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1. 发明授权

US07012157B2 Preparation of (meth)acrylic acid 失效
标题翻译：（甲基）丙烯酸的制备
公开(公告)号：US07012157B2
公开(公告)日：2006-03-14
申请号：US10934624
申请日：2004-09-07
申请人： Frieder Borgmeier , Frank Rosowski , Hans Martan , Klaus Joachim Müller-Engel
发明人： Frieder Borgmeier , Frank Rosowski , Hans Martan , Klaus Joachim Müller-Engel
IPC分类号： C07C51/16
CPC分类号： C07C51/215 , B01J23/002 , B01J23/28 , B01J23/8877 , B01J27/0576 , B01J35/0006 , B01J37/0045 , B01J2523/00 , C07C57/04 , B01J2523/55 , B01J2523/56 , B01J2523/64 , B01J2523/68 , B01J2523/847 , B01J2523/32
摘要： A process for preparing (meth)acrylic acid, in which a saturated hydrocarbon precursor compound is conducted through a catalyst charge which consists of two spatially successive catalyst beds I, II in the flow direction of the reaction mixture, each of which contains different catalysts and has different reaction-selectivity behavior.
摘要翻译：一种制备（甲基）丙烯酸的方法，其中饱和烃前体化合物通过催化剂装料进行，催化剂装料由反应混合物流动方向上的两个空间连续的催化剂床I，II组成，每个催化剂床含有不同的催化剂和具有不同的反应选择性行为。

2. 发明申请

US20050065372A1 Preparation of (meth)acrylic acid 失效
标题翻译：（甲基）丙烯酸的制备
公开(公告)号：US20050065372A1
公开(公告)日：2005-03-24
申请号：US10934624
申请日：2004-09-07
申请人： Frieder Borgmeier , Frank Rosowski , Hans Martan , Klaus Muller-Engel
发明人： Frieder Borgmeier , Frank Rosowski , Hans Martan , Klaus Muller-Engel
IPC分类号： B01J23/00 , B01J23/28 , B01J23/887 , B01J27/057 , B01J35/00 , B01J37/00 , C07C51/215 , C07C51/16 , C07C51/235
CPC分类号： C07C51/215 , B01J23/002 , B01J23/28 , B01J23/8877 , B01J27/0576 , B01J35/0006 , B01J37/0045 , B01J2523/00 , C07C57/04 , B01J2523/55 , B01J2523/56 , B01J2523/64 , B01J2523/68 , B01J2523/847 , B01J2523/32
摘要： A process for preparing (meth)acrylic acid, in which a saturated hydrocarbon precursor compound is conducted through a catalyst charge which consists of two spatially successive catalyst beds I, II in the flow direction of the reaction mixture, each of which contains different catalysts and has different reaction-selectivity behavior.
摘要翻译：一种制备（甲基）丙烯酸的方法，其中饱和烃前体化合物通过催化剂装料进行，催化剂装料由反应混合物流动方向上的两个空间连续的催化剂床I，II组成，每个催化剂床含有不同的催化剂和具有不同的反应选择性行为。

3. 发明授权

US07326802B2 Preparation of at least one partial oxidation and/or ammoxidation product of propylene 有权
标题翻译：制备丙烯的至少一种部分氧化和/或氨氧化产物
公开(公告)号：US07326802B2
公开(公告)日：2008-02-05
申请号：US10465656
申请日：2003-06-20
申请人： Claus Hechler , Götz-Peter Schindler , Jochen Petzoldt , Christoph Adami , Otto Machhammer , Klaus Joachim Müller-Engel , Hans Martan
发明人： Claus Hechler , Götz-Peter Schindler , Jochen Petzoldt , Christoph Adami , Otto Machhammer , Klaus Joachim Müller-Engel , Hans Martan
IPC分类号： C07C253/00 , C07C491/00
CPC分类号： C07C51/215 , B01J23/002 , B01J23/8877 , C07C51/252 , C07C253/24 , Y02P20/52 , C07C57/04 , C07C255/08
摘要： In a process for preparing at least one partial oxidation and/or ammoxidation product of propylene, the propylene is obtained from crude propane by dehydrogenating and subjected in the presence of unconverted propane as a constituent of a gas mixture 2 which comprises a total C4-hydrocarbon content of ≦3% by volume to a heterogeneously catalyzed gas phase partial oxidation and/or partial gas phase ammoxidation.
摘要翻译：在制备丙烯的至少一种部分氧化和/或氨氧化产物的方法中，丙烯通过脱氢从粗丙烷获得，并在未转化的丙烷作为气体混合物2的组分存在下进行，所述气体混合物2包含总C

4. 发明授权

US07238827B2 Preparation of at least one partial oxidation and/or ammoxidation product of propylene 有权
标题翻译：制备丙烯的至少一种部分氧化和/或氨氧化产物
公开(公告)号：US07238827B2
公开(公告)日：2007-07-03
申请号：US10465659
申请日：2003-06-20
申请人： Claus Hechler , Götz-Peter Schindler , Jochen Petzoldt , Christoph Adami , Otto Machhammer , Klaus Joachim Müller-Engel , Hans Martan
发明人： Claus Hechler , Götz-Peter Schindler , Jochen Petzoldt , Christoph Adami , Otto Machhammer , Klaus Joachim Müller-Engel , Hans Martan
IPC分类号： C07C253/24 , C07C27/10 , C07C51/215
CPC分类号： C07C51/215 , B01J23/002 , B01J23/8877 , C07C51/252 , C07C253/24 , Y02P20/52 , C07C57/04 , C07C255/08
摘要： Process for preparing at least one partial oxidation and/or ammoxidation product of propylene, in which the propylene is produced from crude propane by dehydrogenation and is subjected to a heterogeneously catalyzed gas-phase partial oxidation and/or partial gas-phase ammoxidation in the presence of unreacted propane as constituent of a gas mixture 2 containing
摘要翻译：制备丙烯的至少一种部分氧化和/或氨氧化产物的方法，其中丙烯由粗丙烷通过脱氢制备，并在存在下进行非均相催化的气相部分氧化和/或部分气相氨氧化的未反应丙烷作为含有1体积％1-丁烯的气体混合物2的组分。

5. 发明授权

US07019168B2 Heterogeneously catalyzed partial gas phase oxidation of propene to acrylic acid 有权
标题翻译：将丙烯非均相催化部分气相氧化成丙烯酸
公开(公告)号：US07019168B2
公开(公告)日：2006-03-28
申请号：US10465653
申请日：2003-06-20
申请人： Martin Dieterle , Jochen Petzoldt , Klaus Joachim Müller-Engel , Hans Martan
发明人： Martin Dieterle , Jochen Petzoldt , Klaus Joachim Müller-Engel , Hans Martan
IPC分类号： C07C51/16 , C07C57/02
CPC分类号： C07C51/252 , C07C57/04
摘要： In a process for partially oxidizing propene to acrylic acid in the gas phase under heterogeneous catalysis, a starting reaction gas mixture comprising propene and oxygen and having a specific composition is oxidized in a first reaction stage over a first fixed catalyst bed having a volume-specific activity which is constant or increases in the flow direction and the acrolein-containing product gas mixture of the first reaction stage is subsequently oxidized in a second reaction stage over a second fixed catalyst bed having a volume-specific activity increasing in the flow direction, and the shaped catalyst bodies of both fixed catalyst beds are annular and each have a specific multimetal oxide composition.
摘要翻译：在非均相催化下在气相中将丙烯部分氧化为丙烯酸的方法中，包含丙烯和氧并具有特定组成的起始反应气体混合物在第一反应阶段在具有体积特异性的第一固定催化剂床上被氧化随后在第二反应阶段，在流动方向上具有体积比活度增加的第二固定催化剂床上氧化第一反应段的流动方向恒定或增加的含丙烯醛的产物气体混合物的活性，以及两个固定催化剂床的成形催化剂体是环状的，并且各自具有特定的多金属氧化物组合物。

6. 发明授权

US07179875B2 Method for producing water-absorbent resins 有权
标题翻译：吸水树脂的制造方法
公开(公告)号：US07179875B2
公开(公告)日：2007-02-20
申请号：US10485484
申请日：2002-08-02
申请人： Eberhard Fuchs , Hans Martan , Gerhard Nestler , Klaus Joachim Mueller-Engel
发明人： Eberhard Fuchs , Hans Martan , Gerhard Nestler , Klaus Joachim Mueller-Engel
IPC分类号： C08F220/06
CPC分类号： C08F220/06 , A61L15/24 , A61L15/60 , C07C51/215 , C07C51/235 , C07C51/252 , C07C51/43 , C07C51/44 , C07C51/487 , C07C57/04 , C08L33/02
摘要： In a process for preparing water-absorbent resins based on acrylic acid, crude acrylic acid is firstly isolated from the reaction gases from the catalytic gas-phase oxidation of propane, propylene and/or acrolein. This is treated with an aldehyde scavenger and pure acrylic acid is separated by distillation from the treated crude acrylic acid, and this pure acrylic acid can be subjected directly to a free-radical polymerization.
摘要翻译：在制备基于丙烯酸的吸水性树脂的方法中，首先从丙烷，丙烯和/或丙烯醛的催化气相氧化反应气体中分离粗丙烯酸。用醛清除剂进行处理，经处理的粗丙烯酸通过蒸馏分离纯丙烯酸，该纯丙烯酸可直接进行自由基聚合。

7. 发明授权

US07157598B2 Method for producing an aqueous alkali acrylate solution 失效
标题翻译：碱性丙烯酸碱水溶液的制造方法
公开(公告)号：US07157598B2
公开(公告)日：2007-01-02
申请号：US10510236
申请日：2003-05-02
申请人： Eberhard Fuchs , Hans Martan , Klaus Joachim Mueller-Engel
发明人： Eberhard Fuchs , Hans Martan , Klaus Joachim Mueller-Engel
IPC分类号： C07C57/02 , C07C51/42
CPC分类号： C07C51/412 , C07C51/44 , C07C57/04
摘要： A process prepares an aqueous alkali metal acrylate solution by distillatively removing acrylic acid from a mixture as vapors and taking up the vapors immediately from the gas phase into an aqueous alkali solution.
摘要翻译：一种方法通过从混合物中蒸馏除去丙烯酸作为蒸气并将蒸气立即从气相中吸收到碱性水溶液中来制备碱金属丙烯酸水溶液。

8. 发明授权

US06207022B1 Purification of crude (meth) acrylic acid 失效
标题翻译：粗制（甲基）丙烯酸的纯化
公开(公告)号：US06207022B1
公开(公告)日：2001-03-27
申请号：US08319667
申请日：1994-10-07
申请人： Toni Dockner , Gerhard Nestler , Holger Herbst , Helmut Lermer , Hans Martan , Herbert Vogel , Herbert Exner
发明人： Toni Dockner , Gerhard Nestler , Holger Herbst , Helmut Lermer , Hans Martan , Herbert Vogel , Herbert Exner
IPC分类号： B01D334
CPC分类号： C07C51/487 , Y10S203/22 , C07C57/04
摘要： Crude (meth)acrylic acid is purified by a process in which a primary amine compound and an organic sulfonic acid are added to the crude (meth)acrylic acid and the latter is then worked up by distillation.
摘要翻译：粗（甲基）丙烯酸通过其中将伯胺化合物和有机磺酸加入到粗（甲基）丙烯酸中的方法纯化，然后将其通过蒸馏处理。

9. 发明申请

US20060205973A1 Process for preparing alkyl esters of (meth)acrylic acid 审中-公开
标题翻译：制备（甲基）丙烯酸的烷基酯的方法
公开(公告)号：US20060205973A1
公开(公告)日：2006-09-14
申请号：US11358220
申请日：2006-02-22
申请人： Thorsten Habeck , Ulrich Rauh , Thorsten Friese , Hans Martan
发明人： Thorsten Habeck , Ulrich Rauh , Thorsten Friese , Hans Martan
IPC分类号： C07C67/36
CPC分类号： C07C67/327 , C07C67/08 , C07C67/54 , C07C69/54
摘要： A process is described for continuously preparing alkyl esters of (meth)acrylic acid by reacting (meth)acrylic acid and alkanols having from 1 to 5 carbon atoms in homogeneous, liquid, solvent-free phase at elevated temperature and in the presence of an acidic esterification catalyst, in which the (meth)acrylic acid, the alkanol and the acidic esterification catalyst are fed to a reaction zone (5, 6), a reaction mixture (21) is discharged from the reaction zone (5, 6), and is introduced into a rectification unit I and separated by addition of water into a top stream (23), comprising the alkyl ester of (meth)acrylic acid, and a bottom stream (22), and a substream of the bottom stream (22) from the rectification unit I is fed to a residue dissociation unit IV, which comprises a dissociating boiler (61), and is separated therein into a top stream (29), which is recycled into the rectification unit I and a bottom stream (40), which is removed from the system, wherein the residue dissociation unit IV, as well as the dissociating boiler (61), further comprises a rectification column (62), the water content of the liquid obtained at the bottommost stage thereof being less than 0.1% by weight.
摘要翻译：描述了一种通过使（甲基）丙烯酸和具有1至5个碳原子的链烷醇在均相，液体，无溶剂相中在升高的温度和酸性存在下连续制备（甲基）丙烯酸的烷基酯的方法酯化催化剂，其中将（甲基）丙烯酸，链烷醇和酸性酯化催化剂加入到反应区（5,6）中，将反应混合物（21）从反应区（5,6）排出，被引入精馏单元I中，并通过加入包含（甲基）丙烯酸的烷基酯和底部流（22））的顶部流（23）和底部流（22）的分流而分离，来自精馏单元I的残渣解离单元IV包含解离锅炉（61），并分离成顶部物流（29），其被再循环到精馏单元I和底部流（40）中，，其从系统中移除，其中残渣解离单元IV以及解离式锅炉（61）还包括精馏塔（62），其最底部得到的液体的含水量小于0.1重量％。

10. 发明授权

US06458989B1 Method for producing (meth)acrylic acid and (meth)acrylic acid esters 有权
标题翻译：（甲基）丙烯酸和（甲基）丙烯酸酯的制备方法
公开(公告)号：US06458989B1
公开(公告)日：2002-10-01
申请号：US09646126
申请日：2000-09-28
申请人： Heinrich Aichinger , Hans Martan , Gerhard Nestler
发明人： Heinrich Aichinger , Hans Martan , Gerhard Nestler
IPC分类号： C07C6748
CPC分类号： C07C51/50 , B01D3/225 , C07C51/44 , C07C51/487 , C07C67/08 , C07C57/04 , C07C69/54
摘要： A process for preparing pure (meth)acrylic acid or a (meth)acrylate starting from a crude (meth)acrylic acid, which comprises the following stages: A: treating the crude (meth)acrylic acid with at least one compound which is able to remove aldehydes, to give an aldehyde-free crude (meth)acrylic acid; B: subjecting the aldehyde-free crude (meth)acrylic acid to imprecise distillation, to give a low-boiling fraction comprising (meth)acrylic acid and acetic acid and a high-boiling fraction comprising (meth)acrylic acid and high boilers; C: isolating a pure (meth)acrylic acid from the high-boiling fraction and, if desired, D: esterifying the low-boiling fraction comprising (meth)acrylic acid and acetic acid that is obtained in stage B by means of one or more alkanols, to give an esterification mixture comprising one or more (meth)acrylates, one or more acetic esters, and one or more alkanols.
摘要翻译：一种从粗（甲基）丙烯酸开始制备纯（甲基）丙烯酸或（甲基）丙烯酸）的方法，其包括以下阶段：A：用至少一种能够去除醛，得到无醛的粗（甲基）丙烯酸; B：使无醛粗（甲基）丙烯酸不精确地进行蒸馏，得到包含（甲基）丙烯酸和乙酸的低沸点馏分以及包含（甲基）丙烯酸和高沸点剂的高沸点馏分; C：从高沸点馏分中分离出纯的（甲基）丙烯酸，如果需要，D：酯化包含（甲基）丙烯酸的低沸点馏分通过一种或多种链烷醇在阶段B中获得的酸和乙酸，得到包含一种或多种（甲基）丙烯酸酯，一种或多种乙酸酯和一种或多种链烷醇的酯化混合物。

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