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1. 发明授权

US09018121B2 Bimetallic catalyst and use in xylene production 有权
标题翻译：双金属催化剂和用于二甲苯生产
公开(公告)号：US09018121B2
公开(公告)日：2015-04-28
申请号：US13747905
申请日：2013-01-23
申请人： ExxonMobil Chemical Patents Inc.
发明人： April D. Ross , Jane C. Cheng
IPC分类号： B01J29/06 , B01J8/04 , B01J16/00 , C07C5/27 , B01J29/40 , B01J29/44 , B01J29/46 , B01J37/00 , B01J23/42 , B01J23/50 , B01J23/60 , B01J23/62 , B01J23/89
CPC分类号： C07C5/2708 , B01J16/005 , B01J23/42 , B01J23/50 , B01J23/60 , B01J23/62 , B01J23/626 , B01J23/628 , B01J23/8926 , B01J29/405 , B01J29/44 , B01J29/46 , B01J37/0018 , B01J2229/186 , B01J2229/36 , B01J2229/42 , C07C5/222 , C07C5/2556 , C07C5/2737 , C07C5/2754 , C07C15/08 , C07C2529/44 , Y02P20/52
摘要： The invention is directed to a bimetallic catalyst system adapted for the manufacture of xylenes, a process for making said catalyst system, and to the process of manufacture of xylenes using said catalyst system, providing, in embodiments, improved selectivity by at least one of higher ethylene saturation and low xylene loss, decreased susceptibility to poisoning from feedstream impurities, and ability to operate at less severe conditions.
摘要翻译：本发明涉及适用于制造二甲苯的双金属催化剂体系，制备所述催化剂体系的方法，以及使用所述催化剂体系制备二甲苯的方法，在实施方案中，提供了至少一种较高的选择性乙烯饱和度低，二甲苯损失低，对原料杂质中毒的易感性降低，在恶劣条件下操作能力差。

2. 发明授权

US09006125B2 Transalkylation of heavy aromatic hydrocarbon feedstocks 有权
标题翻译：重芳香烃原料的烷基转移
公开(公告)号：US09006125B2
公开(公告)日：2015-04-14
申请号：US13899854
申请日：2013-05-22
申请人： ExxonMobil Chemical Patents Inc.
发明人： Doron Levin , April D. Ross , James H. Beech, Jr.
IPC分类号： B01J29/06 , B01J8/04 , B01J29/064 , B01J29/072 , B01J29/076 , B01J29/44 , B01J29/46 , B01J29/70 , B01J29/76 , B01J35/00 , B01J35/02 , B01J37/20 , C07C6/12 , B01J37/00
CPC分类号： B01J8/04 , B01J29/064 , B01J29/072 , B01J29/076 , B01J29/44 , B01J29/46 , B01J29/7034 , B01J29/7669 , B01J35/0006 , B01J35/023 , B01J37/0009 , B01J37/20 , B01J2229/42 , C07C6/12 , C07C2529/42 , Y02P20/52 , C07C15/08
摘要： In a process for producing xylene by transalkylation of a C9+ aromatic hydrocarbon feedstock with a C6 and/or C7 aromatic hydrocarbon, the C9+ aromatic hydrocarbon feedstock, at least one C6 and/or C7 aromatic hydrocarbon and hydrogen are contacted with a first catalyst comprising (i) a first molecular sieve having a Constraint Index in the range of about 3 to about 12 and (ii) at least first and second different metals or compounds thereof of Groups 6 to 12 of the Periodic Table of the Elements. Contacting with the first catalyst is conducted under conditions effective to dealkylate aromatic hydrocarbons in the feedstock containing C2+ alkyl groups and to saturate C2+ olefins formed so as to produce a first effluent. At least a portion of the first effluent is then contacted with a second catalyst comprising a second molecular sieve having a Constraint Index less than 3 under conditions effective to transalkylate C9+ aromatic hydrocarbons with said at least one C6-C7 aromatic hydrocarbon to form a second effluent comprising xylene.
摘要翻译：在通过C 9 +芳族烃原料与C 6和/或C 7芳烃的烷基转移生产二甲苯的方法中，C 9 +芳烃原料，至少一种C 6和/或C 7芳烃和氢与第一催化剂接触，所述第一催化剂包含（ i）具有在约3至约12范围内的约束指数的第一分子筛和（ii）至少元素周期表第6至12族的第一和第二不同金属或其化合物。与第一催化剂接触在有效地使含有C 2 +烷基的原料中芳族烃脱烷基化并使形成的C 2 +烯烃饱和以产生第一流出物的条件下进行。然后至少一部分第一流出物与包含第二分子筛的第二催化剂接触，该第二催化剂在有效使C 9+芳族烃与所述至少一种C 6 -C 7芳族烃烷基转移的条件下具有小于3的约束指数，以形成第二流出物包括二甲苯。

3. 发明申请

US20140171293A1 Xylene Isomerization Process and Catalyst Therefor 审中-公开
标题翻译：二甲苯异构化方法及催化剂
公开(公告)号：US20140171293A1
公开(公告)日：2014-06-19
申请号：US14186453
申请日：2014-02-21
申请人： EXXONMOBIL CHEMICAL PATENTS INC.
发明人： John D. Ou , April D. Ross , Doron Levin , Mohan Kalyanaraman , Wenyih F. Lai
IPC分类号： B01J29/40
CPC分类号： B01J29/40 , B01J29/70 , B01J29/90 , B01J38/10 , C07C5/2737 , C07C2529/40 , C07C2529/70 , Y02P20/52 , Y02P20/584 , C07C15/08
摘要： The invention concerns a xylenes isomerization process for the production of equilibrium or near-equilibrium xylenes. The process utilizes a catalyst comprising HZSM-5 or MCM-49 and process conditions including a temperature of less than 295° C. and a pressure sufficient to maintain the xylenes in liquid phase. In embodiments, the process can be operated in a continuous mode with ppm levels of dissolved H2 in the feed and in other embodiments in a cyclic mode without the H2 in feed but with periodic regenerations using a feed having low ppm levels of H2.
摘要翻译：本发明涉及用于产生平衡或近平衡二甲苯的二甲苯异构化方法。该方法使用包含HZSM-5或MCM-49的催化剂和包括低于295℃的温度和足以将二甲苯保持在液相中的压力的工艺条件。在实施方案中，该方法可以以进料中的ppm水平的溶解的H 2在进料中以及在其它实施方案中以循环模式操作，而不使用进料中的H 2，而是使用具有低ppm水平的H 2的进料进行周期性再生。

4. 发明申请

US20150197465A1 Bimetallic Catalyst and Use in Xylene Production 有权
标题翻译：双金属催化剂和二甲苯生产中的应用
公开(公告)号：US20150197465A1
公开(公告)日：2015-07-16
申请号：US14669179
申请日：2015-03-26
申请人： ExxonMobil Chemical Patents Inc.
发明人： April D. Ross , Jane C. Cheng
IPC分类号： C07C5/27 , B01J29/44 , B01J37/08 , C07C7/148
CPC分类号： C07C5/2708 , B01J16/005 , B01J23/42 , B01J23/50 , B01J23/60 , B01J23/62 , B01J23/626 , B01J23/628 , B01J23/8926 , B01J29/405 , B01J29/44 , B01J29/46 , B01J37/0018 , B01J2229/186 , B01J2229/36 , B01J2229/42 , C07C5/222 , C07C5/2556 , C07C5/2737 , C07C5/2754 , C07C15/08 , C07C2529/44 , Y02P20/52
摘要： The invention is directed to a bimetallic catalyst system adapted for the manufacture of xylenes, a process for making said catalyst system, and to the process of manufacture of xylenes using said catalyst system, providing, in embodiments, improved selectivity by at least one of higher ethylene saturation and low xylene loss, decreased susceptibility to poisoning from feedstream impurities, and ability to operate at less severe conditions.
摘要翻译：本发明涉及适用于制造二甲苯的双金属催化剂体系，制备所述催化剂体系的方法，以及使用所述催化剂体系制备二甲苯的方法，在实施方案中，提供了至少一种较高的选择性乙烯饱和度低，二甲苯损失低，对原料杂质中毒的易感性降低，在恶劣条件下操作能力差。

5. 发明申请

US20130259775A1 Transalkylation Of Heavy Aromatic Hydrocarbon Feedstocks 有权
标题翻译：重芳香烃原料的烷基转移
公开(公告)号：US20130259775A1
公开(公告)日：2013-10-03
申请号：US13899854
申请日：2013-05-22
申请人： ExxonMobil Chemical Patents Inc.
发明人： Doron Levin , April D. Ross , James H. Beech, JR.
IPC分类号： B01J8/04
CPC分类号： B01J8/04 , B01J29/064 , B01J29/072 , B01J29/076 , B01J29/44 , B01J29/46 , B01J29/7034 , B01J29/7669 , B01J35/0006 , B01J35/023 , B01J37/0009 , B01J37/20 , B01J2229/42 , C07C6/12 , C07C2529/42 , Y02P20/52 , C07C15/08
摘要： In a process for producing xylene by transalkylation of a C9+ aromatic hydrocarbon feedstock with a C6 and/or C7 aromatic hydrocarbon, the C9+ aromatic hydrocarbon feedstock, at least one C6 and/or C7 aromatic hydrocarbon and hydrogen are contacted with a first catalyst comprising (i) a first molecular sieve having a Constraint Index in the range of about 3 to about 12 and (ii) at least first and second different metals or compounds thereof of Groups 6 to 12 of the Periodic Table of the Elements. Contacting with the first catalyst is conducted under conditions effective to dealkylate aromatic hydrocarbons in the feedstock containing C2+ alkyl groups and to saturate C2+ olefins formed so as to produce a first effluent. At least a portion of the first effluent is then contacted with a second catalyst comprising a second molecular sieve having a Constraint Index less than 3 under conditions effective to transalkylate C9+ aromatic hydrocarbons with said at least one C6-C7 aromatic hydrocarbon to form a second effluent comprising xylene.
摘要翻译：在通过C 9 +芳族烃原料与C 6和/或C 7芳烃的烷基转移生产二甲苯的方法中，C 9 +芳烃原料，至少一种C 6和/或C 7芳烃和氢与第一催化剂接触，所述第一催化剂包含（ i）具有在约3至约12范围内的约束指数的第一分子筛和（ii）至少元素周期表第6至12族的第一和第二不同金属或其化合物。与第一催化剂接触在有效地使含有C 2 +烷基的原料中芳族烃脱烷基化并使形成的C 2 +烯烃饱和以产生第一流出物的条件下进行。然后至少一部分第一流出物与包含第二分子筛的第二催化剂接触，该第二催化剂在有效使C 9+芳族烃与所述至少一种C 6 -C 7芳族烃烷基转移的条件下具有小于3的约束指数，以形成第二流出物包括二甲苯。

6. 发明授权

US09096484B1 Bimetallic catalyst and use in xylene production 有权
公开(公告)号：US09096484B1
公开(公告)日：2015-08-04
申请号：US14669179
申请日：2015-03-26
申请人： ExxonMobil Chemical Patents Inc.
发明人： April D. Ross , Jane C. Cheng
IPC分类号： C07C5/22 , C07C5/27 , C07C5/25 , C07C15/08
CPC分类号： C07C5/2708 , B01J16/005 , B01J23/42 , B01J23/50 , B01J23/60 , B01J23/62 , B01J23/626 , B01J23/628 , B01J23/8926 , B01J29/405 , B01J29/44 , B01J29/46 , B01J37/0018 , B01J2229/186 , B01J2229/36 , B01J2229/42 , C07C5/222 , C07C5/2556 , C07C5/2737 , C07C5/2754 , C07C15/08 , C07C2529/44 , Y02P20/52
摘要： The invention is directed to a bimetallic catalyst system adapted for the manufacture of xylenes, a process for making said catalyst system, and to the process of manufacture of xylenes using said catalyst system, providing, in embodiments, improved selectivity by at least one of higher ethylene saturation and low xylene loss, decreased susceptibility to poisoning from feedstream impurities, and ability to operate at less severe conditions.

7. 发明申请

US20130225891A1 Bimetallic Catalyst and Use in Xylene Production 有权
公开(公告)号：US20130225891A1
公开(公告)日：2013-08-29
申请号：US13747905
申请日：2013-01-23
申请人： ExxonMobil Chemical Patents Inc.
发明人： April D. Ross , Jane C. Cheng
IPC分类号： B01J16/00 , C07C5/27
CPC分类号： C07C5/2708 , B01J16/005 , B01J23/42 , B01J23/50 , B01J23/60 , B01J23/62 , B01J23/626 , B01J23/628 , B01J23/8926 , B01J29/405 , B01J29/44 , B01J29/46 , B01J37/0018 , B01J2229/186 , B01J2229/36 , B01J2229/42 , C07C5/222 , C07C5/2556 , C07C5/2737 , C07C5/2754 , C07C15/08 , C07C2529/44 , Y02P20/52
摘要： The invention is directed to a bimetallic catalyst system adapted for the manufacture of xylenes, a process for making said catalyst system, and to the process of manufacture of xylenes using said catalyst system, providing, in embodiments, improved selectivity by at least one of higher ethylene saturation and low xylene loss, decreased susceptibility to poisoning from feedstream impurities, and ability to operate at less severe conditions.

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