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1. 发明授权

US09416198B2 Method for producing alkali cellulose 有权
标题翻译：碱性纤维素的制造方法
公开(公告)号：US09416198B2
公开(公告)日：2016-08-16
申请号：US14115252
申请日：2012-04-27
申请人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Yoichiro Imori , Toru Nishioka
发明人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Yoichiro Imori , Toru Nishioka
IPC分类号： C08B15/00 , C08B1/06 , C08B1/08 , C08B11/08 , C08B11/00 , C08B11/02 , C08B11/06 , C08B11/12 , C08B11/14 , C08B11/20 , C08H8/00 , D21C9/00
CPC分类号： C08B1/08 , C08B1/06 , C08B11/00 , C08B11/02 , C08B11/06 , C08B11/08 , C08B11/12 , C08B11/14 , C08B11/20 , C08H8/00 , D21C9/004 , D21C9/007
摘要： The present invention relates to a method for producing an alkali cellulose with suppressed decrease in the degree of polymerization as well as with small use amount of a basic compound, and to a method for producing a cellulose ether by using the alkali cellulose thus obtained. Provided by the present invention are: (A) a method for producing an alkali cellulose, comprising Step 1 wherein a cellulose-containing raw material (I) is treated by a pulverizing machine thereby obtaining a cellulose-containing raw material (II) which contains a cellulose having crystallinity in the range of 10 to 55% and Step 2 wherein the cellulose-containing raw material (II) obtained in Step 1 is added by a basic compound with the amount thereof being in the range of 0.6 to 1.5 mol relative to 1 mol of an anhydroglucose unit that constitutes the said cellulose as well as by water with the amount thereof being in the range of 20 to 100% by mass relative to the said cellulose thereby obtaining the alkali cellulose; and (B) a method for producing a cellulose ether by reacting the alkali cellulose produced by the foregoing production method with an etherification agent.
摘要翻译：本发明涉及一种碱性纤维素的制造方法，其抑制聚合度的降低以及碱性化合物的使用量的降低，以及通过使用由此得到的碱纤维素制造纤维素醚的方法。本发明提供：（A）碱纤维素的制造方法，其包括步骤1，其中通过粉碎机处理含纤维素的原料（I），从而得到含有纤维素的原料（II），其含有结晶度为10〜55％的纤维素和步骤2，其中步骤1中得到的含纤维素原料（II）相对于碱性化合物为0.6〜1.5mol，相对于 1mol构成上述纤维素的脱水葡萄糖单元以及水相对于所述纤维素为20〜100质量％的水分，得到碱纤维素; 和（B）通过使通过上述制备方法制备的碱纤维素与醚化剂反应制备纤维素醚的方法。

2. 发明申请

US20140073777A1 METHOD FOR PRODUCING ALKALI CELLULOSE 有权
标题翻译：生产碱性纤维素的方法
公开(公告)号：US20140073777A1
公开(公告)日：2014-03-13
申请号：US14115252
申请日：2012-04-27
申请人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Yoichiro Imori , Toru Nishioka
发明人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Yoichiro Imori , Toru Nishioka
IPC分类号： C08B1/08 , C08B11/08
CPC分类号： C08B1/08 , C08B1/06 , C08B11/00 , C08B11/02 , C08B11/06 , C08B11/08 , C08B11/12 , C08B11/14 , C08B11/20 , C08H8/00 , D21C9/004 , D21C9/007
摘要： The present invention relates to a method for producing an alkali cellulose with suppressed decrease in the degree of polymerization as well as with small use amount of a basic compound, and to a method for producing a cellulose ether by using the alkali cellulose thus obtained. Provided by the present invention are: (A) a method for producing an alkali cellulose, comprising Step 1 wherein a cellulose-containing raw material (I) is treated by a pulverizing machine thereby obtaining a cellulose-containing raw material (II) which contains a cellulose having crystallinity in the range of 10 to 55% and Step 2 wherein the cellulose-containing raw material (II) obtained in Step 1 is added by a basic compound with the amount thereof being in the range of 0.6 to 1.5 mol relative to 1 mol of an anhydroglucose unit that constitutes the said cellulose as well as by water with the amount thereof being in the range of 20 to 100% by mass relative to the said cellulose thereby obtaining the alkali cellulose; and (B) a method for producing a cellulose ether by reacting the alkali cellulose produced by the foregoing production method with an etherification agent.
摘要翻译：本发明涉及一种碱性纤维素的制造方法，其抑制聚合度的降低以及碱性化合物的使用量的降低，以及通过使用由此得到的碱纤维素制造纤维素醚的方法。本发明提供：（A）碱纤维素的制造方法，其包括步骤1，其中通过粉碎机处理含纤维素的原料（I），从而得到含有纤维素的原料（II），其含有结晶度为10〜55％的纤维素和步骤2，其中步骤1中得到的含纤维素原料（II）相对于碱性化合物为0.6〜1.5mol，相对于 1mol构成上述纤维素的脱水葡萄糖单元以及水相对于所述纤维素为20〜100质量％的水分，得到碱纤维素; 和（B）通过使通过上述制备方法制备的碱纤维素与醚化剂反应制备纤维素醚的方法。

3. 发明授权

US09416199B2 Method for producing alkali cellulose 有权
标题翻译：碱性纤维素的制造方法
公开(公告)号：US09416199B2
公开(公告)日：2016-08-16
申请号：US14115212
申请日：2012-04-27
申请人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Kenichi Shiba , Rui Takahashi , Yoichiro Imori
发明人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Kenichi Shiba , Rui Takahashi , Yoichiro Imori
IPC分类号： C08B15/00 , C08B1/06 , C08B1/08 , C08B11/08 , C08H8/00 , C08L1/26
CPC分类号： C08B15/00 , C08B1/06 , C08B1/08 , C08B11/08 , C08H8/00 , C08L1/26
摘要： The present invention relates to a method for producing an alkali cellulose with suppressed decrease in the degree of polymerization as well as with small use amount of a basic compound, and to a method for producing a cellulose ether by using the alkali cellulose thus obtained. Provided by the present invention are: (A) a method for producing an alkali cellulose, comprising Step 1 wherein a cellulose-containing raw material is pulverized in the presence of 0.6 to 1.5 mol of a basic compound relative to 1 mol of an anhydroglucose unit that constitutes a cellulose in the said cellulose-containing raw material and under the condition in which the water content therein relative to the cellulose in the cellulose-containing raw material is 10% or less by mass thereby obtaining a cellulose powder mixture having the median diameter of the cellulose-containing raw material made 150 μm or less and Step 2 wherein water content therein is adjusted in the range of 30 to 100% by mass relative to the cellulose by adding water to the cellulose powder mixture thereby obtaining the alkali cellulose in the powder form; and (B) a method for producing a cellulose ether by reacting the alkali cellulose produced by the foregoing production method with an etherification agent.
摘要翻译：本发明涉及一种碱性纤维素的制造方法，其抑制聚合度的降低以及碱性化合物的使用量的降低，以及通过使用由此得到的碱纤维素制造纤维素醚的方法。本发明提供的是：（A）碱纤维素的制造方法，其中，相对于1摩尔脱水葡萄糖单元，在0.6〜1.5摩尔碱性化合物的存在下，将含纤维素原料粉碎的工序1 所述纤维素原料中的纤维素构成纤维素，其中相对于纤维素原料中的纤维素含水量为10质量％以下的条件下，由此得到中等粒径的纤维素粉末混合物的纤维素原料150μm以下，步骤2，其中通过向纤维素粉末混合物中加入水，相对于纤维素将水分含量调节在30〜100质量％的范围内，由此得到粉末形式和（B）通过使通过上述制备方法制备的碱纤维素与醚化剂反应制备纤维素醚的方法。

4. 发明申请

US20140073773A1 METHOD FOR PRODUCING ALKALI CELLULOSE 有权
标题翻译：生产碱性纤维素的方法
公开(公告)号：US20140073773A1
公开(公告)日：2014-03-13
申请号：US14115212
申请日：2012-04-27
申请人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Kenichi Shiba , Rui Takahashi , Yoichiro Imori
发明人： Eisuke Miyoshi , Yutaka Yoshida , Ryo Miyasato , Kenichi Shiba , Rui Takahashi , Yoichiro Imori
IPC分类号： C08B15/00
CPC分类号： C08B15/00 , C08B1/06 , C08B1/08 , C08B11/08 , C08H8/00 , C08L1/26
摘要： The present invention relates to a method for producing an alkali cellulose with suppressed decrease in the degree of polymerization as well as with small use amount of a basic compound, and to a method for producing a cellulose ether by using the alkali cellulose thus obtained. Provided by the present invention are: (A) a method for producing an alkali cellulose, comprising Step 1 wherein a cellulose-containing raw material is pulverized in the presence of 0.6 to 1.5 mol of a basic compound relative to 1 mol of an anhydroglucose unit that constitutes a cellulose in the said cellulose-containing raw material and under the condition in which the water content therein relative to the cellulose in the cellulose-containing raw material is 10% or less by mass thereby obtaining a cellulose powder mixture having the median diameter of the cellulose-containing raw material made 150 μm or less and Step 2 wherein water content therein is adjusted in the range of 30 to 100% by mass relative to the cellulose by adding water to the cellulose powder mixture thereby obtaining the alkali cellulose in the powder form; and (B) a method for producing a cellulose ether by reacting the alkali cellulose produced by the foregoing production method with an etherification agent.
摘要翻译：本发明涉及一种碱性纤维素的制造方法，其抑制聚合度的降低以及碱性化合物的使用量的降低，以及通过使用由此得到的碱纤维素制造纤维素醚的方法。本发明提供的是：（A）碱纤维素的制造方法，其中，相对于1摩尔脱水葡萄糖单元，在0.6〜1.5摩尔碱性化合物的存在下，将含纤维素原料粉碎的工序1 所述纤维素原料中的纤维素构成纤维素，其中相对于纤维素原料中的纤维素含水量为10质量％以下的条件下，由此得到中等粒径的纤维素粉末混合物的纤维素原料制成150μm以下，步骤2，其中通过向纤维素粉末混合物中加入水，相对于纤维素将水分含量调节在30〜100质量％的范围内，由此得到粉末形式和（B）通过使通过上述制备方法制备的碱纤维素与醚化剂反应制备纤维素醚的方法。

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