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1. 发明授权

US4937376A Process for producing N-phosphonomethylglycine 失效
公开(公告)号：US4937376A
公开(公告)日：1990-06-26
申请号：US356484
申请日：1989-05-25
申请人： Donald L. Fields, Jr. , Raymond C. Grabiak , Dennis P. Riley
发明人： Donald L. Fields, Jr. , Raymond C. Grabiak , Dennis P. Riley
IPC分类号： B01J27/053 , B01J27/08 , B01J27/128 , B01J27/24 , B01J27/25 , B01J31/02 , B01J31/04 , B01J31/22 , B01J31/26 , C07B61/00 , C07F9/38 , C07F9/40
CPC分类号： C07F9/3813
摘要： A process for the production of N-phosphonomethylglycine comprising contacting N-phosphonomethyliminoacetic acid with a molecular oxygen-containing gas in the presence of a catalyst selected from the group consisting of the salts and salt complexes of manganese, cobalt, iron, nickel, chromium, ruthenium, aluminum, molybdenum, vanadium and cerium, and an effective amount of a quinone or hydroquinone.

2. 发明授权

US4889906A Amine salts of 1,4,2-oxazaphospholidine-4-acetic acid, 2-alkoxy-2-oxides 失效
标题翻译： 1,4-二氧杂磷杂环丁烷-4-乙酸，2-烷氧基-2-氧化物的胺盐
公开(公告)号：US4889906A
公开(公告)日：1989-12-26
申请号：US276009
申请日：1988-11-25
申请人： Donald L. Fields, Jr. , Raymond C. Grabiak
发明人： Donald L. Fields, Jr. , Raymond C. Grabiak
IPC分类号： A01N57/36 , C07F9/6584
CPC分类号： A01N57/36 , C07F9/6584
摘要： The compounds 1,4,2-oxazaphospholidine-4-acetic acid, 2-alkoxy-2-oxides and their trialkylamine salts represented by the formula ##STR1## wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are individually selected from the group consisting of alkyl having from one to about four carbon atoms are useful as post emergent, selective herbicides and plant growth regulators.

3. 发明授权

US4952723A Process for producing N-phosphonomethylglycine 失效
标题翻译： N-膦酰基甲基甘氨酸的制备方法
公开(公告)号：US4952723A
公开(公告)日：1990-08-28
申请号：US386738
申请日：1989-07-31
申请人： Donald L. Fields, Jr. , Raymond C. Grabiak , Dennis P. Riley
发明人： Donald L. Fields, Jr. , Raymond C. Grabiak , Dennis P. Riley
IPC分类号： B01J27/053 , B01J27/08 , B01J27/128 , B01J27/24 , B01J27/25 , B01J31/02 , B01J31/04 , B01J31/22 , B01J31/26 , C07B61/00 , C07F9/38 , C07F9/40
CPC分类号： C07F9/3813
摘要： A process for the production of N-phosphonomethylglycine comprising contacting N-phosphonomethyliminodiacetic acid with a molecular oxygen-containing gas in the presence of a catalyst selected from the group consisting of the salts and salt complexes of manganese, cobalt, iron, nickel, chromium, ruthenium, aluminum, moleybdenum, vanadium and cerium, and an effective amount of a dipyridyl compound.

4. 发明授权

US5072033A Process for producing N-phosphonomethylglycine 失效
公开(公告)号：US5072033A
公开(公告)日：1991-12-10
申请号：US625342
申请日：1990-12-11
申请人： Donald L. Fields, Jr. , Raymond C. Grabiak , Karl E. Koenig , Dennis P. Riley
发明人： Donald L. Fields, Jr. , Raymond C. Grabiak , Karl E. Koenig , Dennis P. Riley
IPC分类号： B01J27/053 , B01J27/08 , B01J27/128 , B01J31/04 , C07B61/00 , C07F9/38
CPC分类号： C07F9/3813
摘要： A process for the production of N-phosphonomethylglycine comprising contacting N-phosphonomethyliminodiacetic acid with a peroxide in the presence of a catalyst selected from the group consisting of the salts and salt complexes of cobalt and vanadium, and an effective amount of a quinone or hydroquinone.

5. 发明授权

US5061820A Process for producing N-phosphonomethylgylcine 失效
标题翻译： N-膦酰基甲基甘氨酸的制备方法
公开(公告)号：US5061820A
公开(公告)日：1991-10-29
申请号：US600954
申请日：1990-10-22
申请人： Donald L. Fields, Jr. , Raymond C. Grabiak , Karl E. Koenig , Dennis P. Riley
发明人： Donald L. Fields, Jr. , Raymond C. Grabiak , Karl E. Koenig , Dennis P. Riley
IPC分类号： B01J27/053 , B01J27/08 , B01J27/25 , B01J31/04 , C07B61/00 , C07F9/38
CPC分类号： C07F9/3813
摘要： A process for the production of N-phosphonomethylglycine comprising contacting N-phosphonomethyliminodiacetic acid with a peroxide in the presence of a catalyst selected from the group consisting of the salts and salt complexes of cobalt and vancadium, and an effective amount of dipyridyl compound.

6. 发明授权

US4898972A Process for producing N-phosphonomethylglycine 失效
公开(公告)号：US4898972A
公开(公告)日：1990-02-06
申请号：US248663
申请日：1988-09-26
申请人： Donald L. Fields, Jr. , Raymond C. Grabiak , Dennis P. Riley
发明人： Donald L. Fields, Jr. , Raymond C. Grabiak , Dennis P. Riley
IPC分类号： B01J27/06 , B01J27/128 , C07B61/00 , C07F9/38
CPC分类号： C07F9/3813
摘要： N-phosphonomethylglycine can be produced by contacting N-phosphonomethyliminodiacetic acid with a molecular oxygen-containing gas in the presence of an effective amount of a catalyst selected from the group consisting of the salts and salt complexes of manganese and cobalt, and an effective amount of bromide ion.

7. 发明授权

US5077430A Peroxide process for producing N-phosphonomethylglycine 失效
标题翻译：过氧化物生产N-膦酰基甲基甘氨酸的方法
公开(公告)号：US5077430A
公开(公告)日：1991-12-31
申请号：US684751
申请日：1991-04-15
申请人： Donald L. Fields, Jr.
发明人： Donald L. Fields, Jr.
IPC分类号： C07F9/38
CPC分类号： C07F9/3813
摘要： A process is provided for producing N-phosphonomethylglycine by the oxidation of N-phosphonomethyliminodiacetic acid with a peroxide to form an intermediate N-phosphonomethyliminodiacetic acid-N-oxide. Thereafter, the N-phosphonomethyliminodiacetic acid-N-oxide is converted to N-phosphonomethylglycine by adding a catalytic amount of a metal selected from the group consisting of iron, zinc, aluminum, vanadium and copper, or a compound selected from the group consisting of water-soluble vanadium compounds, ferrous salts and cuprous salts.
摘要翻译：提供了通过用过氧化物氧化N-膦酰基甲基亚氨基二乙酸以形成中间体N-膦酰甲基亚氨基二乙酸-N-氧化物来生产N-膦酰基甲基甘氨酸的方法。此后，通过添加催化量的选自铁，锌，铝，钒和铜的金属或选自下组的化合物，将N-膦酰基甲基亚氨基二乙酸-N-氧化物转化成N-膦酰基甲基甘氨酸：水溶性钒化合物，亚铁盐和亚铜盐。

8. 发明授权

US5047579A Process for producing n-phosphonomethylglycine 失效
标题翻译：生产正膦酰基甲基甘氨酸的方法
公开(公告)号：US5047579A
公开(公告)日：1991-09-10
申请号：US543002
申请日：1990-06-25
申请人： Jozef G. Glowka , Kai K. Lau , Henryk Krawczyk , Donald L. Fields, Jr.
发明人： Jozef G. Glowka , Kai K. Lau , Henryk Krawczyk , Donald L. Fields, Jr.
IPC分类号： C07F9/38
CPC分类号： C07F9/3813
摘要： An improved process is disclosed for the preparation of N-phosphonomethylglycine by the oxidation of N-phosphonomethyliminodiacetic acid. In the process N-phosphonomethyliminodiacetic acid is oxidized with a peroxide to form an intermediate, N-phosphonomethyliminodiacetic acid-N-oxide, and thereafter, adding a metabisulfite compound in the presence of a molybdenum compound to convert the intermediate to N-phosphonomethylglycine.
摘要翻译：公开了通过N-膦酰甲基亚氨基二乙酸的氧化制备N-膦酰基甲基甘氨酸的改进方法。在该方法中，N-膦酰甲基亚氨基二乙酸用过氧化物氧化形成中间体N-膦酰甲基亚氨基二乙酸-N-氧化物，然后在钼化合物的存在下加入偏亚硫酸氢盐化合物，将中间体转化为N-膦酰基甲基甘氨酸。

9. 发明授权

US06184385B2 Process for the manufacture of a sulfenimide 有权
标题翻译：制备亚硫酰亚胺的方法
公开(公告)号：US06184385B2
公开(公告)日：2001-02-06
申请号：US09292682
申请日：1999-04-16
申请人： Jayant S. Lodaya , Donald L. Fields, Jr. , Raymond T. Parker , Phillip B. Balderson
发明人： Jayant S. Lodaya , Donald L. Fields, Jr. , Raymond T. Parker , Phillip B. Balderson
IPC分类号： C07D41712
CPC分类号： C07D277/80
摘要： A process for the manufacture of a sulfenimide by reacting sulfenamide in slurry with a water immiscible organic solvent with an acid to yield a solvent slurry comprising sulfenimide product. The product is recovered from the solvent slurry by a method comprising the addition of water to the solvent slurry and the isolating of the product by a single filtration step. While water is added to the solvent slurry an azeotrope of solvent and water may be distilled under vacuum until substantially all solvent is separated from product and product becomes part of an aqueous slurry. Alternatively, water may be added to the solvent slurry while the resulting mixture is being agitated, followed by filtering the mixture in the single filtration step for recovery of product from the mixture.
摘要翻译：通过使浆料中的次磺酰胺与与水不混溶的有机溶剂与酸反应制备亚磺酰亚胺的方法，以产生包含亚硫酰亚胺产物的溶剂浆料。通过包括向溶剂浆料中加入水并通过单一过滤步骤分离产物的方法从溶剂浆料中回收产物。当将水加入到溶剂浆料中时，溶剂和水的共沸物可以在真空下蒸馏，直到基本上所有溶剂与产物分离，并且产物成为含水浆料的一部分。或者，可以在搅拌所得混合物的同时将水加入到溶剂淤浆中，然后在单过滤步骤中过滤混合物以从混合物中回收产物。

10. 发明授权

US5023369A Process for producing N-phosphonomethylglycine 失效
标题翻译： N-膦酰基甲基甘氨酸的制备方法
公开(公告)号：US5023369A
公开(公告)日：1991-06-11
申请号：US543016
申请日：1990-06-25
申请人： Donald L. Fields, Jr.
发明人： Donald L. Fields, Jr.
IPC分类号： B01J23/30 , C07B61/00 , C07F9/38
CPC分类号： C07F9/3813
摘要： A process is provided to produce N-phosphonomethylglycine by the oxidation of N-phosphonomethyliminodiacetic acid to form an intermediate N-phosphonomethyliminodiacetic acid-N-oxide with a peroxide in the presence of an effective amount of a catalyst selected from the group consisting of water-soluble tungsten compounds and a mixture of water-soluble tungsten compounds and a water-soluble molybdenum compound to form the intermediate, and thereafter converting the intermediate N-phosphonomethyliminodiacetic acid-N-oxide to N-phosphonomethylglycine.

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