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1. 发明授权

US4740583A Method for converting cyclic polycarbonate oligomer mixtures to linear polycarbonate, and composition resulting therefrom 失效
标题翻译：将环状聚碳酸酯低聚物混合物转化为线性聚碳酸酯的方法，以及由其制得的组合物
公开(公告)号：US4740583A
公开(公告)日：1988-04-26
申请号：US888673
申请日：1986-07-24
申请人： Daniel J. Brunelle , Thomas L. Evans , Michael A. Vallance , Kevin R. Stewart , Thomas G. Shannon , David A. Williams , Dwight J. Patterson , Niles R. Rosenquist , William Hilakos
发明人： Daniel J. Brunelle , Thomas L. Evans , Michael A. Vallance , Kevin R. Stewart , Thomas G. Shannon , David A. Williams , Dwight J. Patterson , Niles R. Rosenquist , William Hilakos
IPC分类号： C08G64/20 , C08G64/26 , C08G64/30 , C08G75/28 , C08J5/04 , C08K7/02 , C08G63/62
CPC分类号： C08G64/26 , C08G64/30 , C08G75/28 , C08J5/04 , C08K7/02 , C08J2369/00
摘要： Cyclic polycarbonate (or thiol analog) oligomer mixtures are prepared by the reaction of bishaloformates or their thio analogs, or mixtures thereof with dihydroxy or dimercapto compounds, with alkali metal hydroxides and various amines. The oligomer mixtures may be converted to polycarbonates or their thiol analogs by a method which is particularly adaptable to integration with polycarbonate processing operations. Polymerization may be conducted simultaneously with molding, extrusion and the like. The oligomer mixtures are adaptable to the preparation of filled prepregs.
摘要翻译：通过双卤代甲酸酯或其硫代类似物或其与二羟基或二巯基化合物的混合物与碱金属氢氧化物和各种胺的反应制备环状聚碳酸酯（或硫醇类似物）低聚物混合物。低聚物混合物可以通过特别适用于与聚碳酸酯加工操作整合的方法转化为聚碳酸酯或其硫醇类似物。聚合可以与成型，挤出等同时进行。低聚物混合物适用于填充的预浸料的制备。

2. 发明授权

US4638077A Method for the preparation of chloroformate compositions 失效
标题翻译：氯甲酸酯组合物的制备方法
公开(公告)号：US4638077A
公开(公告)日：1987-01-20
申请号：US790909
申请日：1985-10-24
申请人： Daniel J. Brunelle , Thomas G. Shannon , Niles R. Rosenquist
发明人： Daniel J. Brunelle , Thomas G. Shannon , Niles R. Rosenquist
IPC分类号： C07C68/02 , C01B31/24
CPC分类号： C07C68/02
摘要： Chloroformate compositions, particularly bischloroformate compositions, are prepared by the reaction of phosgene with a hydroxy compound, preferably a dihydroxy compound such as bisphenol A, in a heterogeneous mixture, while adding a hydrogen chloride scavenger comprising aqueous base as necessary and maintaining a pH of 0.5-8 during the phosgene addition. When a polyhydroxy compound is employed and the temperature is above 30.degree. C., the phosgene addition rate is maintained at a level high enough to effect rapid and complete reaction with dissolved hydroxy compound. This method uses substantially less phosgene than methods involving a higher pH.
摘要翻译：氯甲酸酯组合物，特别是双氯甲酸酯组合物，通过光气与羟基化合物，优选二羟基化合物如双酚A在非均相混合物中的反应制备，同时根据需要加入包含碱水溶液的氯化氢清除剂并保持pH为0.5 -8在光气加成期间。当使用多羟基化合物并且温度高于30℃时，光气加入速率保持在足够高的水平以便与溶解的羟基化合物进行快速和完全的反应。该方法比涉及较高pH的方法使用的光气明显较少。

3. 发明授权

US4636559A Bis(cyclic carbonates), precursors thereof, and polycarbonate compositions containing them 失效
标题翻译：双（环状碳酸酯），其前体和含有它们的聚碳酸酯组合物
公开(公告)号：US4636559A
公开(公告)日：1987-01-13
申请号：US744074
申请日：1985-06-12
申请人： Niles R. Rosenquist , Thomas L. Evans
发明人： Niles R. Rosenquist , Thomas L. Evans
IPC分类号： C08G63/00 , C08G64/00 , C08G64/06 , C08K5/156 , C08G63/62
CPC分类号： C08G64/06 , C08K5/156
摘要： Novel bis(cyclic carbonates) are useful as cross-linking agents for polycarbonate compositions (including cyclic polycarbonate oligomers), and, in combination with flame retardant agents, as anti-drip agents for polycarbonate resins. This bis(cyclic carbonates) may be prepared by the reaction of phosgene with novel tetraphenols, which in turn may be prepared by the condensation of aliphatic dialdehydes with phenols.
摘要翻译：新型双（环状碳酸酯）可用作聚碳酸酯组合物（包括环状聚碳酸酯低聚物）的交联剂，并且与阻燃剂组合用作聚碳酸酯树脂的防滴落剂。这种双（环状碳酸酯）可以通过光气与新型四酚的反应来制备，其又可以通过脂族二醛与酚的缩合来制备。

4. 发明授权

US4746725A Cyclic polycarbonate-polyepoxide reaction product and method for their preparation 失效
标题翻译：环状聚碳酸酯 - 聚环氧化物反应产物及其制备方法
公开(公告)号：US4746725A
公开(公告)日：1988-05-24
申请号：US19153
申请日：1987-02-25
申请人： Thomas L. Evans , Niles R. Rosenquist , Edgar E. Bostick
发明人： Thomas L. Evans , Niles R. Rosenquist , Edgar E. Bostick
IPC分类号： C08L69/00 , C08G59/00 , C08G59/40 , C08G64/30 , C08L63/00 , C08G63/62
CPC分类号： C08G64/30
摘要： Resinous compositions are prepared by the reaction of a composition comprising cyclic polycarbonate oligomers with at least one polyepoxide compound, in the presence of a polycarbonate formation catalyst. The cyclic polycarbonate oligomer composition is preferably a mixture of oligomers of varying degrees of polymerization, and the polyepoxy compound is preferably triglycidyl isocyanurate or a bis-epoxy-terminated bisphenol A-epichlorohydrin concentrate. There may also be present a polycarbonate crosslinking agent. The product of the reaction is a crosslinked polycarbonate network. The method is particularly useful in reactive processing operations such as reaction injection molding.

5. 发明授权

US5962558A High molecular weight stabilizer compounds for stabilizing polymers 失效
标题翻译：用于稳定聚合物的高分子量稳定剂化合物
公开(公告)号：US5962558A
公开(公告)日：1999-10-05
申请号：US105642
申请日：1998-06-26
申请人： Niles R. Rosenquist
发明人： Niles R. Rosenquist
IPC分类号： C08G64/06 , C07D249/20 , C08G63/64 , C08G64/00 , C08G64/12 , C08G64/14 , C08G64/20 , C08G64/42 , C08K5/3475 , C08L69/00 , C08K5/34
CPC分类号： C08G64/14 , C07D249/20 , C08G64/12 , C08G64/20 , C08G63/64
摘要： A high molecular weight stabilizer compound formed as an ester of 3-(2H-benzotriazol-2-yl)-5-(1,1-dimethylethyl)-4-hydroxy-benzene-propanoic acid, or structural variants thereof, to impart improved resistance to the effects of ultraviolet radiation to polycarbonate comprising polymers, a process for the preparation of said compound, and articles of manufacture comprising said compound.
摘要翻译：作为3-（2H-苯并三唑-2-基）-5-（1,1-二甲基乙基）-4-羟基 - 苯 - 丙酸的酯形成的高分子量稳定剂化合物或其结构变体，以改善耐紫外线对包含聚合物的聚碳酸酯的影响，制备所述化合物的方法和包含所述化合物的制品。

6. 发明授权

US5367044A Blow molded article molded from a composition comprising a randomly branched aromatic polymer 失效
标题翻译：由包含无规分支的芳族聚合物的组合物模制的吹塑制品
公开(公告)号：US5367044A
公开(公告)日：1994-11-22
申请号：US928075
申请日：1992-08-12
申请人： Niles R. Rosenquist
发明人： Niles R. Rosenquist
IPC分类号： C08G64/14 , C08G64/00
CPC分类号： C08G64/14
摘要： A composition comprising a randomly branched aromatic polycarbonate polymer wherein the branching agent 1,1,1-tris-(4-hydroxyphenol)ethane is present in the polymer in quantities ranging from about 0.28 to about 0.36 mole percent compound based on the percent of dihydric phenol present in the polymer.
摘要翻译：一种包含随机支化的芳族聚碳酸酯聚合物的组合物，其中支化剂1,1,1-三（4-羟基苯酚）乙烷以约0.28至约0.36摩尔％的量存在于聚合物中，基于二元的百分比苯酚存在于聚合物中。

7. 发明授权

US5081205A Preparation of cross-linked polycarbonate with cross-linker polycarbonate resin 失效
标题翻译：用交联聚碳酸酯树脂制备交联聚碳酸酯
公开(公告)号：US5081205A
公开(公告)日：1992-01-14
申请号：US542623
申请日：1990-06-25
申请人： Niles R. Rosenquist
发明人： Niles R. Rosenquist
IPC分类号： C08G64/14
CPC分类号： C08G64/14
摘要： A polycarbonate resin, containing in the polymer chain at least one divalent moiety of the formula: ##STR1## wherein E is selected from the group consisting of alkylene containing from 1 to 15 carbon atoms, inclusive, and halogen-substituted alkylene containing from 1 to 15 carbon atoms, inclusive, a is an integer of 0 or 1 and R' is hydrogen or hydrocarbyl or halogen substituted hydrocarbyl amenable to beta elimination upon thermal degradation.
摘要翻译：在聚合物链中含有下式的至少一个二价部分：（I）的聚碳酸酯树脂，其中E选自含有1至15个碳原子的亚烷基，和含有卤素取代的亚烷基 1至15个碳原子，包括端值，a为0或1的整数，R'为氢或烃基或卤素取代的烃基，可在热降解时进行β消除。

8. 发明授权

US5064914A Method of branching polyesters 失效
标题翻译：分支聚酯的方法
公开(公告)号：US5064914A
公开(公告)日：1991-11-12
申请号：US447492
申请日：1989-12-07
申请人： Niles R. Rosenquist , Edgar E. Bostick
发明人： Niles R. Rosenquist , Edgar E. Bostick
IPC分类号： B29C67/24 , C08G63/64 , C08G64/18
CPC分类号： B29C67/246 , C08G63/64 , C08G64/18
摘要： Linear polyester are branched by transesterification with resins having repeating or recurring polymer chain units of the formula: ##STR1## wherein m, n and p are each independent integers of 0 or 1; R represents hydrocarbyl; and E represents alkylene containing from 1 to 15 carbon atoms, inclusive, halogen- substituted alkylene of 1 to 15 carbon atoms, inclusive, alkylene of 1 to 15 carbon atoms, inclusive, substituted with a --COOR group where R is as previously defined, or alkylene having 1 to 15 carbon atoms substituted with a monovalent group of the formula: ##STR2## wherein X represents one of hydrogen, hydrocarbyl or ##STR3## wherein R is as defined above; provided there is at least one moiety present, containing an R group.
摘要翻译：线性聚酯通过与具有下式的重复或重复的聚合物链单元的树脂进行酯交换而支化：其中m，n和p各自独立的整数为0或1; R表示烃基; E表示含有1至15个碳原子的亚烷基，包括1至15个碳原子的卤素取代的亚烷基，包括1至15个碳原子的亚烷基，包括它们被-COOR基团取代，其中R如前所定义，或具有1至15个碳原子的亚烷基，其被下式的单价基团取代：其中X表示氢，烃基或者其中R如上定义; 条件是存在至少一个含有R基团的部分。

9. 发明授权

US4826928A Copolyester-carbonate resins having trimellitic acid units in the polymer backbone and their use as crosslinking or branching agents 失效
标题翻译：在聚合物主链中具有偏苯三酸单元的共聚酯 - 碳酸酯树脂及其作为交联剂或支链剂的用途
公开(公告)号：US4826928A
公开(公告)日：1989-05-02
申请号：US234789
申请日：1988-08-22
申请人： Niles R. Rosenquist
发明人： Niles R. Rosenquist
IPC分类号： C08G63/64
CPC分类号： C08G63/64
摘要： Thermoplastic copolyester-carbonate resins are described, having included in their polymer chains, a moiety of the formula: ##STR1## wherein a and b are each whole number integers of from 0 to 1; and the sum of a+b is 1.The resins are useful intermediates for branched or cross-linked molding compositions.
摘要翻译：描述了在其聚合物链中包含下式的部分的热塑性共聚酯 - 碳酸酯树脂：其中a和b各自的整数为0至1; 并且a + b的总和为1.树脂是支链或交联模塑组合物的有用的中间体。

10. 发明授权

US4778874A Composite produced by impregnating with cyclic carbonate oligomer and polymerizing 失效
标题翻译：通过用环状碳酸酯低聚物浸渍并聚合制得的复合材料
公开(公告)号：US4778874A
公开(公告)日：1988-10-18
申请号：US51804
申请日：1987-05-20
申请人： Niles R. Rosenquist
发明人： Niles R. Rosenquist
IPC分类号： C07D323/00 , C08G64/00 , C08G64/30 , C08G63/62 , B32B27/36
CPC分类号： C07D323/00 , C08G64/00 , C08G64/30 , Y10T428/31507
摘要： A composition comprising at least one oligomer of the formula ##STR1## wherein X is selected from the group consisting of alkylene of two to twelve carbon atoms, inclusive, alkylidene of one to twelve carbon atoms, inclusive, cycloalkylene of four to twelve carbon atoms, inclusive, cycloalkylidene of four to twelve carbon atoms, inclusive, ##STR2## a is zero or 1; n is an integer of one to about fifteen;R is alkylene of two to eight carbon atoms, inclusive, or alkylidene of one to eight carbon atoms, inclusive;R.sup.1 and R.sup.2 are the same or different and are alkyl or one to four carbon atoms, inclusive or halo;b and c are the same or different and are an integer of zero to four; andR.sup.3 and R.sup.4 are the same or different and are alkyl of one to eight carbon atoms, inclusive, or phenyl; andd and e are individually integers of 0.1 or 2 with the proviso that d & e is at least one.
摘要翻译：一种组合物，其包含至少一种式Ⅰ的低聚物，其中X选自2至12个碳原子的亚烷基，包括1至12个碳原子的亚烷基，包括4-12个碳的亚环烷基原子（包括），四至十二个碳原子的环烷叉基，包括α，a为零或1; n是1至约15的整数; R是2至8个碳原子的亚烷基，包括1或8个碳原子的亚烷基，包括1至8个碳原子的亚烷基; R1和R2相同或不同，为烷基或一至四个碳原子，包括或卤素; b和c相同或不同，为0〜4的整数。并且R 3和R 4相同或不同，为1-8个碳原子的烷基，或苯基; d和e分别为0.1或2的整数，条件是d＆e为至少一个。

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