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1. 发明申请

US20150087869A1 CAPTURE OF TRIFLUOROMETHANE USING MOLECUAR SIEVES 审中-公开
标题翻译：使用分子量的三氟甲磺酸的捕获
公开(公告)号：US20150087869A1
公开(公告)日：2015-03-26
申请号：US14032208
申请日：2013-09-20
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： David Richard Corbin , Mark Brandon Shiflett
IPC分类号： B01D53/02 , C07C17/389
CPC分类号： C07C17/389 , B01D53/04 , B01D2253/102 , B01D2253/108 , B01D2253/116 , B01D2257/2066 , C07C17/206 , Y02P20/154 , Y02P20/40 , C07C19/08 , C07C19/10
摘要： A method for capturing trifluoromethane from a gaseous mixture in a vent stream from a chlorodifluoromethane manufacturing process is described. In the method, the gaseous mixture is contacted with a molecular sieve, such as a zeolite or activated carbon, having a pore opening of at least about 5 Angstroms and a Sanderson electronegativity of less than or equal to about 2.75. The method is useful for reducing emissions of trifluoromethane, which has a high global warming potential.
摘要翻译：描述了一种从氯二氟甲烷制造方法中排出的气体中的气体混合物中捕获三氟甲烷的方法。在该方法中，使气体混合物与分子筛（例如沸石或活性炭）接触，孔分布至少约5埃，桑德森电负性小于或等于约2.75。该方法对于减少具有高全球变暖潜能的三氟甲烷的排放是有用的。

2. 发明申请

US20130172584A1 PROCESS FOR THE PRODUCTION OF FURFURAL 有权
标题翻译：生产过程的过程
公开(公告)号：US20130172584A1
公开(公告)日：2013-07-04
申请号：US13729480
申请日：2012-12-28
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： David Richard Corbin , Paul Joseph Fagan , Ronnie Ozer , Bhuma Rajagopalan , Eric J. Till
IPC分类号： C07D307/50
CPC分类号： C07D307/50
摘要： Furfural is produced by mixing an aqueous feedstock solution containing C5 sugar and/or C6 sugar with a heated high boiling, water-miscible solvent, such as sulfolane, and a solid acid catalyst. Furfural product and water can be distilled off, leaving non-volatile solvent behind. Furfural yields of over 70% at as high as 99% conversion have been obtained with this process with sulfolane as the reaction solvent and zeolite beta as the solid acid catalyst. Also, certain by-products (e.g., humins) solubilized in the reaction solvent can be precipitated by addition of water or aqueous feedstock solution and then removed by filtration, thereby providing a convenient and effective way of removing these undesirable byproducts from the reaction mixture.
摘要翻译：通过将含有C5糖和/或C6糖的水性原料溶液与加热的高沸点，水混溶性溶剂如环丁砜和固体酸催化剂混合来制备糠醛。糠醛产品和水可以蒸馏出来，留下非挥发性溶剂。用环丁砜作为反应溶剂和沸石β作为固体酸催化剂，该方法已经获得高达99％转化率的糠醛产率超过70％。此外，溶解在反应溶剂中的某些副产物（例如，胡氏体）可以通过加入水或原料溶液沉淀，然后通过过滤除去，从而提供从反应混合物中除去这些不期望的副产物的方便有效的方法。

3. 发明授权

US09670118B2 Production of alpha, omega-diols 有权
公开(公告)号：US09670118B2
公开(公告)日：2017-06-06
申请号：US14877507
申请日：2015-10-07
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： Alan Martin Allgeier , Torren Ryan Carlson , David Richard Corbin , Wathudura Indika Namal De Silva , Carl Andrew Menning , Joachim C Ritter , Sourav Kumar Sengupta
IPC分类号： C07C29/132 , C07C29/60 , C07C209/16
CPC分类号： C07C29/132 , C07C29/60 , C07C209/16 , C07C31/20 , C07C211/12
摘要： Disclosed herein are processes for preparing an α,ω-Cn-diol, wherein n is 5 or greater, from a feedstock comprising a Cn oxygenate. In one embodiment, the process comprises contacting the feedstock with hydrogen gas in the presence of a catalyst comprising Pt, Cu, Ni, Pd, Pt, Rh, Ir, Ru, or Fe on a WO3 or WOx support. In one embodiment, the process comprises contacting the feedstock with hydrogen in the presence of a catalyst comprising a metal M1 and a metal M2 or an oxide of M2, and optionally a support. In one embodiment, M1 is Pd, Pt, or Ir; and M2 is Mo, W, V, Mn, Re, Zr, Ni, Cu, Zn, Cr, Ge, Sn, Ti, Au, or Co. The Cn oxygenate may be obtained from a biorenewable resource.

4. 发明授权

US09012664B2 Process for the production of furfural 有权
标题翻译：糠醛生产工艺
公开(公告)号：US09012664B2
公开(公告)日：2015-04-21
申请号：US13729445
申请日：2012-12-28
申请人： E I du Pont de Nemours and Company
发明人： David Richard Corbin , Paul Joseph Fagan , Stuart B Fergusson , Keith W Hutchenson , Pranit S Metkar , Ronnie Ozer , Carmo Joseph Pereira , Bhuma Rajagopalan , Sourav Kumar Sengupta , Eric J. Till
IPC分类号： C07D307/48 , C07D307/50
CPC分类号： C07D307/50 , C07D307/48 , Y02P20/127
摘要： Furfural is produced by contacting a feedstock solution containing C5 sugar and/or C6 sugar with a solid acid catalyst using reactive distillation. Both high yield and high conversion are obtained, without production of insoluble char in the reaction vessel. Degradation of furfural is minimized by its low residence time in contact with the solid acid catalyst. Higher catalyst lifetime can be achieved because the catalyst is continually washed with the refluxing aqueous solution and not sitting in high-boiling byproducts like humins, which are known to be deleterious to catalyst lifetime.
摘要翻译：通过使用反应蒸馏将含有C5糖和/或C6糖的原料溶液与固体酸催化剂接触来制备糠醛。获得高产率和高转化率，而在反应容器中不产生不溶性焦炭。通过其与固体酸催化剂接触的低停留时间使糠醛的降解最小化。可以实现更高的催化剂寿命，因为催化剂连续地用回流水溶液洗涤，而不是位于已知对催化剂寿命有害的高沸点副产物如胡氏。

5. 发明申请

US20150110710A1 PROCESS FOR PREPARING POWDER WITH ENHANCED BULK HANDLING PROPERTY 审中-公开
标题翻译：具有增强散货处理性能的粉末制备方法
公开(公告)号：US20150110710A1
公开(公告)日：2015-04-23
申请号：US14396397
申请日：2013-03-29
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： Timothy Allan Bell , David Richard Corbin , Scott Hutchison , Eugene Michael Mccarron, III , Thomas G. Calvarese
IPC分类号： C01G23/08 , C09C1/36
CPC分类号： C01G23/08 , C01P2006/10 , C01P2006/12 , C01P2006/19 , C09C1/36 , C09C1/3653 , C09C1/3669
摘要： The present invention relates to a process for manufacturing low-dusting, smoothly-discharging, easily dispersible, powders such as pigmentary titanium dioxide that resist compaction, aging, lumping, and/or caking. Particularly, the present invention relates to a process for treating powders such as pigmentary titanium dioxide with ammonia or a similarly basic substance prior to or during agglomeration to produce a powder with improved bulk handling properties.
摘要翻译：本发明涉及一种制造低粉尘，平滑排放，容易分散的粉末的方法，例如可以压实，老化，结块和/或结块的颜料二氧化钛。特别地，本发明涉及一种在凝聚之前或期间用氨或类似碱性物质处理粉末的颜料二氧化钛的方法，以产生具有改进的散装处理性能的粉末。

6. 发明申请

US20130181676A1 COMPOSITIONS, ELECTRODES AND METHODS OF MAKING 审中-公开
标题翻译：组合物，电极和制备方法
公开(公告)号：US20130181676A1
公开(公告)日：2013-07-18
申请号：US13743692
申请日：2013-01-17
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： Kostantinos Kourtakis , David Richard Corbin
IPC分类号： H01M4/133 , H01M10/44
CPC分类号： H01M4/133 , C04B38/08 , C04B2111/00853 , H01M4/13 , H01M4/139 , H01M4/362 , H01M10/052 , H01M10/44 , C04B26/02
摘要： There is a composition including polymeric binder and carbon-sulfur (C—S) composite. The C—S composite includes about 5 to 95 wt. % sulfur compound. The C—S composite also includes templated carbon having a surface area of about 50 to 4,000 square meters per gram templated carbon and a pore volume of about 0.5 to 6 cubic centimeters per gram templated carbon. The templated carbon has a carbon microstructure that is complementary with an inorganic microstructure, characterized by a three-dimensional framework, of an inorganic template used in a process for making the templated carbon. There is a method for making the composition. There is also an electrode incorporating the composition, as well as methods for making the electrode. There are also methods relating to using the composition and the electrode.
摘要翻译：存在包括聚合物粘合剂和碳 - 硫（C-S）复合材料的组合物。 C-S复合物包括约5至95wt。％硫化合物。 C-S复合材料还包括模板碳，其表面积为约50至4,000平方米/克模板碳，孔体积为约0.5至6立方厘米/克模板碳。模板碳具有与用于制备模板碳的方法中使用的无机模板的三维骨架的无机微结构互补的碳微结构。有一种制作组合物的方法。还有一种掺入该组合物的电极，以及制造电极的方法。还有关于使用组合物和电极的方法。

7. 发明申请

US20130172583A1 PROCESS FOR THE PRODUCTION OF FURFURAL 有权
公开(公告)号：US20130172583A1
公开(公告)日：2013-07-04
申请号：US13729445
申请日：2012-12-28
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： David Richard Corbin , Paul Joseph Fagan , Stuart B. Fergusson , Keith W. Hutchenson , Michael Stephen McKinnon , Ronnie Ozer , Bhuma Rajagopalan , Sourav Kumar Sengupta , Eric J. Till
IPC分类号： C07D307/48
CPC分类号： C07D307/50 , C07D307/48 , Y02P20/127
摘要： Furfural is produced by contacting a feedstock solution containing C5 sugar and/or C6 sugar with a solid acid catalyst using reactive distillation. Both high yield and high conversion are obtained, without production of insoluble char in the reaction vessel. Degradation of furfural is minimized by its low residence time in contact with the solid acid catalyst. Higher catalyst lifetime can be achieved because the catalyst is continually washed with the refluxing aqueous solution and not sitting in high-boiling byproducts like humins, which are known to be deleterious to catalyst lifetime.

8. 发明授权

US09181211B2 Process for the production of furfural 有权
标题翻译：糠醛生产工艺
公开(公告)号：US09181211B2
公开(公告)日：2015-11-10
申请号：US13729480
申请日：2012-12-28
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： David Richard Corbin , Paul Joseph Fagan , Ronnie Ozer , Bhuma Rajagopalan , Eric J. Till
IPC分类号： C07D311/92 , C07D307/50
CPC分类号： C07D307/50
摘要： Furfural is produced by mixing an aqueous feedstock solution containing C5 sugar and/or C6 sugar with a heated high boiling, water-miscible solvent, such as sulfolane, and a solid acid catalyst. Furfural product and water can be distilled off, leaving non-volatile solvent behind. Furfural yields of over 70% at as high as 99% conversion have been obtained with this process with sulfolane as the reaction solvent and zeolite beta as the solid acid catalyst. Also, certain by-products (e.g., humins) solubilized in the reaction solvent can be precipitated by addition of water or aqueous feedstock solution and then removed by filtration, thereby providing a convenient and effective way of removing these undesirable byproducts from the reaction mixture.
摘要翻译：通过将含有C5糖和/或C6糖的水性原料溶液与加热的高沸点，水混溶性溶剂如环丁砜和固体酸催化剂混合来制备糠醛。糠醛产品和水可以蒸馏出来，留下非挥发性溶剂。用环丁砜作为反应溶剂和沸石β作为固体酸催化剂，该方法已经获得高达99％转化率的糠醛产率超过70％。此外，溶解在反应溶剂中的某些副产物（例如，胡氏体）可以通过加入水或原料溶液沉淀，然后通过过滤除去，从而提供从反应混合物中除去这些不期望的副产物的方便有效的方法。

9. 发明授权

US09181157B2 Production of alpha, omega-diols 有权
公开(公告)号：US09181157B2
公开(公告)日：2015-11-10
申请号：US14568307
申请日：2014-12-12
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： Alan Martin Allgeier , Torren Ryan Carlson , David Richard Corbin , Wathudura Indika Namal De Silva , Ekaterini Korovessi , Carl Andrew Menning , Joachim C Ritter , Sourav Kumar Sengupta
IPC分类号： C07C29/60 , C07C29/132 , C07C209/16
CPC分类号： C07C29/132 , C07C29/60 , C07C209/16 , C07C31/20 , C07C211/12
摘要： Disclosed herein are processes for preparing an α,ω-Cn-diol, wherein n is 5 or greater, from a feedstock comprising a Cn oxygenate. In one embodiment, the process comprises contacting the feedstock with hydrogen gas in the presence of a catalyst comprising Pt, Cu, Ni, Pd, Pt, Rh, Ir, Ru, or Fe on a WO3 or WOx support. In one embodiment, the process comprises contacting the feedstock with hydrogen in the presence of a catalyst comprising a metal M1 and a metal M2 or an oxide of M2, and optionally a support. In one embodiment, M1 is Pd, Pt, or Ir; and M2 is Mo, W, V, Mn, Re, Zr, Ni, Cu, Zn, Cr, Ge, Sn, Ti, Au, or Co. The Cn oxygenate may be obtained from a biorenewable resource.

10. 发明授权

US09018423B2 Production of alpha, omega-diols 有权
标题翻译：生产α，ω-二醇
公开(公告)号：US09018423B2
公开(公告)日：2015-04-28
申请号：US13870066
申请日：2013-04-25
申请人： E I du Pont de Nemours and Company
发明人： Alan Martin Allgeier , Torren Ryan Carlson , David Richard Corbin , Wathudura Indika Namal De Silva , Ekaterini Korovessi , Carl Andrew Menning , Joachim C Ritter , H David Rosenfeld , Sourav Kumar Sengupta
IPC分类号： C07C29/60 , C07C209/16 , C07C29/132
CPC分类号： C07C29/132 , C07C29/60 , C07C209/16 , C07C31/20 , C07C211/12
摘要： Disclosed herein are processes for preparing an α,ω-Cn-diol, wherein n is 5 or greater, from a feedstock comprising a Cn oxygenate. In one embodiment, the process comprises contacting the feedstock with hydrogen gas in the presence of a catalyst comprising Pt, Cu, Ni, Pd, Pt, Rh, Ir, Ru, or Fe on a WO3 or WOx support. In one embodiment, the process comprises contacting the feedstock with hydrogen in the presence of a catalyst comprising a metal M1 and a metal M2 or an oxide of M2, and optionally a support. In one embodiment, M1 is Pd, Pt, or Ir; and M2 is Mo, W, V, Mn, Re, Zr, Ni, Cu, Zn, Cr, Ge, Sn, Ti, Au, or Co. The Cn oxygenate may be obtained from a biorenewable resource.
摘要翻译：本文公开了从包含Cn含氧化合物的原料制备其中n为5或更大的α，ω-Cn-二醇的方法。在一个实施方案中，该方法包括在WO 3或WO x载体上，在包含Pt，Cu，Ni，Pd，Pt，Rh，Ir，Ru或Fe的催化剂存在下使原料与氢气接触。在一个实施方案中，该方法包括在包含金属M1和金属M2或M2的氧化物和任选的载体的催化剂存在下使原料与氢接触。在一个实施方案中，M1是Pd，Pt或Ir; 并且M2是Mo，W，V，Mn，Re，Zr，Ni，Cu，Zn，Cr，Ge，Sn，Ti，Au或Co.Cn含氧化合物可以从生物可再生资源获得。

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