具有比以前在现有技术的磺化苯基烷基苯表面活性剂中可获得的更高的磺化2-苯基烷基苯异构体含量。根据本发明的清洁组合物比现有技术的清洁剂更有效，因为含有较低含量的2-苯基烷基苯异构体的磺化线性烷基苯，由于通常与沉淀相关的水硬度矿物的耐受性出现意想不到的增加，活性洗涤剂。还提供了烷基苯的固体磺酸盐，包括含有它们的干制剂。

5. 发明授权

US06849588B2 Structured liquids made using LAB sulfonates of varied 2-isomer content 失效
标题翻译：使用不同2-异构体含量的LAB磺酸盐制成的结构液体
公开(公告)号：US06849588B2
公开(公告)日：2005-02-01
申请号：US10435525
申请日：2003-05-09
申请人： Curtis M. Elsik , George A. Smith , Samir S. Ashrawi , Prakasa R. Anantaneni , Christopher J. Whewell
发明人： Curtis M. Elsik , George A. Smith , Samir S. Ashrawi , Prakasa R. Anantaneni , Christopher J. Whewell
IPC分类号： B01D3/32 , B01J29/18 , B01J37/26 , C01B39/02 , C07C2/66 , C07C15/107 , C11D1/22 , C11D17/00
CPC分类号： B01D3/322 , B01J29/18 , B01J37/26 , B01J2229/16 , C01B39/026 , C07C2/66 , C07C15/107 , C07C2521/12 , C07C2521/16 , C07C2527/126 , C07C2529/16 , C07C2529/18 , C07C2529/70 , C11D1/22 , C11D17/0026 , C11D17/0073
摘要： Provided herein are structured liquid surfactants produced using a linear alkylbenzene sulfonate having various levels of 2-isomer content.
摘要翻译：本文提供了使用具有不同水平的2-异构体含量的直链烷基苯磺酸盐制备的结构化液体表面活性剂。

6. 发明申请

US20120094890A1 Process Compositions and Production of Acyl Alkylisethionate Compositions 有权
标题翻译：酰基烷基羟乙基磺酸盐组合物的工艺组合和生产
公开(公告)号：US20120094890A1
公开(公告)日：2012-04-19
申请号：US13330782
申请日：2011-12-20
申请人： Prakasa R. Anantaneni , George A. Smith , Martin J. Renner
发明人： Prakasa R. Anantaneni , George A. Smith , Martin J. Renner
IPC分类号： C11D1/28 , C11D3/34 , C11D3/37 , C11D3/10 , C11D3/382 , C11D3/386 , C11D3/20 , C11D3/30
CPC分类号： C07C303/32 , A61K8/466 , A61Q5/02 , A61Q19/10 , C07C303/02 , C07C303/22 , C07C309/12 , C11D1/28 , C07C309/08
摘要： Methods and compositions are provided for forming ester based compositions. The ester based compositions may be used in consumer products. In one aspect, a method is provided for producing acyl alkylisethionate esters by the esterification of a sulfonate composition having two or more sulfonate isomers with fatty acid(s). In another aspect, a method is provided for forming an ester based composition including a blend of acyl alkylisethionate and acylisethionate esters.
摘要翻译：提供了用于形成酯基组合物的方法和组合物。酯基组合物可以用于消费品中。在一个方面，提供了通过具有两个或多个磺酸酯异构体的磺酸盐组合物与脂肪酸的酯化来制备酰基烷基羟乙基磺酸盐酯的方法。在另一方面，提供了一种用于形成酯基组合物的方法，其包括酰基烷基羟乙基磺酸盐和酰基羟乙基磺酸酯的共混物。

7. 发明授权

US06630430B1 Fuel and oil detergents 有权
标题翻译：燃油和油清洁剂
公开(公告)号：US06630430B1
公开(公告)日：2003-10-07
申请号：US09616568
申请日：2000-07-14
申请人： Prakasa R. Anantaneni , George A. Smith
发明人： Prakasa R. Anantaneni , George A. Smith
IPC分类号： C10M000
CPC分类号： C11D1/22 , B01D3/322 , B01J27/12 , B01J29/18 , B01J37/26 , B01J2229/16 , C01B39/026 , C07C2/66 , C07C15/107 , C07C2521/12 , C07C2521/16 , C07C2527/126 , C07C2529/16 , C07C2529/18 , C07C2529/70
摘要： This invention is directed to lubricating compositions which contain detergent components derived from linear alkylbenzenes including sulfonates and salts and esters thereof. Detergents provided by the invention have a higher content of the 2-phenyl alkylbenzene isomers than was previously available in materials of prior art. The detergents of the present invention are more powerful detergents over those previously available and may be employed as additives in various lubricating compositions, including motor oils, cutting fluids, emulsions, and motor fuels.
摘要翻译：本发明涉及含有源自线性烷基苯的洗涤剂组分的润滑组合物，包括磺酸盐及其盐和酯。本发明提供的洗涤剂具有比以前在现有技术材料中可获得的2-苯基烷基苯异构体更高的含量。本发明的洗涤剂比之前可获得的洗涤剂更强大，可用作各种润滑组合物中的添加剂，包括机油，切削液，乳液和机动燃料。

8. 发明申请

US20100215610A1 PROCESS COMPOSITIONS AND PRODUCTION OF ACYL ALKYLISETHIONATE COMPOSITIONS 有权
标题翻译： ACYL ALKYLISETHIONATE组合物的工艺组合物和生产
公开(公告)号：US20100215610A1
公开(公告)日：2010-08-26
申请号：US12298635
申请日：2007-05-01
申请人： Prakasa R. Anantaneni , George A. Smith , Martin J. Renner
发明人： Prakasa R. Anantaneni , George A. Smith , Martin J. Renner
IPC分类号： A61K8/46 , C07C303/30 , C07C309/68 , A61Q5/02 , A61Q19/10 , A61Q1/14 , C09K3/00
CPC分类号： C07C303/32 , A61K8/466 , A61Q5/02 , A61Q19/10 , C07C303/02 , C07C303/22 , C07C309/12 , C11D1/28 , C07C309/08
摘要： Methods and compositions are provided for forming ester based compositions. The ester based compositions may be used in consumer products. In one aspect, a method is provided for producing acyl alkylisethionate esters by the esterification of a sulfonate composition having two or more sulfonate isomers with fatty acid(s). In another aspect, a method is provided for forming an ester based composition including a blend of acyl alkylisethionate and acylisethionate esters.
摘要翻译：提供了用于形成酯基组合物的方法和组合物。酯基组合物可以用于消费品中。在一个方面，提供了通过具有两个或多个磺酸酯异构体的磺酸盐组合物与脂肪酸的酯化来制备酰基烷基羟乙基磺酸盐酯的方法。在另一方面，提供了一种用于形成酯基组合物的方法，其包括酰基烷基羟乙基磺酸盐和酰基羟乙基磺酸酯的共混物。

9. 发明授权

US08105993B2 Process compositions and production of acyl alkylisethionate compositions 有权
标题翻译：酰基烷基羟乙基磺酸盐组合物的方法组合物和生产
公开(公告)号：US08105993B2
公开(公告)日：2012-01-31
申请号：US12298635
申请日：2007-05-01
申请人： Prakasa R. Anantaneni , George A. Smith , Martin J. Renner
发明人： Prakasa R. Anantaneni , George A. Smith , Martin J. Renner
IPC分类号： A61K31/00
CPC分类号： C07C303/32 , A61K8/466 , A61Q5/02 , A61Q19/10 , C07C303/02 , C07C303/22 , C07C309/12 , C11D1/28 , C07C309/08
摘要： Methods and compositions are provided for forming ester based compositions. The ester based compositions may be used in consumer products. In one aspect, a method is provided for producing acyl alkylisethionate esters by the esterification of a sulfonate composition having two or more sulfonate isomers with fatty acid(s). In another aspect, a method is provided for forming an ester based composition including a blend of acyl alkylisethionate and acylisethionate esters.
摘要翻译：提供了用于形成酯基组合物的方法和组合物。酯基组合物可以用于消费品中。在一个方面，提供了通过具有两个或多个磺酸酯异构体的磺酸盐组合物与脂肪酸的酯化来制备酰基烷基羟乙基磺酸盐酯的方法。在另一方面，提供了一种用于形成酯基组合物的方法，其包括酰基烷基羟乙基磺酸盐和酰基羟乙基磺酸酯的共混物。

10. 发明授权

US09598358B2 Acylalkylisethionate esters and applications in consumer products 有权
公开(公告)号：US09598358B2
公开(公告)日：2017-03-21
申请号：US13171039
申请日：2011-06-28
申请人： Prakasa R. Anantaneni , John Gray , Marty J. Renner , George A. Smith , David C. Lewis , Donald H. Champion , Christopher J. Whewell
发明人： Prakasa R. Anantaneni , John Gray , Marty J. Renner , George A. Smith , David C. Lewis , Donald H. Champion , Christopher J. Whewell
IPC分类号： C07C303/32 , A61K8/46 , A61Q5/02 , A61Q19/10 , C07C303/02 , C07C303/22 , C07C309/12 , C11D1/28
CPC分类号： C07C303/32 , A61K8/466 , A61Q5/02 , A61Q19/10 , C07C303/02 , C07C303/22 , C07C309/12 , C11D1/28 , C07C309/08
摘要： Acylalkylisethionate esters are produced by reacting one or more carboxylic acids with one or more alkyl-substituted hydroxyalkyl sulfonates under esterification reaction conditions. The alkyl-substituted hydroxyalkyl sulfonates used as a raw material in producing the esters are prepared by reacting bisulfate with one or more alkylene oxides. The acylalkylisethionate esters may be used in consumer products.

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