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1. 发明授权

US4562264A Process for the recovery of five-membered ring dicarboxylic acid anhydrides 失效
标题翻译：回收五元环二羧酸酐的方法
公开(公告)号：US4562264A
公开(公告)日：1985-12-31
申请号：US646073
申请日：1984-08-31
申请人： Fritz Gude , Ferdinand von Praun
发明人： Fritz Gude , Ferdinand von Praun
IPC分类号： C07C51/573 , C07D307/60 , C07D307/89
CPC分类号： C07C51/573
摘要： A process for the recovery of five-membered ring dicarboxylic acid anhydrides from aqueous solutions of the corresponding dicarboxylic acids which entails (a) washing the aqueous solution of the dicarboxylic acid with a water-insoluble tertiary amine, and separating the resulting amine-acid salt from the water layer; and (b) adding an aromatic hydrocarbon entrainer for the water, removing the entrainer/water azeotrope by distillation and separating the five-membered ring dicarboxylic acid anhydride after phase separation; or adding an aliphatic hydrocarbon entrainer for the water, removing a ternary azeotropic mixture consisting of a hydrolytically stable anhydride, water and entrainer by distillation and separating the five-membered ring dicarboxylic acid anhydride after phase separation.
摘要翻译：从相应的二羧酸的水溶液中回收五元环二羧酸酐的方法，其中（a）用水不溶性叔胺洗涤二羧酸的水溶液，并分离所得的胺酸盐从水层; 和（b）向水中加入芳族烃夹带剂，通过蒸馏除去夹带剂/水共沸物，并在相分离后分离五元环二羧酸酐; 或者向水中加入脂族烃夹带剂，通过蒸馏除去由水解稳定的酸酐，水和夹带剂组成的三元共沸混合物，并在相分离后分离五元环二羧酸酐。

2. 发明授权

US4571426A Process for the production of maleic anhydride 失效
标题翻译：马来酸酐生产工艺
公开(公告)号：US4571426A
公开(公告)日：1986-02-18
申请号：US646155
申请日：1984-08-31
申请人： Fritz Gude , Ferdinand von Praun
发明人： Fritz Gude , Ferdinand von Praun
IPC分类号： C07C51/573 , C07D307/60
CPC分类号： C07C51/573
摘要： A process for the production of maleic anhydride by catalytic air oxidation of hydrocarbons capable of being so oxidized at a temperature in the range of 300.degree.-450.degree. C., which, after air oxidation, entails:(a) introducing the air stream containing maleic anhydride and water vapor(i) at a temperature below the dew point of the accompanying water, into a water-insoluble tertiary amine extracting agent, which is stable to air, and a hydrocarbon diluent entrainer for the water; and separating the formed organic layer; or(ii) at a temperature above the dew point of the accompanying water, into a mixture of a water-insoluble tertiary amine extracting agent, which is stable to air, and a high-boiling alcohol; and separating the formed organic layer; or(iii) into water; and extracting the maleic acid with a water-insoluble tertiary amine extracting agent, which is stable or unstable to air, and a hydrocarbon diluent entrainer for the water; and separating the formed organic layer; and(b) heating the extract obtained according to step (a) to a temperature in the range of 120.degree.-180.degree. C. in vacuo, thereby recovering the maleic anhydride; and wherein said water-insoluble tertiary amines have a pKa value
摘要翻译：通过催化空气氧化生产马来酸酐的方法，其能在300-450℃的温度范围内被氧化，在空气氧化之后需要：（a）引入含有马来酸酐和水蒸汽（i）在低于伴随水的露点的温度下转化成对空气稳定的水不溶性叔胺萃取剂和用于水的烃稀释剂夹带剂; 并分离形成的有机层; 或（ii）在高于所含水露点的温度下，与空气稳定的水不溶性叔胺提取剂和高沸点醇的混合物中; 并分离形成的有机层; 或（iii）加入水中; 并用对水的稳定或不稳定的水不溶性叔胺萃取剂和用于水的烃稀释剂夹带剂萃取马来酸; 并分离所形成的有机层; 和（b）将根据步骤（a）获得的提取物真空加热至120-180℃的温度，从而回收马来酸酐; 并且其中所述水不溶性叔胺的pKa值<9，并且其中对于步骤（a）（i）和（a）（ii），所述叔胺在2-位具有支化的伯脂肪族侧链。

3. 发明授权

US4496710A Process for the production of flat varnishes 失效
标题翻译：平面清漆生产工艺
公开(公告)号：US4496710A
公开(公告)日：1985-01-29
申请号：US583229
申请日：1984-02-24
申请人： Fritz Gude , Herbert Haferkorn , Heinz Riemer , Gunter Dormann
发明人： Fritz Gude , Herbert Haferkorn , Heinz Riemer , Gunter Dormann
IPC分类号： C09D5/00 , C07D233/06 , C08G59/50 , C09D5/03 , C09D5/46 , C08G59/42
CPC分类号： C07D233/06 , C08G59/5093
摘要： The object of the invention is a process for the production of flat varnishes based on powder coatings of 1,2-epoxy compounds with at least one 1,2-epoxy group in the molecule and a lower melting point of >40.degree. C., salts of aromatic carboxylic acids with 3 and more carboxyl groups and imidazolines as curing agents, as well as the usual additives and the application of the powdered varnish upon the objects to be varnished and heating of these objects to temperatures of 160.degree.-240.degree. C., whereby the salt of 2-phenyl-methyl-.DELTA.2-imidazoline and trimellitic acid is substituted up to 60 mole % by a salt of 2-phenyl-.DELTA.2-imidazoline and trimellitic acid.
摘要翻译：本发明的目的是生产基于分子中具有至少一个1,2-环氧基的1,2-环氧化合物的粉末涂料和较低熔点> 40℃的平面清漆的方法，具有3个以上羧基的芳香族羧酸和咪唑啉作为固化剂的盐，以及通常的添加剂以及将该清漆对象上的粉末状清漆和将这些物体加热至160〜-240℃的温度由2-苯基 - 甲基-TATA-2-咪唑啉和偏苯三酸的盐被2-苯基-Δta-2-咪唑啉和偏苯三酸的盐取代直至60摩尔％。

4. 发明授权

US4855488A Process for the preparation of dicyclopentenol esters 失效
标题翻译：制备二环戊烯醇酯的方法
公开(公告)号：US4855488A
公开(公告)日：1989-08-08
申请号：US198749
申请日：1988-05-25
申请人： Fritz Gude , Hans Bellut
发明人： Fritz Gude , Hans Bellut
IPC分类号： C07C69/013 , B01J31/16 , B01J31/22 , B01J31/40 , C07B61/00 , C07C67/04 , C07C69/14 , C07C69/78
CPC分类号： C07C67/04 , B01J31/2226 , B01J31/26 , B01J31/4015 , B01J2531/30 , C07C2103/68 , Y02P20/584
摘要： A process for the preparation of a dicyclopentenol ester of the formula: ##STR1## wherein R is a C.sub.1-12 alkyl group, a C.sub.6-12 aryl group or a C.sub.6-12 substituted aryl group is disclosed. In this process dicyclopentadiene is reacted with an organic carboxylic acid of the formula:R--CO--OHin the presence of a catalyst. The catalyst comprises a readily volatile addition compound of BF.sub.3.
摘要翻译：公开了制备下式的二环戊烯醇酯的方法：其中R是C1-12烷基，C6-12芳基或C6-12取代的芳基。在该方法中，在催化剂存在下，使二环戊二烯与下式R-CO-OH的有机羧酸反应。该催化剂包含易挥发的BF 3的加成化合物。

5. 发明授权

US4250291A Melt adhesive based on polyamide from branched chain diamine 失效
标题翻译：基于支链二胺聚酰胺的熔融粘合剂
公开(公告)号：US4250291A
公开(公告)日：1981-02-10
申请号：US913994
申请日：1978-06-09
申请人： Fritz Gude , Siegfried Brandt
发明人： Fritz Gude , Siegfried Brandt
IPC分类号： C08G69/00 , C08G69/26 , C08G69/36 , C09J177/00 , D06M17/00
CPC分类号： C09J177/00 , C08G69/265 , C08G69/36
摘要： A polyamide copolymer, useful as a melt adhesive especially for textiles, produced from the following monomers1. An unbranched aliphatic dicarboxylic acid with 6-20 C-atoms;2. A diamine mixture consisting of(a) 20-80 mol percent, unbranched aliphatic diamines with 6-20 C-atoms; and(b) 80-20 mol percent branched aliphatic and/or cycloaliphatic diamines;said copolymer having a molecular weight of 2000-40000.
摘要翻译：可用作特殊用于纺织品的熔融粘合剂的聚酰胺共聚物，由以下单体制备1.具有6-20个C原子的无支链脂族二羧酸; 2.由（a）20-80摩尔％的具有6-20个碳原子的无支链脂肪族二胺组成的二胺混合物; 和（b）80-20摩尔％的支链脂族和/或脂环族二胺; 所述共聚物的分子量为2000-40000。

6. 发明授权

US4547578A Process for removing naphthoquinone from phthalic anhydride produced through air oxidation of naphthalene 失效
标题翻译：通过萘的空气氧化生产的邻苯二甲酸酐除去萘醌的方法
公开(公告)号：US4547578A
公开(公告)日：1985-10-15
申请号：US583230
申请日：1984-02-24
申请人： Fritz Gude , Herbert Haferkorn
发明人： Fritz Gude , Herbert Haferkorn
IPC分类号： C07D307/89 , C07C51/47 , C07C51/573
CPC分类号： C07C51/573
摘要： The invention relates to a process for removing naphthoquinone from phthalic anhydride produced by the air oxidation of naphthalene or mixtures containing naphthalene. Specifically, crude phthalic anhydride containing naphthoquinone is treated at a temperature of 180.degree.-280.degree. C. with an unsaturated aliphatic oil produced by the polymerization of 1,3-dienes and optionally isomerized having a molecular weight of 800-5,000, and optionally in the presence of 1-40 ppm of alkali ions, relative to the crude phthalic anhydride.
摘要翻译：本发明涉及一种通过萘的空气氧化或含萘的混合物生产的邻苯二甲酸酐除去萘醌的方法。具体地说，含有萘醌的粗邻苯二甲酸酐在180-280℃下用不饱和脂肪油处理，所述不饱和脂肪油通过1,3-二烯的聚合反应，任选地异构化，分子量为800-5,000，相对于粗邻苯二甲酸酐，存在1-40ppm的碱离子。

7. 发明授权

US4248654A Securing substrates together with melt adhesives based on polyamides 失效
标题翻译：用基于聚酰胺的熔融粘合剂固定基材
公开(公告)号：US4248654A
公开(公告)日：1981-02-03
申请号：US655044
申请日：1976-02-04
申请人： Fritz Gude , Siegfried Brandt
发明人： Fritz Gude , Siegfried Brandt
IPC分类号： C08G69/26 , C09J177/00 , C09J3/12
CPC分类号： C08G69/265 , C09J177/00
摘要： A polyamide copolymer, useful as a melt adhesive especially for textiles, produced from the following monomers1. An unbranched aliphatic dicarboxylic acid with 6-20 C-atoms;2. A diamine mixture consisting of(a) 20-80 mol percent, unbranched aliphatic diamines with 6-20 C-atoms; and(b) 80-20 mol percent branched aliphatic and/or cycloaliphatic diamines;said copolymer having a molecular weight of 2000-40000.
摘要翻译：可用作特殊用于纺织品的熔融粘合剂的聚酰胺共聚物，由以下单体制备1.具有6-20个C原子的无支链脂族二羧酸; 2.由（a）20-80摩尔％的具有6-20个碳原子的无支链脂肪族二胺组成的二胺混合物; 和（b）80-20摩尔％的支链脂族和/或脂环族二胺; 所述共聚物的分子量为2000-40000。

8. 发明授权

US4316977A Copolymer of maleic anhydride, dicyclopentadiene and vinylcyclohexene and its use as anionic paper surface sizing material 失效
标题翻译：马来酸酐，二环戊二烯和乙烯基环己烯的共聚物及其作为阴离子纸表面施胶材料的用途
公开(公告)号：US4316977A
公开(公告)日：1982-02-23
申请号：US192853
申请日：1980-10-01
申请人： Fritz Gude , Herbert Haferkorn , Felix Schulde
发明人： Fritz Gude , Herbert Haferkorn , Felix Schulde
IPC分类号： C08F222/06 , D21H17/43
CPC分类号： C08F222/06 , D21H17/43
摘要： Terpolymers of maleic anhydride, dicyclopentadiene, and a vinylcyclohexene, preferably 1-vinylcyclohexene-3, are highly effective paper sizing materials.
摘要翻译：马来酸酐，二环戊二烯和乙烯基环己烯，优选1-乙烯基环己烯-3的三元共聚物是高效的纸浆施胶材料。

9. 发明授权

US4014954A Method for preparing moldings and coatings 失效
标题翻译：制备模塑料和涂料的方法
公开(公告)号：US4014954A
公开(公告)日：1977-03-29
申请号：US582534
申请日：1975-05-30
申请人： Fritz Gude , Siegfried Brandt , Elmar Wolf , Johann Obendorf
发明人： Fritz Gude , Siegfried Brandt , Elmar Wolf , Johann Obendorf
IPC分类号： C09D5/03 , C08G59/00 , C08G59/50 , C08J3/20 , C08L63/00 , C09D5/46 , C09D163/00 , C08L63/02
CPC分类号： C08L63/00
摘要： Molding method and polyadducts for molding objects and coatings from 1,2-epoxy compounds having more than one epoxy group in the molecule and ureas having the formula: ##STR1## wherein N .gtoreq. 1,R' is an alkylene or arylene radical,R" is hydrogen and at least one radical from the group of ##STR2## THE GROUP ##STR3## R'" being the same or different radical from the group of hydrogen and alkyl, X being an R'"OOC--, R'".sub.2 NOC-- or NC-- radical and R"" being alkyl or aryl.
摘要翻译：在分子中具有多于一个环氧基的1,2-环氧化合物和具有下式的脲的成型物和涂料的成型方法和聚合物：其中N≥1，R'是亚烷基或亚芳基， R“是氢，并且来自基团的至少一个基团是与氢和烷基的基团相同或不同的基团，X是R”OOC-， R“'2OC-或NC-基，R”“是烷基或芳基。

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