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    • 5. 发明授权
    • Process for making dense thin films
    • 制造薄膜的工艺
    • US06921557B2
    • 2005-07-26
    • US10323137
    • 2002-12-18
    • Craig P. JacobsonSteven J. ViscoLutgard C. DeJonghe
    • Craig P. JacobsonSteven J. ViscoLutgard C. DeJonghe
    • B05D1/36B05D3/02H01M8/12
    • H01M8/1213H01M4/9066H01M8/1226H01M8/1246Y02E60/525Y02P70/56
    • Provided are low-cost, mechanically strong, highly electronically conductive porous substrates and associated structures for solid-state electrochemical devices, techniques for forming these structures, and devices incorporating the structures. The invention provides solid state electrochemical device substrates of novel composition and techniques for forming thin electrode/membrane/electrolyte coatings on the novel or more conventional substrates. In particular, in one embodiment the invention provides techniques for firing of device substrate to form densified electrolyte/membrane films 5 to 20 microns thick. In another embodiment, densified electrolyte/membrane films 5 to 20 microns thick may be formed on a pre-sintered substrate by a constrained sintering process. In some cases, the substrate may be a porous metal, alloy, or non-nickel cermet incorporating one or more of the transition metals Cr, Fe, Cu and Ag, or alloys thereof.
    • 提供了低成本,机械强度高的电子导电多孔基底和用于固态电化学装置的相关结构,用于形成这些结构的技术以及结合该结构的装置。 本发明提供了用于在新颖或更传统的基底上形成薄电极/膜/电解质涂层的新型组成和技术的固态电化学装置基板。 特别地,在一个实施例中,本发明提供了用于烧制器件衬底以形成5至20微米厚的致密化电解质/膜膜的技术。 在另一个实施方案中,可以通过约束烧结工艺在预烧结衬底上形成5至20微米厚的致密化电解质/膜膜。 在一些情况下,基底可以是包含一种或多种过渡金属Cr,Fe,Cu和Ag的多孔金属,合金或非镍金属陶瓷,或其合金。
    • 6. 发明授权
    • Method of making a layered composite electrode/electrolyte
    • 制备层状复合电极/电解质的方法
    • US06846511B2
    • 2005-01-25
    • US10724558
    • 2003-11-26
    • Steven J. ViscoCraig P. JacobsonLutgard C. DeJonghe
    • Steven J. ViscoCraig P. JacobsonLutgard C. DeJonghe
    • H01M4/86H01M4/88H01M8/12B05D5/12H01M6/00
    • H01M4/9066H01M4/8626H01M4/8885H01M8/1246H01M2004/8689H01M2008/1293Y02E60/525Y02P70/56Y10T29/49115
    • An electrode/electrolyte structure is prepared by a plurality of methods. An unsintered (possibly bisque fired) moderately catalytic electronically-conductive or homogeneous mixed ionic electronic conductive electrode material is deposited on a layer composed of a sintered or unsintered ionically-conductive electrolyte material prior to being sintered. A layer of particulate electrode material is deposited on an unsintered (“green”) layer of electrolyte material and the electrode and electrolyte layers are sintered simultaneously, sometimes referred to as “co-firing,” under conditions suitable to fully densify the electrolyte while the electrode retains porosity. Or, the layer of particulate electrode material is deposited on a previously sintered layer of electrolyte, and then sintered. Subsequently, a catalytic material is added to the electrode structure by infiltration of an electrolcatalyst precursor (e.g., a metal salt such as a transition metal nitrate). This may be followed by low temperature firing to convert the precursor to catalyst. The invention allows for an electrode with high electronic conductivity and sufficient catalytic activity to achieve high power density in an ionic (electrochemical) device such as fuel cells and electrolytic gas separation systems.
    • 通过多种方法制备电极/电解质结构。 在烧结之前,在由烧结或未烧结的离子导电电解质材料构成的层上沉积未烧结(可能是烧结的)中等催化的电子导电或均匀混合的离子电子导电电极材料。 一层颗粒状电极材料沉积在电解质材料的未烧结(“绿色”)层上,电极和电解质层同时烧结,有时也被称为“共烧结”,在适合于使电解质完全致密化的条件下 电极保留孔隙度。 或者,将粒状电极材料层沉积在预先烧结的电解质层上,然后烧结。 随后,通过电催化剂前体(例如金属盐如过渡金属硝酸盐)的渗透将催化材料加入到电极结构中。 然后可以进行低温烧制,将前体转化为催化剂。 本发明允许具有高电子导电性和足够的催化活性的电极在诸如燃料电池和电解气体分离系统的离子(电化学)装置中实现高功率密度。