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    • 4. 发明授权
    • Rapid synthesis of fuel cell catalyst using controlled microwave heating
    • 使用受控微波加热快速合成燃料电池催化剂
    • US08563463B1
    • 2013-10-22
    • US13537842
    • 2012-06-29
    • Ellazar V. NiangarTaehee Han
    • Ellazar V. NiangarTaehee Han
    • B01J23/00
    • B01J37/346H01M4/921H01M4/923H01M4/926Y02E60/50
    • Methods for the rapid synthesis of catalyst are disclosed herein, as well as catalyst formed from such methods. One method of the rapid synthesis of catalyst comprises first forming a solution that comprises a solvent, a precious metal precursor, a catalyst substrate, a reducing agent and a stabilizer. The solution is homogenized. The precious metal precursor is reduced to nanoparticles of the precious metal and the nanoparticles are deposited onto the catalyst substrate to form catalyst particles. Reducing and depositing comprise increasing a temperature of the solution with microwave irradiation at a controlled rate to a predetermined temperature and holding the solution at the predetermined temperature with microwave irradiation until the reduction and depositing are detected to be complete.
    • 本文公开了快速合成催化剂的方法,以及由这些方法形成的催化剂。 快速合成催化剂的一种方法包括首先形成包含溶剂,贵金属前体,催化剂底物,还原剂和稳定剂的溶液。 将溶液均化。 将贵金属前体还原成贵金属的纳米颗粒,并将纳米颗粒沉积到催化剂基质上以形成催化剂颗粒。 还原和沉积包括以微波照射将微波照射的温度控制在一定温度,并用微波照射将溶液保持在预定温度,直到检测到还原和沉积完成。