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1. 发明授权

US06331608B1 Process for producing poly(arylene sulfide) 有权
标题翻译：生产聚（亚芳基硫醚）的方法
公开(公告)号：US06331608B1
公开(公告)日：2001-12-18
申请号：US09394790
申请日：1999-09-13
申请人： Fernando C. Vidaurri , Jon F. Geibel , James W. Waterman , Jay M. Chaffin , Aubrey South, Jr. , Jeffrey S. Fodor , Glenn F. Kile
发明人： Fernando C. Vidaurri , Jon F. Geibel , James W. Waterman , Jay M. Chaffin , Aubrey South, Jr. , Jeffrey S. Fodor , Glenn F. Kile
IPC分类号： C08G7514
CPC分类号： C07D207/267 , C08G75/0281
摘要： A process is provided to recover at least one modifier compound and at least one polar organic compound from a reaction mixture comprising high molecular weight Poly(arylene sulfide) product, low molecular weight P(AS), cyclic and linear P(AS) oligomers, at least one POC, at least one modifier, an alkali metal halide by-product, and water.
摘要翻译：提供了一种从包含高分子量聚（亚芳基硫醚）产物，低分子量P（AS），环状和线型P（AS）低聚物的反应混合物中回收至少一种改性剂化合物和至少一种极性有机化合物的方法，至少一种POC，至少一种改性剂，碱金属卤化物副产物和水。

2. 发明授权

US06946540B2 Method of measuring extent of curing of compacted poly(arylene sulfide) 失效
标题翻译：测定压实聚（亚芳基硫）的固化程度的方法
公开(公告)号：US06946540B2
公开(公告)日：2005-09-20
申请号：US10395919
申请日：2003-03-24
申请人： Fernando C. Vidaurri , Aubrey South, Jr. , David A. Soules , Jeffrey S. Fodor
发明人： Fernando C. Vidaurri , Aubrey South, Jr. , David A. Soules , Jeffrey S. Fodor
IPC分类号： C08L81/02 , C08G10/02
CPC分类号： C08L81/02
摘要： Disclosed herein is a process for preparing cured arylene sulfide polymers. A first curing vessel comprising a first agitator is used to cure a poly(arylene sulfide) compacted powder. The curing proceeds until the compacted powder reaches a melt flow rate within a target range. When the melt flow rate of the compacted powder first reaches the target range, the power consumption of the first agitator is determined. A second curing vessel comprising a second agitator is charged with a second quantity of the compacted poly(arylene sulfide) powder. The second quantity of compacted powder is cured in the second vessel until the power consumption of the second agitator reaches the value at which the melt flow rate in the first curing vessel first reached the target range.
摘要翻译：本文公开了一种制备硫化亚芳基硫醚聚合物的方法。使用包含第一搅拌器的第一固化容器来固化聚（亚芳基硫醚）压实粉末。固化进行直到压实粉末达到目标范围内的熔体流动速率。当压实粉末的熔体流动速率首先达到目标范围时，确定第一搅拌器的功率消耗。装有第二搅拌器的第二固化容器装有第二量压实的聚（亚芳基硫醚）粉末。第二量的压实粉末在第二容器中固化，直到第二搅拌器的功率消耗达到第一固化容器中的熔体流动速率首先达到目标范围的值。

3. 发明授权

US06307011B1 Recovery of modifier compounds and polar organic compounds from a poly(arylene sulfide) recycle mixture 有权
标题翻译：从聚（亚芳基硫醚）再循环混合物回收改性剂化合物和极性有机化合物
公开(公告)号：US06307011B1
公开(公告)日：2001-10-23
申请号：US09394489
申请日：1999-09-13
申请人： Jeffrey S. Fodor , Jon F. Geibel , Fernando C. Vidaurri
发明人： Jeffrey S. Fodor , Jon F. Geibel , Fernando C. Vidaurri
IPC分类号： C08F608
CPC分类号： C07D207/267 , C08G75/0281
摘要： A process is provided to recover at least one modifier compound and at least one polar organic compound from a P(AS) recycle mixture.
摘要翻译：提供了从P（AS）再循环混合物回收至少一种改性剂化合物和至少一种极性有机化合物的方法。

4. 发明授权

US5296579A Arylene sulfide polymers 失效
标题翻译：亚芳基硫化物聚合物
公开(公告)号：US5296579A
公开(公告)日：1994-03-22
申请号：US155179
申请日：1988-02-11
申请人： Jon F. Geibel , Robert W. Campbell , Guy Senatore , Fernando C. Vidaurri , Mark A. Haney
发明人： Jon F. Geibel , Robert W. Campbell , Guy Senatore , Fernando C. Vidaurri , Mark A. Haney
IPC分类号： C08G75/02 , C08F8/32
CPC分类号： C08G75/025 , Y02P20/582
摘要： A process for the production of arylene sulfide polymers is provided which comprises subjecting a mixture of at least one first sulfur source, at least one second sulfur source comprised of at least one organic monothiol compound, at least one polyhalo-substituted aromatic compound and at least one polar organic compound to polymerization conditions sufficient to produce the arylene sulfide polymer. The organic monothiol compound can be added at any time prior to substantial completion of polymerization to provide arylene sulfide polymers of increased extrusion rate.
摘要翻译：提供了一种生产亚芳基硫化物聚合物的方法，其包括使至少一种第一硫源，至少一种由至少一种有机一硫醇化合物组成的至少一种第二硫源，至少一种多卤代芳香族化合物和至少一种极性有机化合物与足以产生亚芳基硫醚聚合物的聚合条件。可以在基本上完成聚合之前的任何时间加入有机单硫代化合物，以提供具有增加的挤出速率的亚芳基硫醚聚合物。

5. 发明授权

US4370470A Multistage, agitated contactor and its use in continuous production of arylene sulfide polymer 失效
标题翻译：多级搅拌接触器及其在连续生产亚芳基硫醚聚合物中的应用
公开(公告)号：US4370470A
公开(公告)日：1983-01-25
申请号：US254679
申请日：1981-04-16
申请人： Fernando C. Vidaurri , Kenneth L. Anderson
发明人： Fernando C. Vidaurri , Kenneth L. Anderson
IPC分类号： B01J19/18 , C08G75/02 , C08G75/06 , C08G75/14
CPC分类号： B01J19/1862 , C08G75/025 , B01J2219/00094 , B01J2219/00162
摘要： A contacting apparatus that is a vertically elongated, cylindrical shell having closed ends and separated by horizontal baffle plates into a multiplicity of discrete chambers with access from one chamber to another through concentric circular holes, axially centered in the baffles with a continuously rotatable shaft extending concentric with the baffles within the shell with at least one agitator means attached to the shaft positioned in each chamber and with the shaft in the circular openings providing annular openings in the baffles such the the ratio of backflow rate to feed rate through the openings is less than 1.5.A method for continuously producing arylene sulfide polymer in which reactants suitable for producing poly(arylene sulfide) are introduced into at least a first chamber of the contacting vessel described above thereby forming a reaction mixture which is passed through the chambers of the contactor while maintaining each chamber within conditions for producing arylene sulfide polymer and recovering arylene sulfide polymer from a chamber removed from the chamber into which the initial reactants are introduced.
摘要翻译：一种接触装置，其是具有闭合端并由水平挡板分隔成多个不连续室的接触装置，其中多个离散的室具有从一个室到另一个通过同心的圆孔，轴向居中在挡板中，具有连续可旋转的轴同心延伸壳体内的挡板具有连接到位于每个室中的轴的至少一个搅拌器装置，并且在圆形开口中的轴提供挡板中的环形开口，使得回流速率与通过开口的进给速率之比小于 1.5。一种连续生产亚芳基硫醚聚合物的方法，其中适用于生产聚（亚芳基硫醚）的反应物被引入到上述接触容器的至少第一室中，从而形成反应混合物，该反应混合物通过接触器的室，同时保持每个在产生亚芳基硫醚聚合物的条件下，从从引入初始反应物的室中除去的室中回收亚芳硫醚聚合物。

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