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1. 发明授权

US3947384A Method for making matt finish coatings 失效
标题翻译：制造无光饰面涂层的方法
公开(公告)号：US3947384A
公开(公告)日：1976-03-30
申请号：US470232
申请日：1974-05-15
申请人： Felix Schulde , Johann Obendorf , Kurt Neubold , Gunter Dormann
发明人： Felix Schulde , Johann Obendorf , Kurt Neubold , Gunter Dormann
IPC分类号： C09D5/00 , B01J19/24 , C08G59/00 , C08G59/40 , C08G59/50 , C09D5/03 , C09D5/46 , C09D163/00
CPC分类号： C08G59/5093 , B01J19/2405
摘要： Coatings having a matt finish are made by applying a powder varnish composition to a substrate and thereafter reacting the varnish at a temperature of 100.degree. to 240.degree.C to form the matt finish coating. The powder varnish composition is a finely divided, particulate mixture ofI. a 1,2-epoxy compound having a melting point greater than 40.degree.C and containing at least one 1,2-epoxy group; andIi. a salt of a polycarboxylic acid (such as pyromellitic acid) containing three or more carboxyl groups and a cyclic amidine (such as 2-phenylimidazoline).
摘要翻译：通过将粉末状清漆组合物涂布在基材上，然后使该清漆在100〜240℃的温度下反应，形成无光饰面涂层，制成具有亚光光洁度的涂料。粉末清漆组合物是I的细碎的颗粒混合物。具有40℃以上并且含有至少一个1,2-环氧基的熔点大于1:1的1,2-环氧化合物; 和II。含有三个或更多个羧基的聚碳酸（如吡啶甲酸）的盐和一个环状的氨基（如2-苯基咪唑啉）。

2. 发明授权

US4007299A Method for making matt finish coatings 失效
标题翻译：制造无光饰面涂层的方法
公开(公告)号：US4007299A
公开(公告)日：1977-02-08
申请号：US606623
申请日：1975-08-21
申请人： Felix Schulde , Johann Obendorf , Kurt Neubold , Gunter Dormann
发明人： Felix Schulde , Johann Obendorf , Kurt Neubold , Gunter Dormann
IPC分类号： B05D5/02 , C08G59/50 , B05D3/02 , B05D3/10
CPC分类号： B05D5/02 , C08G59/5093 , C08K5/09 , B05D2401/32 , Y10S525/934
摘要： Coatings having a matt finish are made by applying a powder varnish composition to a substrate and thereafter reacting the varnish at a temperature of 100.degree. to 240.degree. C to form the matt finish coating. The powder varnish composition is a finely divided, particulate mixture ofI. a 1,2-epoxy compound having a melting point greater than 40.degree. C and containing at least one 1,2-epoxy group; andIi. a salt of a polycarboxylic acid (such as pyromellite acid) containing three or more carboxyl groups and a cyclic amidine (such as 2-phenylimidazoline).
摘要翻译：通过将粉末状清漆组合物涂布在基材上，然后使该清漆在100〜240℃的温度下反应，形成无光饰面涂层，制成具有亚光光洁度的涂料。粉末清漆组合物是I的细碎的颗粒混合物。具有40℃以上并且含有至少一个1,2-环氧基的熔点大于1:1的1,2-环氧化合物; 和II。含有三个或更多个羧基的聚碳酸（如氰尿酸）和环状氨基酸（如2-苯基咪唑啉）等。

3. 发明授权

US4382876A Method for producing catalysts for gas phase oxidation of saturated and/or unsaturated C.sub.4 -hydrocarbons to maleic anhydride 失效
标题翻译：用于生产饱和和/或不饱和C 4烃至马来酸酐的气相氧化催化剂的方法
公开(公告)号：US4382876A
公开(公告)日：1983-05-10
申请号：US244112
申请日：1981-03-16
申请人： Kurt Neubold , Klaus-Dieter Gollmer
发明人： Kurt Neubold , Klaus-Dieter Gollmer
IPC分类号： C07D307/60 , B01J23/22 , B01J27/18 , B01J27/198 , C01B25/45 , C07B61/00 , C07C51/215 , C07C51/25 , B01J27/14
CPC分类号： C07C51/252 , B01J23/002 , B01J23/22 , B01J27/198 , C07C51/215 , B01J2523/00
摘要： A method for producing catalysts for gas phase oxidation of saturated or unsaturated hydrocarbons to maleic anhydride is disclosed comprising: (a) mixing a vanadium compound containing pentavalent vanadium with orthophosphoric acid in an alcohol from the series of monohydric lower aliphatic alcohols having 2-8 C-atoms in the optional presence of promoters, and a reducing agent combination of H.sub.3 PO.sub.3 +alcohol wherein the sum of H.sub.3 PO.sub.3 and H.sub.3 PO.sub.4 is so controlled that an atomic ratio of P to V of 1.0 to 1.2 is attained and wherein said H.sub.3 PO.sub.3 is used in such sub-stoichiometric amounts that it is sufficient to reduce the vanadium to an oxidation state only of 4.2 to 4.4, and then said reducing agent combination is used to further reduce the vanadium to an oxidation state between 3.9 to 4.0, any water if present being distilled off as an azeotrope with the alcohol by heating; (b) adding titanium dioxide obtained through high temperature pyrolysis of titanium tetrahalide and optional additional promoters Ni, Fe, Li, Mg; (c) forming precipitated catalyst in a known manner; and (d) activating the catalyst in an oxidation reactor at temperatures of about 450.degree. to 510.degree. C. for about 12 to 72 hours in the presence of an air-hydrocarbon stream.
摘要翻译：公开了一种制备用于将饱和或不饱和烃气相氧化成马来酸酐的催化剂的方法，其包括：（a）将含有五价钒的钒化合物与醇中的正磷酸从具有2-8C的一系列一元低级脂族醇混合原子在可选的助催化剂存在下进行，以及H 3 PO 3 +醇的还原剂组合，其中H 3 PO 3和H 3 PO 4的总和被控制以使得P与V的原子比为1.0至1.2，并且其中所述H 3 PO 3用于亚化学计量的量，足以将钒还原成氧化态仅为4.2至4.4，然后所述还原剂组合用于进一步将钒还原为3.9至4.0之间的氧化态，任何水（如果存在）蒸馏通过加热与酒精共沸; （b）加入通过四卤化钛的高温热解获得的二氧化钛和任选的另外的助催化剂Ni，Fe，Li，Mg; （c）以已知方式形成沉淀的催化剂; 和（d）在空气 - 烃流的存在下，在约450℃至510℃的温度下在氧化反应器中活化催化剂约12至72小时。

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