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1. 发明授权

US5753766A Amphipathic graft copolymers and copolymer compositions and methods of making 失效
标题翻译：两亲性接枝共聚物和共聚物组合物和制备方法
公开(公告)号：US5753766A
公开(公告)日：1998-05-19
申请号：US844187
申请日：1997-04-18
申请人： Craig J. Bott , Dale M. Pickelman , Thomas E. Fisk
发明人： Craig J. Bott , Dale M. Pickelman , Thomas E. Fisk
IPC分类号： C08F291/00 , C08F290/04 , C08F290/08
CPC分类号： C08F291/00
摘要： The present invention provides amphipathic graft copolymers which comprises a hydrophobic polymer portion to which is grafted at least one amphipathic polymer portion containing pH independent ionic groups. The amphipathic graft copolymers can be prepared employing a procedure which comprises polymerizing at least two hydrophobic monomers, wherein at least one of the monomers is a graftable monomer, and at least one hydrophilic monomer, including at least one anionic and/or cationic pH independent ionic monomer, or a post reactive non-ionic monomer that can be converted to a pH independent ionic derivative, in a reaction medium and recovering the thus prepared amphipathic graft copolymer. Stable, substantially non-aqueous solution compositions of said amphipathic graft copolymer containing less than 15 percent by weight water are also provided. The present invention is also useful in preparing a substantially non-aqueous concentrate formulation of a non-ionic surfactant and an amphipathic graft copolymer composition in admixture with a water insoluble organic pesticide which concentrate formulation can be easily diluted with water to form non-settling, freeze-thaw stable formulations.
摘要翻译：本发明提供两亲性接枝共聚物，其包含疏水性聚合物部分，其中接枝至少一个含有pH独立离子基团的两亲性聚合物部分。两亲性接枝共聚物可以使用包括使至少两种疏水单体聚合的方法制备，其中至少一种单体是可接枝的单体，和至少一种亲水性单体，包括至少一种阴离子和/或阳离子的pH独立离子单体或可以转化为不依赖于pH的离子衍生物的后反应性非离子单体，并回收如此制备的两亲性接枝共聚物。还提供了含有小于15重量％水的所述两亲接枝共聚物的稳定的基本上非水溶液组合物。本发明还可用于制备非水性非离子表面活性剂的非水性浓缩物制剂和与水不溶性有机农药混合的两亲性接枝共聚物组合物，浓缩物制剂可以容易地用水稀释以形成非沉降，冻融稳定配方。

2. 发明授权

US5693716A Amphipathic graft copolymers and copolymer compositions and methods of making 失效
标题翻译：两亲性接枝共聚物和共聚物组合物和制备方法
公开(公告)号：US5693716A
公开(公告)日：1997-12-02
申请号：US560232
申请日：1995-11-21
申请人： Craig J. Bott , Dale M. Pickelman , Thomas E. Fisk
发明人： Craig J. Bott , Dale M. Pickelman , Thomas E. Fisk
IPC分类号： C08F291/00 , C08F290/04 , C08F290/08
CPC分类号： C08F291/00
摘要： The present invention provides amphipathic graft copolymers which comprises a hydrophobic polymer portion to which is grafted at least one amphipathic polymer portion containing pH independent ionic groups. The amphipathic graft copolymers can be prepared employing a procedure which comprises polymerizing at least two hydrophobic monomers, wherein at least one of the monomers is a graftable monomer, and at least one hydrophilic monomer, including at least one anionic and/or cationic pH independent ionic monomer, or a post reactive non-ionic monomer that can be converted to a pH independent ionic derivative, in a reaction medium and recovering the thus prepared amphipathic graft copolymer. Stable, substantially non-aqueous solution compositions of said amphipathic graft copolymer containing less than 15 percent by weight water are also provided. The present invention is also useful in preparing a substantially non-aqueous concentrate formulation of a non-ionic surfactant and an amphipathic graft copolymer composition in admixture with a water insoluble organic pesticide which concentrate formulation can be easily diluted with water to form non-settling, freeze-thaw stable formulations.
摘要翻译：本发明提供两亲性接枝共聚物，其包含疏水性聚合物部分，其中接枝至少一个含有pH独立离子基团的两亲性聚合物部分。两亲性接枝共聚物可以使用包括使至少两种疏水单体聚合的方法制备，其中至少一种单体是可接枝的单体，和至少一种亲水性单体，包括至少一种阴离子和/或阳离子的pH独立离子单体或可以转化为不依赖于pH的离子衍生物的后反应性非离子单体，并回收如此制备的两亲性接枝共聚物。还提供了含有小于15重量％水的所述两亲接枝共聚物的稳定的基本上非水溶液组合物。本发明还可用于制备非水性非离子表面活性剂的非水性浓缩物制剂和与水不溶性有机农药混合的两亲性接枝共聚物组合物，浓缩物制剂可以容易地用水稀释以形成非沉降，冻融稳定配方。

3. 发明申请

US20150021339A1 PASSIVATION, pH PROTECTIVE OR LUBRICITY COATING FOR PHARMACEUTICAL PACKAGE, COATING PROCESS AND APPARATUS 审中-公开
标题翻译：钝化，pH值保护或润滑涂料用于药物包装，涂装工艺和装置
公开(公告)号：US20150021339A1
公开(公告)日：2015-01-22
申请号：US14357418
申请日：2012-11-09
申请人： John T. Felts , Thomas E. Fisk , Robert S. Abrams , John Ferguson , Jonathan R. Freedman , Robert J. Pangborn , Peter J. Sagona , Christopher Weikart
发明人： John T. Felts , Thomas E. Fisk , Robert S. Abrams , John Ferguson , Jonathan R. Freedman , Robert J. Pangborn , Peter J. Sagona , Christopher Weikart
IPC分类号： B65D25/14
CPC分类号： B65D25/14 , A61J1/05 , A61M5/3129 , A61M2005/3109 , A61M2005/3131 , C23C16/045 , C23C16/30 , C23C16/36 , C23C16/401 , C23C16/507
摘要： A method for providing a passivation layer or pH protective coating on a substrate surface by PECVD is provided, the method comprising generating a plasma from a gaseous reactant comprising polymerizing gases. The lubricity, passivation, pH protective, hydrophobicity, and/or barrier properties of the passivation layer or pH protective coating are set by setting the ratio of the O2 to the organosilicon precursor in the precursor feed, and/or by setting the electric power used for generating the plasma. In particular, a passivation layer or pH protective coating made by the method is provided. Pharmaceutical packages coated by the method and the use of such packages protecting a composition contained in the vessel against mechanical and/or chemical effects of the surface of the package without a passivation layer or pH protective coating material are also provided.
摘要翻译：提供了一种通过PECVD在衬底表面上提供钝化层或pH保护涂层的方法，该方法包括从包含聚合气体的气态反应物产生等离子体。钝化层或pH保护涂层的润滑性，钝化性，pH保护性，疏水性和/或阻隔性能通过设定前体进料中O 2与有机硅前体的比例和/或通过设定所用的功率来设定用于产生等离子体。特别地，提供了由该方法制成的钝化层或pH保护涂层。还提供了通过该方法涂覆的药物包装，并且使用这种包装保护容器中包含的组合物免受包装表面的机械和/或化学作用而没有钝化层或pH保护涂层材料。

4. 发明授权

US08911625B2 Spiral wound module including membrane sheet with capillary channels 有权
标题翻译：螺旋缠绕模块包括具有毛细通道的膜片
公开(公告)号：US08911625B2
公开(公告)日：2014-12-16
申请号：US13320756
申请日：2010-07-01
申请人： Gerald F. Billovits , Thomas E. Fisk , Steven D. Jons , David J. Moll
发明人： Gerald F. Billovits , Thomas E. Fisk , Steven D. Jons , David J. Moll
IPC分类号： B01D63/10 , B01D65/00
CPC分类号： B01D63/10 , B01D63/103 , B01D65/003 , B01D2313/04 , B01D2313/146
摘要： The invention includes a spiral wound module comprising at least one membrane sheet wrapped about a permeate collection tube wherein the membrane sheet (14) comprises a plurality of capillary channels in parallel arrangement with each other and which are in fluid communication with the permeate collection tube (12). Many additional embodiments are disclosed along with methods for making and using the module and corresponding components.
摘要翻译：本发明包括螺旋缠绕模块，其包括围绕渗透物收集管缠绕的至少一个膜片，其中所述膜片（14）包括彼此平行布置并与渗透物采集管流体连通的多个毛细通道（ 12）。公开了许多附加实施例以及用于制造和使用模块和相应部件的方法。

5. 发明申请

US20120097597A1 SPIRAL WOUND MODULE INCLUDING MEMBRANE SHEET WITH CAPILLARY CHANNELS 有权
标题翻译：螺旋形模块，包括带有毛细管道的薄膜
公开(公告)号：US20120097597A1
公开(公告)日：2012-04-26
申请号：US13320756
申请日：2010-07-01
申请人： Gerald Billovits , Thomas E. Fisk , Steven D. Jons , David J. Moll
发明人： Gerald Billovits , Thomas E. Fisk , Steven D. Jons , David J. Moll
IPC分类号： B01D63/10
CPC分类号： B01D63/10 , B01D63/103 , B01D65/003 , B01D2313/04 , B01D2313/146
摘要： The invention includes a spiral wound module comprising at least one membrane sheet wrapped about a permeate collection tube wherein the membrane sheet (14) comprises a plurality of capillary channels in parallel arrangement with each other and which are in fluid communication with the permeate collection tube (12). Many additional embodiments are disclosed along with methods for making and using the module and corresponding components.
摘要翻译：本发明包括螺旋缠绕模块，其包括围绕渗透物收集管缠绕的至少一个膜片，其中所述膜片（14）包括彼此平行布置并与渗透物采集管流体连通的多个毛细通道（ 12）。公开了许多附加实施例以及用于制造和使用模块和相应部件的方法。

6. 发明授权

US07985188B2 Vessel, coating, inspection and processing apparatus 有权
标题翻译：船舶，涂料，检验和加工设备
公开(公告)号：US07985188B2
公开(公告)日：2011-07-26
申请号：US12779007
申请日：2010-05-12
申请人： John T. Felts , Thomas E. Fisk , Robert S. Abrams , John Ferguson , Johathan R. Freedman , Robert J. Pangborn , Peter J. Sagona
发明人： John T. Felts , Thomas E. Fisk , Robert S. Abrams , John Ferguson , Johathan R. Freedman , Robert J. Pangborn , Peter J. Sagona
IPC分类号： A61B5/00 , B65D81/00 , C08F2/46 , C08J7/18 , H05H1/00 , H05H1/24 , C23C14/14 , C23C14/16 , B05D3/14 , H01L21/469
CPC分类号： C23C16/50 , A61M5/31513 , B05D1/62 , B05D5/08 , B05D7/02 , B65D25/14 , C23C16/045 , C23C16/401 , C23C16/505 , C23C16/52 , C23C16/54 , G01N15/082 , G01N2033/0096 , Y10T428/24975 , Y10T428/31663
摘要： Methods for processing a vessel, for example to provide a gas barrier or lubricity, are disclosed. First and second PECVD or other vessel processing stations or devices and a vessel holder comprising a vessel port are provided. An opening of the vessel can be seated on the vessel port. The interior surface of the seated vessel can be processed via the vessel port by the first and second processing stations or devices. Vessel barrier, lubricity and hydrophobic coatings and coated vessels, for example syringes and medical sample collection tubes are disclosed. A vessel processing system and vessel inspection apparatus and methods are also disclosed.
摘要翻译：公开了处理容器的方法，例如提供阻气或润滑性。提供第一和第二PECVD或其他容器加工站或装置以及包括容器端口的容器保持器。船只的开口可以坐在船只港口上。坐便器的内表面可以通过第一和第二处理站或设备经容器端口处理。公开了船舶屏障，润滑性和疏水涂层以及涂覆的容器，例如注射器和医用样品收集管。还公开了一种容器处理系统和容器检查装置和方法。

7. 发明授权

US09272095B2 Vessels, contact surfaces, and coating and inspection apparatus and methods 有权
标题翻译：容器，接触面，以及涂层检查装置和方法
公开(公告)号：US09272095B2
公开(公告)日：2016-03-01
申请号：US13436252
申请日：2012-03-30
申请人： John T. Felts , Thomas E. Fisk , Robert Abrams , John Ferguson , Jonathan Freedman , Robert Pangborn , Peter Sagona
发明人： John T. Felts , Thomas E. Fisk , Robert Abrams , John Ferguson , Jonathan Freedman , Robert Pangborn , Peter Sagona
IPC分类号： A61M5/31 , C23C16/02 , C23C16/04 , C23C16/30 , C23C16/36
CPC分类号： A61M5/3129 , A61M2005/3104 , A61M2005/3131 , C23C16/0272 , C23C16/045 , C23C16/30 , C23C16/36
摘要： Methods for processing a contact surface, for example to provide a gas barrier or lubricity or to modify the wetting properties on a medical device, are disclosed. First and second PECVD or other contact surface processing stations or devices and a contact surface holder comprising a contact surface port are provided. An opening of the contact surface can be seated on the contact surface port. The interior contact surface of the seated contact surface can be processed via the contact surface port by the first and second processing stations or devices. contact surface barrier, lubricity and hydrophobic coatings and coated contact surfaces, for example syringes and medical sample collection tubes are disclosed. A contact surface processing system and contact surface inspection apparatus and methods are also disclosed.
摘要翻译：公开了用于处理接触表面的方法，例如提供阻气性或润滑性或改变医疗装置上的润湿性能。提供第一和第二PECVD或其他接触表面处理站或设备以及包括接触表面端口的接触表面保持器。接触表面的开口可以位于接触表面端口上。坐着的接触表面的内部接触表面可以通过第一和第二处理站或设备经由接触表面端口进行处理。公开了接触表面屏障，润滑性和疏水性涂层以及涂覆的接触表面，例如注射器和医用样品收集管。还公开了接触表面处理系统和接触表面检查装置和方法。

8. 发明申请

US20140069202A1 DETECTION OF MECHANICAL STRESS ON COATED ARTICLES 审中-公开
标题翻译：检测涂层制品的机械应力
公开(公告)号：US20140069202A1
公开(公告)日：2014-03-13
申请号：US14003095
申请日：2012-03-14
申请人： Thomas E. Fisk
发明人： Thomas E. Fisk
IPC分类号： A61M5/50 , G01L1/24
CPC分类号： G01L1/24 , A61M5/3129 , A61M5/347 , A61M5/5086 , A61M2005/3104 , A61M2205/0294 , A61M2205/6081
摘要： A medical device comprising a wall, a coating of SiOx, and a piezochromic material is disclosed. The piezochromic material is associated with the wall, and changes its appearance when the wall is exposed to mechanical stress exceeding a threshold intensity. Also disclosed is a method of interrogating a closed medical device for processing damage, comprising at least the acts of providing a closed medical device and inspecting the medical device. The medical device is inspected from the exterior for a change in the appearance of at least some of its piezochromic material that is characteristic of exposure of the wall to mechanical stress exceeding a threshold intensity greater than zero. Optionally in any embodiment inspecting is carried out using a spectrophotometer to determine the change in the color of at least some of its piezochromic material.
摘要翻译：公开了包括壁，SiOx涂层和压敏变色材料的医疗装置。压电变色材料与壁相关联，并且当壁暴露于超过阈值强度的机械应力时改变其外观。还公开了询问用于处理损伤的封闭式医疗装置的方法，至少包括提供封闭的医疗装置和检查医疗装置的动作。医疗设备从外部检查其至少一些其压电色素材料的外观变化，其特征在于壁的机械应力超过超过零的阈值强度。可选地，在任何实施例中，使用分光光度计进行检查以确定其压电色素材料的至少一些的颜色变化。

9. 发明申请

US20130041241A1 PECVD COATING METHODS FOR CAPPED SYRINGES, CARTRIDGES AND OTHER ARTICLES 有权
标题翻译： PECVD涂覆方法用于封盖式注射器，卡盒和其他文章
公开(公告)号：US20130041241A1
公开(公告)日：2013-02-14
申请号：US13651299
申请日：2012-10-12
申请人： John T. Felts , Thomas E. Fisk , Shawn Kinney , Christopher Weikart , Benjamin Hunt , Adrian Raiche , Brian Fitzpatrick , Peter J. Sagona , Adam Stevenson
发明人： John T. Felts , Thomas E. Fisk , Shawn Kinney , Christopher Weikart , Benjamin Hunt , Adrian Raiche , Brian Fitzpatrick , Peter J. Sagona , Adam Stevenson
IPC分类号： A61M5/31 , A61M5/178 , A61M5/30 , A61B5/145 , A61J7/00 , A61M15/00 , A61B6/00 , A61M35/00 , B05D7/22 , A61M5/315
CPC分类号： C23C16/401 , A61B5/1405 , A61B5/15003 , A61B5/150236 , A61B5/150244 , A61B5/150274 , A61B5/150389 , A61B5/150519 , A61B5/150595 , A61B5/150717 , A61B5/150755 , A61B5/153 , A61B5/154 , A61L31/08 , A61M5/3202 , B05D7/22 , C23C16/045 , C23C16/505 , C23C16/52 , C23C16/54 , G01M3/329 , G01N2033/0096
摘要： A method is disclosed in which a vapor-deposited coating or layer is directly or indirectly applied to at least a portion of the internal wall of the barrel of a capped pre-assembly comprising a barrel, optionally a dispensing portion, and a cap. The cap is secured to the barrel and at least substantially isolates the distal opening of the dispensing portion from pressure conditions outside the cap. A vapor-deposited coating or layer is applied directly or indirectly to at least a portion of the internal wall of the barrel while the pre-assembly is capped. The coating or layer is applied under conditions effective to maintain communication from the barrel lumen to the exterior via the front opening, optionally further via the dispensing portion lumen if present, at the end of the applying step. The capped pre-assembly can be pressure tested easily and rapidly, for example with a test duration between 1 and 60 seconds, to determine whether it has container closure integrity.
摘要翻译：公开了一种方法，其中气相沉积的涂层或层直接或间接地施加到包括桶，任选地分配部分和盖的封盖预组件的筒的内壁的至少一部分上。盖被固定到筒体上，并且至少基本上将分配部分的远端开口与帽外的压力条件隔离。当预组件被盖住时，气相沉积的涂层或层直接或间接施加到筒的内壁的至少一部分。在施加步骤结束时，有效地保持通过前开口保持从筒内腔到外部的通信，任选地进一步经由分配部分腔（如果存在）进一步施加涂层或层。封盖预组件可以容易且快速地进行压力测试，例如在1至60秒之间的测试持续时间，以确定其是否具有容器封闭完整性。

10. 发明申请

US20100129646A1 COATED OBJECT 审中-公开
标题翻译：涂层物体
公开(公告)号：US20100129646A1
公开(公告)日：2010-05-27
申请号：US12598132
申请日：2008-05-19
申请人： Thomas E. Fisk , John M. Warakomski , Christina A. Rhoton , Mark G.C. Vreys , Ludo M. Aerts
发明人： Thomas E. Fisk , John M. Warakomski , Christina A. Rhoton , Mark G.C. Vreys , Ludo M. Aerts
IPC分类号： B32B27/00 , B32B5/00 , B05D3/06
CPC分类号： C08G18/757 , C08G18/0895 , C08G18/3206 , C08G18/3212 , C08G18/6674 , Y10T428/265
摘要： A coated object, wherein at least a portion of the surface of the object is an amide containing polymer wherein at least a portion of a surface of the amide containing polymer has a plasma enhanced chemical vapor deposition exposed coating thereon. A method for making a coated object, wherein at least a portion of the surface of the object comprises an amide containing polymer, by the step of coating at least a portion of a surface of the polymer containing an amide group by a plasma enhanced chemical vapor deposition coating process to form a plasma enhanced chemical vapor deposition exposed coating thereon.
摘要翻译：一种涂覆物体，其中物体表面的至少一部分是含酰胺的聚合物，其中含酰胺聚合物的表面的至少一部分具有等离子体增强的化学气相沉积曝光涂层。一种制造涂覆物体的方法，其中所述物体的至少一部分表面包含含酰胺的聚合物，通过以下步骤：通过等离子体增强化学蒸气涂覆含有酰胺基团的聚合物的至少一部分表面的步骤沉积涂覆工艺以在其上形成等离子体增强的化学气相沉积暴露涂层。

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