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    • 3. 发明申请
    • Methods For Preparing Iron Source Material And Ferrous Oxalate for Lithium Ferrous Phosphate
    • 磷酸铁锂铁源和草酸亚铁的制备方法
    • US20090252668A1
    • 2009-10-08
    • US12176319
    • 2008-07-18
    • Wenyu CaoShuiyuan ZhangFeng Xiao
    • Wenyu CaoShuiyuan ZhangFeng Xiao
    • C01B25/30
    • C01B25/45H01M4/5825H01M10/052
    • Methods for preparing iron source material and ferrous oxalate for lithium ferrous phosphate are disclosed. One method comprises bringing solution containing ferrite and soluble non-ferrous metal salts in contact with oxalate solution; wherein said method of contact is to allow a flow of the ferrite solution containing ferrite and soluble non-ferrous metal salts to come in contact with a flow of oxalate solution. Another method comprises brings a stream of ferrite solution in contact with a stream of oxalate solution, wherein the flow rates of the ferrite solution and oxalate solution give the resulting slurry a pH of 2-6. The ferrous oxalate particles produces by the methods of the present invention are regularly shaped and have small and evenly distributed diameters. Lithium ferrous phosphate made from iron source material and ferrous oxalate prepared using the methods of the present invention has small particle diameter, homogeneous particle size, good electrical conductivity, and superior electrochemical properties.
    • 公开了用于制备磷酸亚铁的铁源材料和草酸亚铁的方法。 一种方法包括将含铁素体和可溶性有色金属盐的溶液与草酸盐溶液接触; 其中所述接触方法是允许含有铁素体和可溶性有色金属盐的铁素体溶液与草酸溶液流接触。 另一种方法包括使铁酸盐溶液与草酸溶液流接触,其中铁酸盐溶液和草酸溶液的流速使得到的浆料的pH为2-6。 通过本发明的方法生产的草酸亚铁颗粒是规则形状的并且具有小且均匀分布的直径。 由本发明方法制备的由铁源材料和草酸亚铁制成的磷酸亚铁锂具有粒径小,粒径均匀,导电性好,电化学性能优异的特点。