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1. 发明授权

US4048258A Method for preparing moisture curable polymers containing randomly distributed sites of conjugated olefinic unsaturation 失效
标题翻译：制备含有共轭烯属不饱和键随机分布位点的湿固化聚合物的方法
公开(公告)号：US4048258A
公开(公告)日：1977-09-13
申请号：US679809
申请日：1976-04-23
申请人： Francis P. Baldwin , James A. Rae , Gary Ver Strate
发明人： Francis P. Baldwin , James A. Rae , Gary Ver Strate
IPC分类号： C08F8/42 , C08F8/46 , C08F255/08 , C08F255/10 , C08F279/02
CPC分类号： C08F8/42 , C08F8/46
摘要： Disclosed is a method of preparing a moisture curable elastomer by reacting an elastomer containing randomly distributed sites of conjugated olefinic unsaturation with a cyclic unsaturated anhydride then blending the reaction product with a polyvalent metal compound and, optionally, a basic hydrolysis catalyst.
摘要翻译：本发明公开了一种制备湿固化弹性体的方法，该方法是使含有共轭烯属不饱和官能团随机分布的弹性体与环状不饱和酸酐反应，然后将反应产物与多价金属化合物和任选的碱性水解催化剂混合。

2. 发明授权

US4068051A Process for preparing conjugated diene butyl 失效
标题翻译：共轭二烯丁基的制备方法
公开(公告)号：US4068051A
公开(公告)日：1978-01-10
申请号：US631483
申请日：1975-11-13
申请人： Francis P. Baldwin , James A. Rae
发明人： Francis P. Baldwin , James A. Rae
IPC分类号： C08F8/00 , C08F8/26
CPC分类号： C08F8/26
摘要： Improved processes for the dehydrohalogenation of halogenated butyl rubber in order to prepare a butyl rubber having randomly distributed sites of conjugated unsaturation are disclosed. Such processes, which include the contacting of a solution of halogenated butyl rubber with a soluble metal carboxylate, a soluble carboxylic acid, and an oxide or hydroxide of a metal selected from Groups Ia and IIa of the Periodic Table, are carried out in a reaction zone which is maintained substantially free of free water vapor. Preferably, excess amounts of hydrophilic reagents are added to the reaction zone or in the alternative the reaction zone is purged with a drying gas.
摘要翻译：公开了用于制备具有共轭不饱和度的随机分布位点的丁基橡胶的卤化丁基橡胶的脱卤化氢的改进方法。这些方法包括将卤代丁基橡胶与可溶性金属羧酸盐的溶液，可溶性羧酸和选自元素周期表第Ia和IIa族的金属的氧化物或氢氧化物的接触反应在反应中进行保持基本上不含游离水蒸气的区域。优选地，将过量的亲水试剂加入到反应区中，或者在反应区中用干燥气体吹扫反应区。

3. 发明授权

US4038472A Novel curing system for conjugated diene butyl elastomers 失效
标题翻译：新型固化丁二烯弹性体固化体系
公开(公告)号：US4038472A
公开(公告)日：1977-07-26
申请号：US661286
申请日：1976-02-25
申请人： James A. Rae
发明人： James A. Rae
IPC分类号： C08K5/13 , C08F8/00 , C08F8/06 , C08F8/42
CPC分类号： C08K5/13
摘要： Conjugated diene butyl (CDB) elastomer copolymers are cured with a system comprising dihydroxybenzene and an oxidant or oxidation catalyst whereby benzoquinone is formed which acts as the crosslinking dienophile. The process allows for satisfactory cures at room temperature.

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